CH140303A - Process for the preparation of a strong, durable diazo compound. - Google Patents

Process for the preparation of a strong, durable diazo compound.

Info

Publication number
CH140303A
CH140303A CH140303DA CH140303A CH 140303 A CH140303 A CH 140303A CH 140303D A CH140303D A CH 140303DA CH 140303 A CH140303 A CH 140303A
Authority
CH
Switzerland
Prior art keywords
durable
preparation
diazo compound
strong
solution
Prior art date
Application number
Other languages
German (de)
Inventor
Aktiengesellschaft Kalle Co
Original Assignee
Kalle & Co Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kalle & Co Ag filed Critical Kalle & Co Ag
Publication of CH140303A publication Critical patent/CH140303A/en

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  • Photoreceptors In Electrophotography (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

  Verfahren zur Darstellung einer festen, haltbaren     Diazoverbindung.       Gegenstand der vorliegenden Erfindung  ist ein Verfahren zur Darstellung einer festen,  haltbaren     Diazoverbindung,    darin bestehend,  dass man eine Lösung von dianotiertem     o-          Chloranilin    mit     Cadmiumchlorid    versetzt. Das  Endprodukt stellt ein weisses, kristallines,  haltbares, in Wasser lösliches Pulver dar,  welches zur Herstellung von     Azofarbstoffen     Verwendung findet.  



  <I>Beispiel:</I>  Eine aus 128 Teilen     o-Chloranilin,    600  Teilen 15     %iger    Salzsäure und 175 Teilen  40     o/oiger        Natriumnitritlösung    hergestellte       Diazolösung    wird mit einer Lösung von 130  Teilen kristallisiertem     Cadmiumchlorid    in  130 Teilen Wasser versetzt. Die     Diazover-          bindung    scheidet sich alsbald als Cadmium  doppelsalz aus. Die     Abscheidung    kann durch  Zusatz von Kochsalz vervollständigt werden.  Das     Diazosalz    wird     abfiltriert    und in üblicher  Weise fertig gemacht.

   Es stellt ein weisses,  kristallines, haltbares, in Wasser lösliches    Pulver dar, welches zur Herstellung von       Azofarbstoffen    Verwendung findet.



  Process for the preparation of a strong, durable diazo compound. The subject of the present invention is a process for the preparation of a solid, durable diazo compound, which consists in adding cadmium chloride to a solution of dianotized o-chloroaniline. The end product is a white, crystalline, durable, water-soluble powder that is used for the production of azo dyes.



  <I> Example: </I> A diazo solution prepared from 128 parts of o-chloroaniline, 600 parts of 15% hydrochloric acid and 175 parts of 40% sodium nitrite solution is mixed with a solution of 130 parts of crystallized cadmium chloride in 130 parts of water. The diazo compound is soon separated out as a cadmium double salt. The separation can be completed by adding table salt. The diazo salt is filtered off and made ready in the usual way.

   It is a white, crystalline, durable, water-soluble powder which is used for the production of azo dyes.

 

Claims (1)

PATENTANSPRUCH: Verfahren zur Darstellung einer festen, haltbaren Diazoverbindung folgender Kon stitution EMI0001.0020 dadurch gekennzeichnet, dass man eine Lösung von dianotiertem o-Chloranilin mit Cadmium chlorid versetzt. Das Endprodukt stellt ein weisses, kristal lines, haltbares, in Wasser lösliches Pulver dar, welches zur Herstellung von Azofarb- stoffen Verwendung findet. PATENT CLAIM: Process for the preparation of a solid, durable diazo compound of the following constitution EMI0001.0020 characterized in that cadmium chloride is added to a solution of dianotized o-chloroaniline. The end product is a white, crystalline, durable, water-soluble powder which is used to manufacture azo dyes.
CH140303D 1927-07-21 1928-07-19 Process for the preparation of a strong, durable diazo compound. CH140303A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE140303X 1927-07-21
CH138596T 1928-07-19

Publications (1)

Publication Number Publication Date
CH140303A true CH140303A (en) 1930-05-31

Family

ID=25713189

Family Applications (1)

Application Number Title Priority Date Filing Date
CH140303D CH140303A (en) 1927-07-21 1928-07-19 Process for the preparation of a strong, durable diazo compound.

Country Status (1)

Country Link
CH (1) CH140303A (en)

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