CH140303A - Process for the preparation of a strong, durable diazo compound. - Google Patents
Process for the preparation of a strong, durable diazo compound.Info
- Publication number
- CH140303A CH140303A CH140303DA CH140303A CH 140303 A CH140303 A CH 140303A CH 140303D A CH140303D A CH 140303DA CH 140303 A CH140303 A CH 140303A
- Authority
- CH
- Switzerland
- Prior art keywords
- durable
- preparation
- diazo compound
- strong
- solution
- Prior art date
Links
Landscapes
- Photoreceptors In Electrophotography (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Verfahren zur Darstellung einer festen, haltbaren Diazoverbindung. Gegenstand der vorliegenden Erfindung ist ein Verfahren zur Darstellung einer festen, haltbaren Diazoverbindung, darin bestehend, dass man eine Lösung von dianotiertem o- Chloranilin mit Cadmiumchlorid versetzt. Das Endprodukt stellt ein weisses, kristallines, haltbares, in Wasser lösliches Pulver dar, welches zur Herstellung von Azofarbstoffen Verwendung findet.
<I>Beispiel:</I> Eine aus 128 Teilen o-Chloranilin, 600 Teilen 15 %iger Salzsäure und 175 Teilen 40 o/oiger Natriumnitritlösung hergestellte Diazolösung wird mit einer Lösung von 130 Teilen kristallisiertem Cadmiumchlorid in 130 Teilen Wasser versetzt. Die Diazover- bindung scheidet sich alsbald als Cadmium doppelsalz aus. Die Abscheidung kann durch Zusatz von Kochsalz vervollständigt werden. Das Diazosalz wird abfiltriert und in üblicher Weise fertig gemacht.
Es stellt ein weisses, kristallines, haltbares, in Wasser lösliches Pulver dar, welches zur Herstellung von Azofarbstoffen Verwendung findet.
Process for the preparation of a strong, durable diazo compound. The subject of the present invention is a process for the preparation of a solid, durable diazo compound, which consists in adding cadmium chloride to a solution of dianotized o-chloroaniline. The end product is a white, crystalline, durable, water-soluble powder that is used for the production of azo dyes.
<I> Example: </I> A diazo solution prepared from 128 parts of o-chloroaniline, 600 parts of 15% hydrochloric acid and 175 parts of 40% sodium nitrite solution is mixed with a solution of 130 parts of crystallized cadmium chloride in 130 parts of water. The diazo compound is soon separated out as a cadmium double salt. The separation can be completed by adding table salt. The diazo salt is filtered off and made ready in the usual way.
It is a white, crystalline, durable, water-soluble powder which is used for the production of azo dyes.
Claims (1)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE140303X | 1927-07-21 | ||
CH138596T | 1928-07-19 |
Publications (1)
Publication Number | Publication Date |
---|---|
CH140303A true CH140303A (en) | 1930-05-31 |
Family
ID=25713189
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH140303D CH140303A (en) | 1927-07-21 | 1928-07-19 | Process for the preparation of a strong, durable diazo compound. |
Country Status (1)
Country | Link |
---|---|
CH (1) | CH140303A (en) |
-
1928
- 1928-07-19 CH CH140303D patent/CH140303A/en unknown
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