CH116505A - Process for the production of a new dye. - Google Patents
Process for the production of a new dye.Info
- Publication number
- CH116505A CH116505A CH116505DA CH116505A CH 116505 A CH116505 A CH 116505A CH 116505D A CH116505D A CH 116505DA CH 116505 A CH116505 A CH 116505A
- Authority
- CH
- Switzerland
- Prior art keywords
- production
- new dye
- dye
- new
- yellow
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 3
- 239000000975 dye Substances 0.000 claims description 9
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 6
- DYRDKSSFIWVSNM-UHFFFAOYSA-N acetoacetanilide Chemical compound CC(=O)CC(=O)NC1=CC=CC=C1 DYRDKSSFIWVSNM-UHFFFAOYSA-N 0.000 claims description 3
- QOWZHEWZFLTYQP-UHFFFAOYSA-K chromium(3+);triformate Chemical compound [Cr+3].[O-]C=O.[O-]C=O.[O-]C=O QOWZHEWZFLTYQP-UHFFFAOYSA-K 0.000 claims description 3
- 230000008878 coupling Effects 0.000 claims description 3
- 238000010168 coupling process Methods 0.000 claims description 3
- 238000005859 coupling reaction Methods 0.000 claims description 3
- 239000002253 acid Substances 0.000 claims description 2
- 239000000987 azo dye Substances 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 235000011121 sodium hydroxide Nutrition 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 210000002268 wool Anatomy 0.000 claims description 2
- 239000000243 solution Substances 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000011651 chromium Substances 0.000 description 1
- 235000002639 sodium chloride Nutrition 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B45/00—Complex metal compounds of azo dyes
- C09B45/02—Preparation from dyes containing in o-position a hydroxy group and in o'-position hydroxy, alkoxy, carboxyl, amino or keto groups
- C09B45/14—Monoazo compounds
- C09B45/16—Monoazo compounds containing chromium
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Coloring (AREA)
Description
Zusatzpatent zum Hauptpateut Nr. 111564. I Verfahren zur Herstellung eines neuen Farbstoffes. Es wurde gefunden, dass man einen neuen Farbstoff erhält, wenn man den Azofarb- stoff, welcher durch Kuppeln von diazotier- ter 4-Nitro-2-amino-l-phenol-6-sulfosäure mit Acetessiganilid erhalten wird, mit Chrom- formiat behandelt.
Der neue Farbstoff bil det ein braunes Pulver, löst sich in Wasser mit gelber, in verdünnter Natronlauge mit oranger Farbe und färbt Wolle aus saurem Bade in sehr gleichmässigen, echten, rot stichig gelben Tönen an. Beispiel: 44,4 Teile des Farbstoffes, erhalten durch Kuppeln von 4-Nitro-2-diazo-l-phenol-6- sulfosäure mit Acetessiganilid, werden einige Zeit in wässeriger Lösung mit einer Chromformiatlösung, entsprechend 22,5 Tei- len Cr,03, erwärmt. Die Lösung wird so dann eingedampft und der Farbstoff mit Kochsalz ausgefällt.
Additional patent to the main patron No. 111564. I Process for the production of a new dye. It has been found that a new dye is obtained if the azo dye, which is obtained by coupling diazotized 4-nitro-2-amino-1-phenol-6-sulfonic acid with acetoacetanilide, is treated with chromium formate .
The new dye forms a brown powder, dissolves in water with yellow, in dilute caustic soda with orange color and dyes wool from acid baths in very even, genuine, red-tinged yellow tones. Example: 44.4 parts of the dye, obtained by coupling 4-nitro-2-diazo-1-phenol-6-sulfonic acid with acetoacetanilide, are for some time in an aqueous solution with a chromium formate solution, corresponding to 22.5 parts of Cr, 03, warmed up. The solution is then evaporated and the dye is precipitated with common salt.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH116505T | 1924-06-17 | ||
| CH111564T | 1924-06-17 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH116505A true CH116505A (en) | 1926-09-01 |
Family
ID=25707871
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH116505D CH116505A (en) | 1924-06-17 | 1924-06-17 | Process for the production of a new dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH116505A (en) |
-
1924
- 1924-06-17 CH CH116505D patent/CH116505A/en unknown
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