CA2966361A1 - Production of a spinel material - Google Patents

Production of a spinel material Download PDF

Info

Publication number
CA2966361A1
CA2966361A1 CA2966361A CA2966361A CA2966361A1 CA 2966361 A1 CA2966361 A1 CA 2966361A1 CA 2966361 A CA2966361 A CA 2966361A CA 2966361 A CA2966361 A CA 2966361A CA 2966361 A1 CA2966361 A1 CA 2966361A1
Authority
CA
Canada
Prior art keywords
lmo
lithium
cathode
manganese
cell
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
CA2966361A
Other languages
English (en)
French (fr)
Inventor
Kenneth Ikechukwu Ozoemena
Funeka NKOSI
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Council for Scientific and Industrial Research CSIR
Original Assignee
Council for Scientific and Industrial Research CSIR
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Council for Scientific and Industrial Research CSIR filed Critical Council for Scientific and Industrial Research CSIR
Publication of CA2966361A1 publication Critical patent/CA2966361A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00Compounds of manganese
    • C01G45/12Complex oxides containing manganese and at least one other metal element
    • C01G45/1221Manganates or manganites with trivalent manganese, tetravalent manganese or mixtures thereof
    • C01G45/1242Manganates or manganites with trivalent manganese, tetravalent manganese or mixtures thereof of the type (Mn2O4)-, e.g. LiMn2O4 or Li(MxMn2-x)O4
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/052Li-accumulators
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/052Li-accumulators
    • H01M10/0525Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/058Construction or manufacture
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/30Three-dimensional structures
    • C01P2002/32Three-dimensional structures spinel-type (AB2O4)
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/50Solid solutions
    • C01P2002/52Solid solutions containing elements as dopants
    • C01P2002/54Solid solutions containing elements as dopants one element only
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/70Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/80Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/82Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by IR- or Raman-data
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/80Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/85Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by XPS, EDX or EDAX data
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/01Particle morphology depicted by an image
    • C01P2004/03Particle morphology depicted by an image obtained by SEM
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/01Particle morphology depicted by an image
    • C01P2004/04Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/40Electric properties
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M2004/026Electrodes composed of, or comprising, active material characterised by the polarity
    • H01M2004/028Positive electrodes
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/50Manufacturing or production processes characterised by the final manufactured product

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Secondary Cells (AREA)
CA2966361A 2014-10-31 2015-10-30 Production of a spinel material Abandoned CA2966361A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
ZA2014/07986 2014-10-31
ZA201407986 2014-10-31
PCT/ZA2015/050019 WO2016070205A2 (en) 2014-10-31 2015-10-30 Production of a spinel material

Publications (1)

Publication Number Publication Date
CA2966361A1 true CA2966361A1 (en) 2016-05-06

Family

ID=55802547

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2966361A Abandoned CA2966361A1 (en) 2014-10-31 2015-10-30 Production of a spinel material

Country Status (9)

Country Link
US (1) US20180277844A1 (enExample)
EP (1) EP3212578A2 (enExample)
JP (1) JP2018500722A (enExample)
KR (1) KR20170078791A (enExample)
CN (1) CN107108260B (enExample)
AR (1) AR102483A1 (enExample)
BR (1) BR112017009040B1 (enExample)
CA (1) CA2966361A1 (enExample)
WO (1) WO2016070205A2 (enExample)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20180375097A1 (en) * 2015-12-22 2018-12-27 Csir Spinel material
US11024898B2 (en) * 2017-02-22 2021-06-01 Toyota Motor Europe Lithium-ion battery high temperature aging process
EP3412633A1 (en) * 2017-06-08 2018-12-12 Basf Se Process for manufacturing an electrode active material
CL2017002221A1 (es) * 2017-09-01 2018-01-19 Univ Antofagasta Espinela de manganeso dopada con magnesio, material catódico que la comprende, método de preparación, y batería de ion litio que la comprende
US11621416B2 (en) * 2017-10-09 2023-04-04 Csir Campus Cathode material
CN107887600B (zh) * 2017-11-07 2020-05-05 哈尔滨工业大学 一种锂离子电池用预激活富锂锰基正极材料的制备方法
KR102533794B1 (ko) * 2018-11-30 2023-05-19 주식회사 엘지에너지솔루션 팔면체 구조의 리튬 망간계 양극 활물질, 이를 포함하는 양극 및 리튬 이차전지
KR102394065B1 (ko) * 2020-09-07 2022-05-09 한국에너지기술연구원 고결정성 리튬-금속 산화물 입자 및 이의 제조방법

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH09320603A (ja) * 1996-03-28 1997-12-12 Aichi Steel Works Ltd リチウム二次電池用粉末状活物質の製造方法
DE19815611A1 (de) * 1998-04-07 1999-10-14 Riedel De Haen Gmbh Verfahren zur Herstellung von Lithium-Metall-Oxiden
JP4360143B2 (ja) * 2003-07-17 2009-11-11 株式会社豊田中央研究所 リチウム二次電池用活物質の製造方法
CN1249832C (zh) * 2004-02-16 2006-04-05 厦门大学 一种锂锰氧化物的制备方法及其在电池中的应用
CN102790203B (zh) * 2011-05-19 2016-03-30 中国科学院宁波材料技术与工程研究所 一种锂离子电池正极材料的制备方法
US9834854B2 (en) * 2012-08-10 2017-12-05 Csir Production of a spinel material
JP6081782B2 (ja) * 2012-11-23 2017-02-15 日本ケミコン株式会社 リチウムイオン二次電池用電極材料、リチウムイオン二次電池用電極材料の製造方法、及びリチウムイオン二次電池

Also Published As

Publication number Publication date
KR20170078791A (ko) 2017-07-07
BR112017009040A2 (pt) 2018-07-03
JP2018500722A (ja) 2018-01-11
EP3212578A2 (en) 2017-09-06
WO2016070205A2 (en) 2016-05-06
AR102483A1 (es) 2017-03-01
BR112017009040B1 (pt) 2022-06-14
US20180277844A1 (en) 2018-09-27
WO2016070205A3 (en) 2016-09-09
CN107108260A (zh) 2017-08-29
CN107108260B (zh) 2019-08-23

Similar Documents

Publication Publication Date Title
Kim et al. Li-ion diffusivity and electrochemical performance of Ni-rich cathode material doped with fluoride ions
US11183692B2 (en) Production of a layered lithium-manganese-nickel-cobalt oxide material
Sun et al. The effect of cation mixing controlled by thermal treatment duration on the electrochemical stability of lithium transition-metal oxides
Jamil et al. Improved high-voltage performance of LiNi0. 87Co0. 1Al0. 03O2 by Li+-conductor coating
KR102402147B1 (ko) 마그네슘으로 도핑된 망간 스피넬, 상기 망간 스피넬을 포함하는 캐소드 재료, 이들의 조제 방법 및 상기 스피넬을 포함하는 리튬 이온 배터리
CA2966361A1 (en) Production of a spinel material
Saroha et al. Electrochemical performances of Li-rich layered-layered Li2MnO3-LiMnO2 solid solutions as cathode material for lithium-ion batteries
Yang et al. Preparing LiNi0. 5Mn1. 5O4 nanoplates with superior properties in lithium-ion batteries using bimetal–organic coordination-polymers as precursors
Wen et al. Effects of magnesium and fluorine co-doping on the structural and electrochemical performance of the spinel LiMn2O4 cathode materials
JP7412264B2 (ja) リチウムイオン二次電池用正極活物質およびその製造方法
Kocak et al. The effect of vanadium doping on the cycling performance of LiNi0. 5Mn1. 5O4 spinel cathode for high voltage lithium-ion batteries
CA2880876C (en) Production of a spinel material
Zhu et al. Facile synthesis of truncated octahedron LiNi0. 10Mn1. 90O4 for high-performance Li-ion batteries
Ajayi et al. Atmospheric plasma spray pyrolysis of lithiated nickel-manganese-cobalt oxides for cathodes in lithium ion batteries
Zeng et al. Effect of cationic and anionic substitutions on the electrochemical properties of LiNi0. 5Mn1. 5O4 spinel cathode materials
Wang et al. Role of fluorine surface modification in improving electrochemical cyclability of concentration gradient Li [Ni 0.73 Co 0.12 Mn 0.15] O 2 cathode material for Li-ion batteries
Peng et al. Electrochemical performance of spinel LiAlxMn2− xO4 prepared rapidly by glucose-assisted solid-state combustion synthesis
Zhu et al. A layered/spinel heterostructured cathode for Li-ion batteries prepared by ultrafast Joule heating
JP7185838B2 (ja) 高強度リチウムイオン二次電池用正極活物質の製造方法
Nyamaa et al. Enhanced LiMn 2 O 4 cathode performance in lithium-ion batteries through synergistic cation and anion substitution
Liu et al. Improved electrochemical performance of Co-free Ni-rich cathode material for lithium-ion battery through multi-element composite modification
Liang et al. Preparation of Ni–Zn dual-doped polyhedral LiMn2O4 for endurable cycling lithium ion batteries at high rate
Raja et al. Alanine-assisted low-temperature combustion synthesis of nanocrystalline LiMn2O4 for lithium-ion batteries
Chen et al. A boron-nitride based dispersive composite coating on nickel-rich layered cathodes for enhanced cycle stability and safety
Arof et al. Electrochemical properties of LiMn2O4 prepared with tartaric acid chelating agent

Legal Events

Date Code Title Description
FZDE Discontinued

Effective date: 20191030