CA2963565A1 - Process for concentration of lithium containing solutions - Google Patents

Process for concentration of lithium containing solutions Download PDF

Info

Publication number
CA2963565A1
CA2963565A1 CA2963565A CA2963565A CA2963565A1 CA 2963565 A1 CA2963565 A1 CA 2963565A1 CA 2963565 A CA2963565 A CA 2963565A CA 2963565 A CA2963565 A CA 2963565A CA 2963565 A1 CA2963565 A1 CA 2963565A1
Authority
CA
Canada
Prior art keywords
solution
membrane
flow
lithium
chamber
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
CA2963565A
Other languages
English (en)
French (fr)
Inventor
Jackson R. Switzer
Neal J. Colonius
Chi Hung Cheng
Pieter Johannes Daudey
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Albemarle Corp
Original Assignee
Albemarle Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Albemarle Corp filed Critical Albemarle Corp
Publication of CA2963565A1 publication Critical patent/CA2963565A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/58Multistep processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/002Forward osmosis or direct osmosis
    • B01D61/0021Forward osmosis or direct osmosis comprising multiple forward osmosis steps
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/02Reverse osmosis; Hyperfiltration ; Nanofiltration
    • B01D61/025Reverse osmosis; Hyperfiltration
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00Lithium compounds
    • C01D15/04Halides
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/44Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
    • C02F1/441Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by reverse osmosis
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/44Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
    • C02F1/445Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by forward osmosis
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2311/00Details relating to membrane separation process operations and control
    • B01D2311/25Recirculation, recycling or bypass, e.g. recirculation of concentrate into the feed
    • B01D2311/252Recirculation of concentrate
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2315/00Details relating to the membrane module operation
    • B01D2315/10Cross-flow filtration
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/02Non-contaminated water, e.g. for industrial water supply
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/08Seawater, e.g. for desalination
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/10Nature of the water, waste water, sewage or sludge to be treated from quarries or from mining activities
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2209/00Controlling or monitoring parameters in water treatment
    • C02F2209/001Upstream control, i.e. monitoring for predictive control
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2209/00Controlling or monitoring parameters in water treatment
    • C02F2209/02Temperature
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2301/00General aspects of water treatment
    • C02F2301/08Multistage treatments, e.g. repetition of the same process step under different conditions
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A20/00Water conservation; Efficient water supply; Efficient water use
    • Y02A20/124Water desalination
    • Y02A20/131Reverse-osmosis
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W10/00Technologies for wastewater treatment
    • Y02W10/30Wastewater or sewage treatment systems using renewable energies
    • Y02W10/37Wastewater or sewage treatment systems using renewable energies using solar energy

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Environmental & Geological Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Nanotechnology (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
CA2963565A 2014-10-20 2015-10-16 Process for concentration of lithium containing solutions Abandoned CA2963565A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201462065965P 2014-10-20 2014-10-20
US62/065,965 2014-10-20
PCT/US2015/056090 WO2016064689A2 (en) 2014-10-20 2015-10-16 Process for concentration of lithium containing solutions

Publications (1)

Publication Number Publication Date
CA2963565A1 true CA2963565A1 (en) 2016-04-28

Family

ID=55310889

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2963565A Abandoned CA2963565A1 (en) 2014-10-20 2015-10-16 Process for concentration of lithium containing solutions

Country Status (8)

Country Link
US (1) US20180147532A1 (https=)
JP (1) JP2017532197A (https=)
KR (1) KR20170071502A (https=)
AR (1) AR102363A1 (https=)
AU (1) AU2015336234A1 (https=)
CA (1) CA2963565A1 (https=)
CL (2) CL2017000964A1 (https=)
WO (1) WO2016064689A2 (https=)

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JP2018118186A (ja) * 2017-01-23 2018-08-02 株式会社東芝 正浸透膜および水処理システム
AR112663A1 (es) 2017-08-02 2019-11-27 Lilac Solutions Inc Extracción de litio con perlas porosas de intercambio iónico
US10439200B2 (en) 2017-08-02 2019-10-08 Lilac Solutions, Inc. Ion exchange system for lithium extraction
US10648090B2 (en) 2018-02-17 2020-05-12 Lilac Solutions, Inc. Integrated system for lithium extraction and conversion
KR102667270B1 (ko) * 2018-02-17 2024-05-17 리락 솔루션즈, 인크. 리튬 추출 및 전환을 위한 통합 시스템
KR20200116526A (ko) 2018-02-28 2020-10-12 리락 솔루션즈, 인크. 리튬 추출을 위한 입자 트랩을 가진 이온 교환 반응기
US11235282B2 (en) * 2018-03-09 2022-02-01 Terralithium Llc Processes for producing lithium compounds using forward osmosis
US11174532B1 (en) 2018-03-09 2021-11-16 Terralithium Llc Processes for producing lithium compounds using reverse osmosis
WO2020033668A1 (en) * 2018-08-09 2020-02-13 Ut-Battelle, Llc Forward osmosis composite membranes for concentration of lithium containing solutions
JP7186557B2 (ja) * 2018-09-14 2022-12-09 旭化成株式会社 溶媒含有物品の濃縮システム
CL2020001650A1 (es) 2019-06-18 2021-01-29 Schlumberger Technology Bv Extracción de litio
CN112108001B (zh) * 2019-06-20 2022-09-13 国家能源投资集团有限责任公司 一种反渗透系统及其浓缩含锂盐水的方法
US12297519B2 (en) 2019-09-25 2025-05-13 Veolia Water Solutions & Technologies Support Energy efficient process for concentrating and recovering lithium from a lithium containing brine
KR20220119166A (ko) 2020-01-09 2022-08-26 리락 솔루션즈, 인크. 바람직하지 않은 금속의 분리 방법
GB202003685D0 (en) * 2020-03-13 2020-04-29 Ide Projects Ltd Forward osmotic separation system and method
CA3178825A1 (en) 2020-06-09 2021-12-16 David Henry SNYDACKER Lithium extraction in the presence of scalants
US12391566B2 (en) 2020-08-21 2025-08-19 Schlumberger Technology Corporation Lithium extraction improvements
CA3199218A1 (en) 2020-11-20 2022-05-27 David Henry SNYDACKER Lithium production with volatile acid
KR20240014047A (ko) 2021-04-23 2024-01-31 리락 솔루션즈, 인크. 리튬 추출을 위한 이온 교환 장치
AU2022317068A1 (en) 2021-07-30 2024-02-15 Schlumberger Technology B.V. Lithium recovery thermal management
US20230032153A1 (en) * 2021-07-30 2023-02-02 Schlumberger Technology Corporation Lithium purification and conversion
US12215035B2 (en) * 2021-07-30 2025-02-04 Schlumberger Technology Corporation Lithium purification and conversion
US20250128211A1 (en) * 2021-08-26 2025-04-24 Massachusetts Institute Of Technology Harnessing Metal Ions from Brines
US12590539B2 (en) 2022-03-14 2026-03-31 Schlumberger Technology Corporation Systems and methods for analysis of drilling fluid
EP4499260A4 (en) 2022-03-28 2026-04-01 Lilac Solutions Inc DEVICES FOR THE EFFICIENT USE OF SORBANTS IN LITHIUM EXTRACTION
AR128953A1 (es) 2022-04-01 2024-06-26 Lilac Solutions Inc Extracción de litio con aditivos químicos
EP4519471A1 (en) 2022-05-04 2025-03-12 Services Pétroliers Schlumberger Lithium recovery using aqueous sources
US11502323B1 (en) 2022-05-09 2022-11-15 Rahul S Nana Reverse electrodialysis cell and methods of use thereof
US11502322B1 (en) 2022-05-09 2022-11-15 Rahul S Nana Reverse electrodialysis cell with heat pump
US12421137B2 (en) 2022-12-07 2025-09-23 Schlumberger Technology Corporation Hydrocarbon and sulfide removal in direct aqueous extraction
WO2024123398A1 (en) 2022-12-07 2024-06-13 Schlumberger Technology Corporation Hydrocarbon and sulfide removal in direct aqueous extraction
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JP2025538227A (ja) 2022-11-15 2025-11-26 エス ナナ,ラフル 逆電気透析または圧力遅延浸透セルおよびその使用方法
WO2025012681A1 (es) * 2023-07-11 2025-01-16 Universidad Católica De La Santísima Concepción Sistema y método para concentración de salmueras de litio y purificación de agua
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Also Published As

Publication number Publication date
AR102363A1 (es) 2017-02-22
WO2016064689A3 (en) 2016-07-28
AU2015336234A1 (en) 2017-04-20
US20180147532A1 (en) 2018-05-31
CL2017000964A1 (es) 2017-11-03
WO2016064689A2 (en) 2016-04-28
JP2017532197A (ja) 2017-11-02
CL2019002546A1 (es) 2019-11-15
KR20170071502A (ko) 2017-06-23

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Legal Events

Date Code Title Description
FZDE Discontinued

Effective date: 20220106