CA2872333C - Procede de fractionnement de la lignine - Google Patents

Procede de fractionnement de la lignine Download PDF

Info

Publication number
CA2872333C
CA2872333C CA2872333A CA2872333A CA2872333C CA 2872333 C CA2872333 C CA 2872333C CA 2872333 A CA2872333 A CA 2872333A CA 2872333 A CA2872333 A CA 2872333A CA 2872333 C CA2872333 C CA 2872333C
Authority
CA
Canada
Prior art keywords
lignin
mixture
present
fractions
organic solvent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CA2872333A
Other languages
English (en)
Other versions
CA2872333A1 (fr
Inventor
Kati Eskelinen
Sanna VALKONEN
Suvi Pietarinen
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
UPM Kymmene Oy
Original Assignee
UPM Kymmene Oy
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by UPM Kymmene Oy filed Critical UPM Kymmene Oy
Publication of CA2872333A1 publication Critical patent/CA2872333A1/fr
Application granted granted Critical
Publication of CA2872333C publication Critical patent/CA2872333C/fr
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08H—DERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
    • C08H6/00—Macromolecular compounds derived from lignin, e.g. tannins, humic acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07G—COMPOUNDS OF UNKNOWN CONSTITUTION
    • C07G1/00—Lignin; Lignin derivatives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
    • C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
    • C08L23/04—Homopolymers or copolymers of ethene
    • C08L23/06—Polyethene
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L97/00—Compositions of lignin-containing materials
    • C08L97/005—Lignin
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J197/00—Adhesives based on lignin-containing materials
    • C09J197/005—Lignin
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
    • D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
    • D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
    • D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
    • D01F9/16—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from products of vegetable origin or derivatives thereof, e.g. from cellulose acetate
    • D01F9/17—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from products of vegetable origin or derivatives thereof, e.g. from cellulose acetate from lignin

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Polymers & Plastics (AREA)
  • Medicinal Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Textile Engineering (AREA)
  • Compounds Of Unknown Constitution (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)

Abstract

Cette invention concerne un procédé de fractionnement de la lignine, le procédé comprenant les étapes suivantes : (i) dissolution de la lignine dans un mélange contenant un solvant organique et de l'eau ; et (ii) ultrafiltration du mélange formé à l'étape (i) par passage par une ou plusieurs membranes de filtration pour obtenir un nombre prédéfini de fractions de lignine, chaque fraction contenant une lignine ayant un poids moléculaire dans une plage prédéfinie. Cette invention concerne également une fraction de lignine et ses utilisations.
CA2872333A 2012-06-06 2013-06-05 Procede de fractionnement de la lignine Active CA2872333C (fr)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FI20125613 2012-06-06
FI20125613A FI127816B (en) 2012-06-06 2012-06-06 Process for fractionating lignin
PCT/FI2013/050607 WO2013182751A1 (fr) 2012-06-06 2013-06-05 Procédé de fractionnement de la lignine

Publications (2)

Publication Number Publication Date
CA2872333A1 CA2872333A1 (fr) 2013-12-12
CA2872333C true CA2872333C (fr) 2020-07-07

Family

ID=48703598

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2872333A Active CA2872333C (fr) 2012-06-06 2013-06-05 Procede de fractionnement de la lignine

Country Status (7)

Country Link
US (1) US9896469B2 (fr)
EP (2) EP2859006B1 (fr)
BR (1) BR112014029231B1 (fr)
CA (1) CA2872333C (fr)
CL (1) CL2014003318A1 (fr)
FI (1) FI127816B (fr)
WO (1) WO2013182751A1 (fr)

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2596852A1 (fr) * 2011-11-28 2013-05-29 Annikki GmbH Procédé de préparation d'une solution aqueuse contenant de la lignine
FI126737B (en) 2013-11-26 2017-04-28 Upm Kymmene Corp Process for treating lignin and preparing a binder composition
FI126736B (en) 2013-11-26 2017-04-28 Upm Kymmene Corp A process for treating lignin and preparing a binder composition
WO2015137861A1 (fr) * 2014-03-12 2015-09-17 Ren Fuel K2B Ab Procédé de traitement de liqueur noire
US10458066B2 (en) * 2014-08-01 2019-10-29 Organic Chemical Llc Process for the isolation of lignin from black liquor and modification of the lignin for plastic applications
SE538572C2 (en) 2014-12-22 2016-09-20 Innventia Ab Method of producing lignin with reduced amount of odorous substances
SE539560C2 (en) * 2015-03-06 2017-10-10 Innventia Ab Electrode active coating for a lithium-ion battery and method of production therefore
DE102015120377A1 (de) * 2015-11-25 2017-06-01 Deutsche Institute Für Textil- Und Faserforschung Denkendorf Verfahren zur Herstellung einer Lignin-basierten Zusammensetzung
SE540485C2 (en) 2016-06-22 2018-09-25 Valmet Oy Method of producing lignin with reduced amount of odorous substances
IT201600068623A1 (it) * 2016-07-01 2018-01-01 Upm Kymmene Corp “use of a lignin fraction as an anti-phytopathogenic agent and anti-phytopathogenic compositions comprising the same” / “uso di una frazione di lignina come agente antifitopatogenico e composizioni antifitopatogeniche che la comprendono”
EP3481939A4 (fr) * 2016-07-06 2020-02-26 Virdia, Inc. Procédés de raffinage d'un hydrolysat lignocellulosique
GB201614578D0 (en) * 2016-08-26 2016-10-12 Univ Court Of The Univ Of St Andrews The Modified lignin and separation methods
AT519535A1 (de) 2016-12-23 2018-07-15 Univ Wien Tech Herstellungsverfahren
EP3676314A4 (fr) * 2017-08-31 2021-06-09 Attis Innovations, LLC Procédé de séparation et de récupération de lignine et de polymères de biolignine fluides fusibles
WO2019081819A1 (fr) * 2017-10-26 2019-05-02 Aalto University Foundation Sr Dispersions aqueuses de lignine et procédés de préparation associés
FI20205740A1 (en) * 2017-12-22 2020-07-09 Green Innovation Gmbh Use of lignin fraction as an ingredient in dietary supplements for humans and animals
WO2019165443A1 (fr) * 2018-02-26 2019-08-29 The Texas A&M University System Fractionnement et fabrication de lignine pour fibre de carbone de qualité
AT521393B1 (de) 2018-06-27 2021-02-15 Univ Wien Tech Verfahren zur Herstellung von Ligninpartikel im Rahmen eines kontinuierlichen Verfahrens
IT201800006764A1 (it) * 2018-06-28 2019-12-28 Trattamento delle acque reflue delle cartiere.
CN109456496A (zh) * 2018-11-26 2019-03-12 广州楹鼎生物科技有限公司 一种木质素的纯化方法
EP3922664A1 (fr) 2020-06-10 2021-12-15 Borealis AG Mélange de lignine-phénol stable à utiliser dans des résines de phénol-formaldéhyde modifiées par de la lignine
EP4242252A1 (fr) 2022-03-07 2023-09-13 Borealis AG Procédé de préparation d'un mélange lignine-phénol stable et mélange lignine-phénol stable obtenu selon ledit procédé

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FI62114C (fi) 1979-11-05 1982-11-10 Flowcon Oy Ligninprodukt foer att goera cement och andra finfoerdelade mieralmaterial laettflytande
SE453840B (sv) * 1984-12-21 1988-03-07 Mo Och Domsjoe Ab Forfarande vid framstellning av cellulosamassa
JPS6290389A (ja) 1985-10-14 1987-04-24 王子製紙株式会社 アルカリ性パルプ蒸解廃液の処理方法
EP0364632A1 (fr) 1988-10-17 1990-04-25 Zeneca Limited Récupération de la lignine
US5202403A (en) * 1992-01-15 1993-04-13 Georgia-Pacific Resins, Inc. Lignin modified phenol-formaldehyde resins
US5749926A (en) * 1996-09-12 1998-05-12 Westvaco Corporation Method of preparing high activity sulfonated lignin dye dispersants
US5777086A (en) * 1997-05-12 1998-07-07 Thermo Fibergen, Inc. Method of recovering lignin from pulp and paper sludge
US6172204B1 (en) * 1999-06-04 2001-01-09 Regents Of The University Of Minnesota Compositions based on lignin derivatives
US20020065400A1 (en) * 2000-04-06 2002-05-30 Mikhail Raskin Resin material and method of producing same
US8585863B2 (en) * 2007-09-21 2013-11-19 Api Intellectual Property Holdings, Llc Separation of lignin from hydrolyzate
JP5062593B2 (ja) * 2007-12-03 2012-10-31 独立行政法人産業技術総合研究所 リグニンを原料とする炭素微粒子及びその製造方法
WO2010106182A1 (fr) * 2009-03-20 2010-09-23 Sika Technology Ag Procédé de fabrication de produits de dégradation de la lignine chimiquement modifiés
EP2298710A1 (fr) * 2009-09-21 2011-03-23 Sika Technology AG Additif pour liant minéral
CA2800234C (fr) * 2010-03-08 2018-08-28 Forestry And Forest Products Research Institute Agent de stabilisation de ligninases
BR112013003100A2 (pt) * 2010-08-11 2016-06-28 Iogen Energy Corp reciclagem de lixiviado durante o processo de conversão lignocelulósica
CA2812685A1 (fr) * 2010-09-23 2012-03-29 Toho Tenax Europe Gmbh Lignine thermoplastique pour la fabrication de fibres de carbone
AT510812A1 (de) * 2010-10-29 2012-06-15 Annikki Gmbh Verfahren zur gewinnung von lignin
BR112013025862A2 (pt) * 2011-04-07 2017-11-14 Virdia Ltd composições de lignina, métodos de produzir as composições, métodos de utilizar composições de lignina e produtos produzidos desse modo
EP2596852A1 (fr) * 2011-11-28 2013-05-29 Annikki GmbH Procédé de préparation d'une solution aqueuse contenant de la lignine
FI123934B (en) * 2012-03-29 2013-12-31 Upm Kymmene Corp Use of low molecular weight lignin to prepare a binder composition
FI127010B (en) * 2012-08-24 2017-09-29 Upm Kymmene Corp Process for the recovery of low molecular weight lignin from a filtrate

Also Published As

Publication number Publication date
FI20125613A (fi) 2013-12-07
BR112014029231A2 (pt) 2017-06-27
WO2013182751A1 (fr) 2013-12-12
EP2859006B1 (fr) 2019-01-02
EP2859006A1 (fr) 2015-04-15
CL2014003318A1 (es) 2015-03-06
US9896469B2 (en) 2018-02-20
CA2872333A1 (fr) 2013-12-12
FI127816B (en) 2019-03-15
US20150183813A1 (en) 2015-07-02
EP3495375A1 (fr) 2019-06-12
BR112014029231B1 (pt) 2019-11-12

Similar Documents

Publication Publication Date Title
CA2872333C (fr) Procede de fractionnement de la lignine
CA2856145C (fr) Procede d'augmentation de la reactivite de la lignine
US10017636B2 (en) Use of low molecular weight lignin together with lignin for the production of a phenol-formaldehyde binder composition
US20230339998A1 (en) Method of making a binder composition, and binder composition
FI124944B (fi) Menetelmä sideainekoostumuksen valmistamiseksi, sideainekoostumus, liima-ainekoostumus, kerrostettu komposiittirakenne, ja sideainekoostumuksen ja liimakoostumuksen käyttöjä
US10301437B2 (en) Method for treating lignin and for producing a binder composition
DE202014011146U1 (de) Reaktives Lignin
AU2014301654A1 (en) Phenolic resin obtained by polycondensation of formaldehyde, phenol and lignin

Legal Events

Date Code Title Description
EEER Examination request

Effective date: 20180605