CA2335927A1 - Dispersions a base de titanate de baryum - Google Patents
Dispersions a base de titanate de baryum Download PDFInfo
- Publication number
- CA2335927A1 CA2335927A1 CA002335927A CA2335927A CA2335927A1 CA 2335927 A1 CA2335927 A1 CA 2335927A1 CA 002335927 A CA002335927 A CA 002335927A CA 2335927 A CA2335927 A CA 2335927A CA 2335927 A1 CA2335927 A1 CA 2335927A1
- Authority
- CA
- Canada
- Prior art keywords
- particles
- slurry
- dispersion
- slip
- aqueous medium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
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- 239000006185 dispersion Substances 0.000 title claims abstract description 80
- 229910002113 barium titanate Inorganic materials 0.000 title claims description 103
- JRPBQTZRNDNNOP-UHFFFAOYSA-N barium titanate Chemical compound [Ba+2].[Ba+2].[O-][Ti]([O-])([O-])[O-] JRPBQTZRNDNNOP-UHFFFAOYSA-N 0.000 title claims description 100
- 239000002245 particle Substances 0.000 claims abstract description 245
- 239000002002 slurry Substances 0.000 claims abstract description 80
- 238000000576 coating method Methods 0.000 claims abstract description 54
- 238000000034 method Methods 0.000 claims abstract description 46
- 238000002156 mixing Methods 0.000 claims abstract description 45
- 229910052751 metal Inorganic materials 0.000 claims abstract description 43
- 239000002184 metal Substances 0.000 claims abstract description 43
- -1 organic acid salt Chemical class 0.000 claims abstract description 43
- 239000011248 coating agent Substances 0.000 claims abstract description 41
- 239000012736 aqueous medium Substances 0.000 claims abstract description 33
- 229910044991 metal oxide Inorganic materials 0.000 claims abstract description 29
- 150000004706 metal oxides Chemical class 0.000 claims abstract description 29
- 229910052788 barium Inorganic materials 0.000 claims abstract description 21
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 claims abstract description 21
- 239000010936 titanium Substances 0.000 claims abstract description 18
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims abstract description 17
- 229910052719 titanium Inorganic materials 0.000 claims abstract description 16
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 107
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical group CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 53
- 239000002270 dispersing agent Substances 0.000 claims description 50
- 235000019441 ethanol Nutrition 0.000 claims description 44
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 42
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N Methyl ethyl ketone Natural products CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 claims description 40
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 33
- 239000002904 solvent Substances 0.000 claims description 22
- 239000000203 mixture Substances 0.000 claims description 18
- 238000004821 distillation Methods 0.000 claims description 17
- 238000009826 distribution Methods 0.000 claims description 17
- 239000011230 binding agent Substances 0.000 claims description 15
- 230000008569 process Effects 0.000 claims description 15
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 14
- 239000003960 organic solvent Substances 0.000 claims description 14
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 12
- 239000007822 coupling agent Substances 0.000 claims description 12
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 10
- 238000001914 filtration Methods 0.000 claims description 10
- 229920000642 polymer Polymers 0.000 claims description 10
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 9
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims description 8
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 8
- 229910000000 metal hydroxide Inorganic materials 0.000 claims description 8
- 150000004692 metal hydroxides Chemical class 0.000 claims description 8
- 229910052759 nickel Inorganic materials 0.000 claims description 7
- 229910052710 silicon Inorganic materials 0.000 claims description 7
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 6
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 claims description 6
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 6
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims description 6
- 238000001027 hydrothermal synthesis Methods 0.000 claims description 6
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims description 6
- 229910052718 tin Inorganic materials 0.000 claims description 6
- 229910052726 zirconium Inorganic materials 0.000 claims description 6
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 5
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims description 5
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 5
- 229910052791 calcium Inorganic materials 0.000 claims description 5
- 239000011575 calcium Substances 0.000 claims description 5
- 229910052735 hafnium Inorganic materials 0.000 claims description 5
- VBJZVLUMGGDVMO-UHFFFAOYSA-N hafnium atom Chemical compound [Hf] VBJZVLUMGGDVMO-UHFFFAOYSA-N 0.000 claims description 5
- 150000001282 organosilanes Chemical class 0.000 claims description 5
- 239000010703 silicon Substances 0.000 claims description 5
- 229910052712 strontium Inorganic materials 0.000 claims description 5
- CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 claims description 5
- 229910052725 zinc Inorganic materials 0.000 claims description 5
- 239000011701 zinc Substances 0.000 claims description 5
- KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 claims description 4
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 4
- JPOXNPPZZKNXOV-UHFFFAOYSA-N bromochloromethane Chemical compound ClCBr JPOXNPPZZKNXOV-UHFFFAOYSA-N 0.000 claims description 4
- XUPYJHCZDLZNFP-UHFFFAOYSA-N butyl butanoate Chemical compound CCCCOC(=O)CCC XUPYJHCZDLZNFP-UHFFFAOYSA-N 0.000 claims description 4
- 229910017052 cobalt Inorganic materials 0.000 claims description 4
- 239000010941 cobalt Substances 0.000 claims description 4
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 4
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 claims description 4
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 claims description 4
- 229910052749 magnesium Inorganic materials 0.000 claims description 4
- 239000011777 magnesium Substances 0.000 claims description 4
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims description 4
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 claims description 4
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims description 3
- 229910052796 boron Inorganic materials 0.000 claims description 3
- 235000011187 glycerol Nutrition 0.000 claims description 3
- 229910052758 niobium Inorganic materials 0.000 claims description 3
- 239000010955 niobium Substances 0.000 claims description 3
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 claims description 3
- UOCLXMDMGBRAIB-UHFFFAOYSA-N 1,1,1-trichloroethane Chemical compound CC(Cl)(Cl)Cl UOCLXMDMGBRAIB-UHFFFAOYSA-N 0.000 claims description 2
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims description 2
- NTIZESTWPVYFNL-UHFFFAOYSA-N Methyl isobutyl ketone Chemical compound CC(C)CC(C)=O NTIZESTWPVYFNL-UHFFFAOYSA-N 0.000 claims description 2
- UIHCLUNTQKBZGK-UHFFFAOYSA-N Methyl isobutyl ketone Natural products CCC(C)C(C)=O UIHCLUNTQKBZGK-UHFFFAOYSA-N 0.000 claims description 2
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims description 2
- CYTYCFOTNPOANT-UHFFFAOYSA-N Perchloroethylene Chemical group ClC(Cl)=C(Cl)Cl CYTYCFOTNPOANT-UHFFFAOYSA-N 0.000 claims description 2
- 241000779819 Syncarpia glomulifera Species 0.000 claims description 2
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical group ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 claims description 2
- 229940072049 amyl acetate Drugs 0.000 claims description 2
- PGMYKACGEOXYJE-UHFFFAOYSA-N anhydrous amyl acetate Natural products CCCCCOC(C)=O PGMYKACGEOXYJE-UHFFFAOYSA-N 0.000 claims description 2
- 229910052787 antimony Inorganic materials 0.000 claims description 2
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 claims description 2
- 229910052797 bismuth Inorganic materials 0.000 claims description 2
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 claims description 2
- SWXVUIWOUIDPGS-UHFFFAOYSA-N diacetone alcohol Chemical compound CC(=O)CC(C)(C)O SWXVUIWOUIDPGS-UHFFFAOYSA-N 0.000 claims description 2
- 229940093499 ethyl acetate Drugs 0.000 claims description 2
- 235000019439 ethyl acetate Nutrition 0.000 claims description 2
- MNWFXJYAOYHMED-UHFFFAOYSA-M heptanoate Chemical compound CCCCCCC([O-])=O MNWFXJYAOYHMED-UHFFFAOYSA-M 0.000 claims description 2
- 229910052747 lanthanoid Inorganic materials 0.000 claims description 2
- 150000002602 lanthanoids Chemical class 0.000 claims description 2
- 229910052746 lanthanum Inorganic materials 0.000 claims description 2
- FZLIPJUXYLNCLC-UHFFFAOYSA-N lanthanum atom Chemical compound [La] FZLIPJUXYLNCLC-UHFFFAOYSA-N 0.000 claims description 2
- 229910052744 lithium Inorganic materials 0.000 claims description 2
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 claims description 2
- WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 claims description 2
- 239000001739 pinus spp. Substances 0.000 claims description 2
- 235000019260 propionic acid Nutrition 0.000 claims description 2
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 claims description 2
- 229910052706 scandium Inorganic materials 0.000 claims description 2
- SIXSYDAISGFNSX-UHFFFAOYSA-N scandium atom Chemical compound [Sc] SIXSYDAISGFNSX-UHFFFAOYSA-N 0.000 claims description 2
- 229910052715 tantalum Inorganic materials 0.000 claims description 2
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 claims description 2
- 229950011008 tetrachloroethylene Drugs 0.000 claims description 2
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 claims description 2
- 229910052721 tungsten Inorganic materials 0.000 claims description 2
- 239000010937 tungsten Substances 0.000 claims description 2
- 229940036248 turpentine Drugs 0.000 claims description 2
- 229910052720 vanadium Inorganic materials 0.000 claims description 2
- 239000008096 xylene Substances 0.000 claims description 2
- 229910052727 yttrium Inorganic materials 0.000 claims description 2
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 claims description 2
- 238000001704 evaporation Methods 0.000 claims 1
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 abstract description 4
- 239000000843 powder Substances 0.000 description 37
- 239000010410 layer Substances 0.000 description 35
- 239000007787 solid Substances 0.000 description 31
- 239000000463 material Substances 0.000 description 23
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- 239000011164 primary particle Substances 0.000 description 20
- 239000000243 solution Substances 0.000 description 14
- 150000002739 metals Chemical class 0.000 description 13
- 239000003125 aqueous solvent Substances 0.000 description 12
- 239000012530 fluid Substances 0.000 description 12
- 239000007788 liquid Substances 0.000 description 12
- 239000003990 capacitor Substances 0.000 description 11
- 239000006087 Silane Coupling Agent Substances 0.000 description 10
- 238000000108 ultra-filtration Methods 0.000 description 10
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- 229910019142 PO4 Inorganic materials 0.000 description 7
- 239000004020 conductor Substances 0.000 description 7
- 230000000694 effects Effects 0.000 description 7
- 235000021317 phosphate Nutrition 0.000 description 7
- 239000000758 substrate Substances 0.000 description 7
- 229920002125 Sokalan® Polymers 0.000 description 6
- 239000008346 aqueous phase Substances 0.000 description 6
- 230000007062 hydrolysis Effects 0.000 description 6
- 238000006460 hydrolysis reaction Methods 0.000 description 6
- BFXIKLCIZHOAAZ-UHFFFAOYSA-N methyltrimethoxysilane Chemical compound CO[Si](C)(OC)OC BFXIKLCIZHOAAZ-UHFFFAOYSA-N 0.000 description 6
- 239000010452 phosphate Substances 0.000 description 6
- 238000012545 processing Methods 0.000 description 6
- 238000005245 sintering Methods 0.000 description 6
- 239000003981 vehicle Substances 0.000 description 6
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- 239000003985 ceramic capacitor Substances 0.000 description 5
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- 238000012360 testing method Methods 0.000 description 5
- 239000011135 tin Substances 0.000 description 5
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 4
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 4
- 230000015556 catabolic process Effects 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 4
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- 239000002019 doping agent Substances 0.000 description 4
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- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- 239000004698 Polyethylene Substances 0.000 description 3
- 239000002202 Polyethylene glycol Substances 0.000 description 3
- 229910008051 Si-OH Inorganic materials 0.000 description 3
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- 239000002253 acid Substances 0.000 description 3
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- RQPZNWPYLFFXCP-UHFFFAOYSA-L barium dihydroxide Chemical compound [OH-].[OH-].[Ba+2] RQPZNWPYLFFXCP-UHFFFAOYSA-L 0.000 description 3
- 229910001863 barium hydroxide Inorganic materials 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 150000001768 cations Chemical class 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical class OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
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- 125000000956 methoxy group Chemical group [H]C([H])([H])O* 0.000 description 3
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- 125000005372 silanol group Chemical group 0.000 description 3
- 239000004332 silver Substances 0.000 description 3
- 229910001316 Ag alloy Inorganic materials 0.000 description 2
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 2
- IRIAEXORFWYRCZ-UHFFFAOYSA-N Butylbenzyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCC1=CC=CC=C1 IRIAEXORFWYRCZ-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
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- 235000014113 dietary fatty acids Nutrition 0.000 description 2
- FLKPEMZONWLCSK-UHFFFAOYSA-N diethyl phthalate Chemical compound CCOC(=O)C1=CC=CC=C1C(=O)OCC FLKPEMZONWLCSK-UHFFFAOYSA-N 0.000 description 2
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- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical class CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 2
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- PLDDOISOJJCEMH-UHFFFAOYSA-N neodymium(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Nd+3].[Nd+3] PLDDOISOJJCEMH-UHFFFAOYSA-N 0.000 description 2
- 229910000480 nickel oxide Inorganic materials 0.000 description 2
- GNRSAWUEBMWBQH-UHFFFAOYSA-N oxonickel Chemical compound [Ni]=O GNRSAWUEBMWBQH-UHFFFAOYSA-N 0.000 description 2
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- 238000004626 scanning electron microscopy Methods 0.000 description 2
- 229910052709 silver Inorganic materials 0.000 description 2
- NTWXWSVUSTYPJH-UHFFFAOYSA-M sodium;1,4-bis(2-methylpropoxy)-1,4-dioxobutane-2-sulfonate Chemical compound [Na+].CC(C)COC(=O)CC(S([O-])(=O)=O)C(=O)OCC(C)C NTWXWSVUSTYPJH-UHFFFAOYSA-M 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
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- HNJBEVLQSNELDL-UHFFFAOYSA-N pyrrolidin-2-one Chemical compound O=C1CCCN1 HNJBEVLQSNELDL-UHFFFAOYSA-N 0.000 description 1
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- YWQIGRBJQMNGSN-UHFFFAOYSA-M sodium;1,4-dioxo-1,4-di(tridecoxy)butane-2-sulfonate Chemical compound [Na+].CCCCCCCCCCCCCOC(=O)CC(S([O-])(=O)=O)C(=O)OCCCCCCCCCCCCC YWQIGRBJQMNGSN-UHFFFAOYSA-M 0.000 description 1
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- 239000011975 tartaric acid Chemical class 0.000 description 1
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- 238000007669 thermal treatment Methods 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 238000004448 titration Methods 0.000 description 1
- 230000001131 transforming effect Effects 0.000 description 1
- RIUWBIIVUYSTCN-UHFFFAOYSA-N trilithium borate Chemical compound [Li+].[Li+].[Li+].[O-]B([O-])[O-] RIUWBIIVUYSTCN-UHFFFAOYSA-N 0.000 description 1
- PHYFQTYBJUILEZ-IUPFWZBJSA-N triolein Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CCCCCCCC)COC(=O)CCCCCCC\C=C/CCCCCCCC PHYFQTYBJUILEZ-IUPFWZBJSA-N 0.000 description 1
- BIKXLKXABVUSMH-UHFFFAOYSA-N trizinc;diborate Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]B([O-])[O-].[O-]B([O-])[O-] BIKXLKXABVUSMH-UHFFFAOYSA-N 0.000 description 1
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/62605—Treating the starting powders individually or as mixtures
- C04B35/62625—Wet mixtures
- C04B35/6264—Mixing media, e.g. organic solvents
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/46—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates
- C04B35/462—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates
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Abstract
L'invention concerne des suspensions, des dispersions ou des coulages de particules à base de titanate de baryum dans un milieu non aqueux et des procédés de fabrication correspondants. Lesdites particules ont un revêtement qui comprend un oxyde métallique, un oxyde métallique hydraté, un hydroxyde métallique ou un sel d'acide organique de métal autre que le baryum ou le titane. Au moins 90 % des particules ont une taille inférieure à 0,9 micromètre lorsque les particules revêtues sont dispersées par mélange à cisaillement élevé.
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US9040898P | 1998-06-23 | 1998-06-23 | |
US60/090,408 | 1998-06-23 | ||
US9666898P | 1998-08-14 | 1998-08-14 | |
US60/096,668 | 1998-08-14 | ||
PCT/US1999/013980 WO1999067189A1 (fr) | 1998-06-23 | 1999-06-21 | Dispersions a base de titanate de baryum |
Publications (1)
Publication Number | Publication Date |
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CA2335927A1 true CA2335927A1 (fr) | 1999-12-29 |
Family
ID=26782238
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA002335927A Abandoned CA2335927A1 (fr) | 1998-06-23 | 1999-06-21 | Dispersions a base de titanate de baryum |
Country Status (12)
Country | Link |
---|---|
EP (1) | EP1109758A1 (fr) |
JP (1) | JP2002518290A (fr) |
KR (1) | KR20010034928A (fr) |
CN (1) | CN1313842A (fr) |
AU (1) | AU4581299A (fr) |
BR (1) | BR9911406A (fr) |
CA (1) | CA2335927A1 (fr) |
IL (1) | IL140454A0 (fr) |
RU (1) | RU2001101934A (fr) |
SI (1) | SI20526A (fr) |
TW (1) | TW552250B (fr) |
WO (1) | WO1999067189A1 (fr) |
Families Citing this family (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE60012591T2 (de) * | 1999-01-28 | 2005-07-14 | Shin-Etsu Chemical Co., Ltd. | Mit seltener Erde oberflächenbeschichtete Bariumtitanatteilchen |
US6656590B2 (en) * | 2001-01-10 | 2003-12-02 | Cabot Corporation | Coated barium titanate-based particles and process |
KR100528950B1 (ko) * | 2001-01-29 | 2005-11-16 | 제이에스알 가부시끼가이샤 | 유전체용 복합 입자, 초미립자 복합 수지 입자, 유전체형성용 조성물 및 그의 용도 |
KR100439738B1 (ko) * | 2002-03-11 | 2004-07-12 | 한국과학기술연구원 | 액상 응결법에 의한 분말 과립 제조 및 그 성형 방법 |
US20040009350A1 (en) * | 2002-07-12 | 2004-01-15 | Krause Stephen J. | Methods of heat treating barium titanate-based particles and compositions formed from the same |
EP1513165A1 (fr) * | 2003-09-03 | 2005-03-09 | JSR Corporation | Composition pour former un diélectrique, comprenant des particules de structure crystalline de type perovskite, son procédé de préparation et son emploi et procédé de préparation des particules de structure crystalline de type perovskite |
CN1989072B (zh) * | 2005-03-30 | 2010-05-19 | 株式会社村田制作所 | 镁化合物溶胶其制造方法、及使用其的陶瓷原料的制造方法 |
JP2010195694A (ja) * | 2009-02-24 | 2010-09-09 | Miyoshi Kasei Inc | 粉体分散物とこの粉体分散物を含有する化粧料 |
USRE48877E1 (en) * | 2012-03-30 | 2022-01-04 | Taiyo Yuden Co., Ltd. | Multi-layer ceramic capacitor and method of manufacturing the same |
CN103943358B (zh) * | 2014-03-28 | 2017-01-18 | 张海鹏 | 一种用于稀释贴片电容浆料的稀释剂 |
CN105132935A (zh) * | 2015-09-28 | 2015-12-09 | 苏州龙腾万里化工科技有限公司 | 一种溶剂型金属清洗剂 |
JP6781540B2 (ja) * | 2015-10-30 | 2020-11-04 | 太陽誘電株式会社 | チタン酸バリウム系粉末、積層セラミックコンデンサ及びその製造方法 |
JP6839585B2 (ja) * | 2017-03-30 | 2021-03-10 | 花王株式会社 | 印刷インキ用分散剤組成物 |
JP6564551B1 (ja) * | 2018-11-27 | 2019-08-21 | 株式会社アドマテックス | 表面改質チタン酸バリウム粒子材料、チタン酸バリウム含有樹脂組成物、及びチタン酸バリウム分散液 |
CN111825447B (zh) * | 2020-07-06 | 2022-08-26 | 武汉理工大学 | 一种高储能密度的钛酸钡基介质薄膜及其制备方法 |
CN112390644B (zh) * | 2020-11-23 | 2022-11-22 | 中国振华集团云科电子有限公司 | 一种改善mct陶瓷一次球磨混料质量的方法 |
CN113264764A (zh) * | 2021-07-05 | 2021-08-17 | 山东国瓷功能材料股份有限公司 | 溶剂体系、钛酸钡流延浆料和陶瓷膜片 |
CN113754428B (zh) * | 2021-09-16 | 2022-08-26 | 山东国瓷功能材料股份有限公司 | 超细水热钛酸钡有机浆料及其制备方法、陶瓷膜片 |
CN114315349B (zh) * | 2021-12-17 | 2023-01-24 | 西安理工大学 | 一种制备介孔锆钛酸钡陶瓷纳米颗粒的方法 |
CN115286379B (zh) * | 2022-08-03 | 2023-02-10 | 景德镇陶瓷大学 | 一种外场促进缩聚非水沉淀工艺制备钛酸钡基陶瓷粉的方法 |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3490927A (en) * | 1966-08-01 | 1970-01-20 | Sprague Electric Co | Nb2o5 and ta2o5 doped bat1o3 ceramic body and process therefor |
GB2193713B (en) * | 1986-07-14 | 1990-12-05 | Cabot Corp | Method of producing perovskite-type compounds. |
US5296426A (en) * | 1990-06-15 | 1994-03-22 | E. I. Du Pont De Nemours And Company | Low-fire X7R compositions |
US6268054B1 (en) * | 1997-02-18 | 2001-07-31 | Cabot Corporation | Dispersible, metal oxide-coated, barium titanate materials |
-
1999
- 1999-06-21 JP JP2000555845A patent/JP2002518290A/ja active Pending
- 1999-06-21 CN CN99809978A patent/CN1313842A/zh active Pending
- 1999-06-21 AU AU45812/99A patent/AU4581299A/en not_active Abandoned
- 1999-06-21 KR KR1020007014726A patent/KR20010034928A/ko not_active Application Discontinuation
- 1999-06-21 IL IL14045499A patent/IL140454A0/xx unknown
- 1999-06-21 RU RU2001101934/03A patent/RU2001101934A/ru not_active Application Discontinuation
- 1999-06-21 CA CA002335927A patent/CA2335927A1/fr not_active Abandoned
- 1999-06-21 EP EP99928831A patent/EP1109758A1/fr not_active Withdrawn
- 1999-06-21 BR BR9911406-2A patent/BR9911406A/pt not_active IP Right Cessation
- 1999-06-21 WO PCT/US1999/013980 patent/WO1999067189A1/fr not_active Application Discontinuation
- 1999-06-21 SI SI9920059A patent/SI20526A/sl not_active IP Right Cessation
- 1999-06-23 TW TW088110565A patent/TW552250B/zh not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
WO1999067189A1 (fr) | 1999-12-29 |
CN1313842A (zh) | 2001-09-19 |
EP1109758A1 (fr) | 2001-06-27 |
AU4581299A (en) | 2000-01-10 |
SI20526A (sl) | 2001-10-31 |
BR9911406A (pt) | 2002-09-24 |
RU2001101934A (ru) | 2003-01-10 |
IL140454A0 (en) | 2002-02-10 |
TW552250B (en) | 2003-09-11 |
KR20010034928A (ko) | 2001-04-25 |
JP2002518290A (ja) | 2002-06-25 |
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FZDE | Discontinued |