CA2079720A1 - Procede pour la surveillance et la regulation d'un procede de reaction d'alkanolamine - Google Patents

Procede pour la surveillance et la regulation d'un procede de reaction d'alkanolamine

Info

Publication number
CA2079720A1
CA2079720A1 CA2079720A CA2079720A CA2079720A1 CA 2079720 A1 CA2079720 A1 CA 2079720A1 CA 2079720 A CA2079720 A CA 2079720A CA 2079720 A CA2079720 A CA 2079720A CA 2079720 A1 CA2079720 A1 CA 2079720A1
Authority
CA
Canada
Prior art keywords
anion exchange
exchange resin
effluent
acid anions
alkanolamine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CA2079720A
Other languages
English (en)
Other versions
CA2079720C (fr
Inventor
Arthur L. Cummings
Fred C. Veatch
Alfred E. Keller
James C. Thomsen
Regina A. Severson
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ConocoPhillips Co
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of CA2079720A1 publication Critical patent/CA2079720A1/fr
Application granted granted Critical
Publication of CA2079720C publication Critical patent/CA2079720C/fr
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/1425—Regeneration of liquid absorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/1412—Controlling the absorption process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J41/00—Anion exchange; Use of material as anion exchangers; Treatment of material for improving the anion exchange properties
    • B01J41/04—Processes using organic exchangers
    • B01J41/05—Processes using organic exchangers in the strongly basic form
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/80—Automatic regeneration
    • B01J49/85—Controlling or regulating devices therefor
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S423/00—Chemistry of inorganic compounds
    • Y10S423/09—Reaction techniques
    • Y10S423/14—Ion exchange; chelation or liquid/liquid ion extraction

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Treatment Of Water By Ion Exchange (AREA)
CA002079720A 1991-10-08 1992-10-02 Procede pour la surveillance et la regulation d'un procede de reaction d'alkanolamine Expired - Lifetime CA2079720C (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US07/773,387 1991-10-08
US07/773,387 US5162084A (en) 1991-10-08 1991-10-08 Process for monitoring and controlling an alkanolamine reaction process

Publications (2)

Publication Number Publication Date
CA2079720A1 true CA2079720A1 (fr) 1993-04-09
CA2079720C CA2079720C (fr) 1999-12-21

Family

ID=25098100

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002079720A Expired - Lifetime CA2079720C (fr) 1991-10-08 1992-10-02 Procede pour la surveillance et la regulation d'un procede de reaction d'alkanolamine

Country Status (6)

Country Link
US (1) US5162084A (fr)
EP (1) EP0537938B1 (fr)
JP (1) JP2891827B2 (fr)
CA (1) CA2079720C (fr)
DE (1) DE69229532T2 (fr)
ES (1) ES2133306T3 (fr)

Families Citing this family (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3348109B2 (ja) * 1992-01-02 2002-11-20 コノコ・インコーポレーテッド 水酸化ナトリウムで陽イオン交換樹脂からアルカノールアミンを選択的に再生するためのモニターおよび制御システム
EP0810904B1 (fr) * 1995-02-24 1998-09-02 MPR Services, Inc. Extraction de sel d'amine stable a la chaleur d'une resine echangeuse d'anions de type ii
US5877386A (en) * 1995-10-05 1999-03-02 Union Carbide Chemicals & Plastics Technology Corporation Method for sweetening of liquid petroleum gas by contacting with tea and another amine
US6071484A (en) * 1997-01-24 2000-06-06 Mpr Services, Inc. Process for treating gas with ultra-lean amine
FR2763330B1 (fr) * 1997-05-15 1999-07-30 Atochem Elf Sa Procede de purification de liquides organiques quasi anhydres
US5994147A (en) * 1997-05-23 1999-11-30 Union Pacific Resources Co. System and method for determining acid-gas (CO2, H2 S) loadings in an alkanolamine system
US6660875B1 (en) 1998-06-09 2003-12-09 Ppt Technologies, Llc Ion exchange purification of dielectric condensate precursor fluids and silicate esters such as tetraethylorthosilicate (TEOS)
US7329354B2 (en) * 1998-06-09 2008-02-12 Ppt Technologies, Llc Purification of organic solvent fluids
US6416670B1 (en) 1999-03-12 2002-07-09 Mpr Services, Inc. Regenerable hydrocarbon filter
US6245128B1 (en) 1999-06-15 2001-06-12 Mobil Oil Corporation Process for the reclamation of spent alkanolamine solution
US6334886B1 (en) 2000-05-12 2002-01-01 Air Products And Chemicals, Inc. Removal of corrosive contaminants from alkanolamine absorbent process
US6767746B2 (en) * 2001-07-30 2004-07-27 Spartan Controls Ltd. Method and apparatus for analyzing acid gas loading within an amine solution
CN100333823C (zh) * 2004-08-03 2007-08-29 中国石化镇海炼油化工股份有限公司 一种用强碱性阴离子交换树脂净化劣化胺液的方法
JP2009502483A (ja) * 2005-07-28 2009-01-29 グローバル リサーチ テクノロジーズ，エルエルシー 空気からの二酸化炭素除去
JP5320778B2 (ja) * 2008-03-07 2013-10-23 栗田エンジニアリング株式会社 アミン液の再生方法
KR101007418B1 (ko) 2008-05-28 2011-01-12 순천향대학교 산학협력단 아민 포함 폐수로부터의 아민 회수 방법
US8097068B2 (en) * 2008-11-06 2012-01-17 Cansolv Technologies Inc. Method for treating a diamine absorbent stream
JP5584984B2 (ja) * 2009-03-18 2014-09-10 栗田エンジニアリング株式会社 アミン液の再生方法
JP5585025B2 (ja) * 2009-08-18 2014-09-10 栗田エンジニアリング株式会社 アミン液の再生方法
JP5589327B2 (ja) * 2009-09-16 2014-09-17 栗田エンジニアリング株式会社 アミン液の再生方法
JP5564967B2 (ja) * 2010-02-04 2014-08-06 栗田エンジニアリング株式会社 アミン液の再生に用いたイオン交換樹脂の再生方法
JP5660303B2 (ja) * 2010-11-18 2015-01-28 栗田エンジニアリング株式会社 アミン液の再生方法
JP6088266B2 (ja) * 2013-01-30 2017-03-01 オルガノ株式会社 Ｎｍｐ精製システム
JP6088267B2 (ja) * 2013-01-30 2017-03-01 オルガノ株式会社 Ｎｍｐ精製システム
KR101549089B1 (ko) 2014-11-11 2015-09-02 부산대학교 산학협력단 음이온성 금속수산화물 재생용액을 이용한 이온교환수지의 재생공정을 포함하는 산성가스의 흡수방법
CN106267888A (zh) * 2015-08-10 2017-01-04 中国石油化工股份有限公司 一种脱除脱硫醇胺溶液中热稳盐的方法
CN109253558B (zh) * 2018-03-19 2021-02-26 华洋通信科技股份有限公司 一种循环氨水余热利用制冷机组自动反冲洗装置及方法
CN110862326A (zh) * 2018-08-28 2020-03-06 浙江工业大学 一种由氯化胆碱制备高纯胆碱的方法
JP7146568B2 (ja) * 2018-10-24 2022-10-04 オルガノ株式会社 有機溶媒の精製方法及び精製装置
US20220371887A1 (en) * 2019-11-08 2022-11-24 Minoru Terada Method for preparing hypochlorous acid aqueous solution and method for regenerating weakly acidic cation exchanger

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2628191A (en) * 1946-10-29 1953-02-10 Permutit Co Regeneration of ion exchangers
GB672754A (en) * 1949-12-14 1952-05-28 John Thompson Kennicott Ltd Improvements in ion-exchange processes for the treatment of water
US2797188A (en) * 1953-12-04 1957-06-25 Dow Chemical Co Refining petroleum with an alkanolamine absorbent and reactivation of the spent alkanol amine
US2938868A (en) * 1955-03-11 1960-05-31 Infilco Inc Method of controlling regeneration of ion exchangers and apparatus
US3246759A (en) * 1963-04-05 1966-04-19 Culligan Inc Regeneration control for ion exchange beds
US3531252A (en) * 1966-10-17 1970-09-29 Calgon C0Rp Methods of analyzing conductive solutions
SU446289A1 (ru) * 1973-02-02 1974-10-15 Наладочно-монтажное управление Треста "Электроюжмонтаж" Способ контрол степени истощени ионитовыхфильтров
US4170628A (en) * 1977-03-25 1979-10-09 Union Carbide Corporation Process for removing SO2 from effluent gases and for removing heat stable salts from systems in which they accumulate using an anion exchange resin
US4199323A (en) * 1978-06-08 1980-04-22 The Dow Chemical Company Analytical technique for quantitating acid/salt and base/salt samples for species concentration
US4242097A (en) * 1979-03-05 1980-12-30 Dionex Corporation Method and apparatus for quantitative analysis of weakly ionized anions or cations
US4320206A (en) * 1980-10-14 1982-03-16 Rohm And Haas Company Emulsion regenerant for ion exchange resins
AU548884B2 (en) * 1981-03-05 1986-01-09 Northern Engineering Industries Plc Regenerating ion-exchange materials
US4477419A (en) * 1983-03-03 1984-10-16 The Dow Chemical Company Process for the recovery of CO2 from flue gases
US4814281A (en) * 1986-01-07 1989-03-21 Westinghouse Electric Corp. Differential conductivity sulfate monitor
US4880513A (en) * 1986-06-20 1989-11-14 The Graver Company Method and apparatus for generating acid and base regenerants and the use thereof to regenerate ion-exchange resins
US4970344A (en) * 1987-07-02 1990-11-13 Conoco Inc. Reactivation of spent alkanolamine
US4795565A (en) * 1987-10-28 1989-01-03 Mobil Oil Corporation Clean up of ethanolamine to improve performance and control corrosion of ethanolamine units
US4952386A (en) * 1988-05-20 1990-08-28 Athens Corporation Method and apparatus for purifying hydrogen fluoride
JPH02167816A (ja) * 1988-12-21 1990-06-28 Nkk Corp 脱硫廃液からのチオシアン酸塩の回収方法
US5006258A (en) * 1989-10-26 1991-04-09 Conoco Inc. Regeneration of acidic cationic exchange resin used in the reactivation of spent alkanolamine
CA2027435A1 (fr) * 1989-10-26 1991-04-27 Fred C. Veatch Elimination des anions thermostables des sels d'alcanolamines

Also Published As

Publication number Publication date
ES2133306T3 (es) 1999-09-16
EP0537938B1 (fr) 1999-07-07
EP0537938A1 (fr) 1993-04-21
JPH05294902A (ja) 1993-11-09
DE69229532T2 (de) 1999-10-28
US5162084A (en) 1992-11-10
DE69229532D1 (de) 1999-08-12
JP2891827B2 (ja) 1999-05-17
CA2079720C (fr) 1999-12-21

Similar Documents

Publication Publication Date Title
CA2079720A1 (fr) Procede pour la surveillance et la regulation d'un procede de reaction d'alkanolamine
CA2199497A1 (fr) Procede de traitement des eaux
CA2120177A1 (fr) Procede pour la recuperation et la regeneration de liquide d'etamage
CA2018667A1 (fr) Preparation de resines desinfectantes a base de i5-polyiodide
IE43536L (en) Ion-exchange separation of proteins
EP0538040A3 (fr) Procédé pour l'élimination des composés iodures des acides carboxyliques et des anhydrides d'acides carboxyliques
CA2081226A1 (fr) Systeme de surveillance et de controle pour la regeneration selective d'aminoalcanol a partir d'une resine echangeuse de cation, a l'aide d'hydroxyde de sodium
AU7016600A (en) Method and installation for eliminating metal cations from liquid with polyazacycloalkane resins grafted on a support
EP0111999A3 (en) Spherical ion exchange resin, method for producing the same and method for adsorption treatment using the same
EP1167288A3 (fr) Procédé de production d'une solution purifiée aqueuse de peroxyde d'hydrogène
FI921437A7 (fi) Menetelmä tasakokoisten ioninvaihtohartsihiukkasten valmistamiseksi
AU3663989A (en) Process and apparatus for ion exchangers, particularly for regeneration after softening and demineralization of aqueous solutions
TW272968B (fr)
AU4177793A (en) Separation of metal ions on an anion exchange resin by chromatographic elution
DE3280059D1 (de) Verfahren zum entfernen von uebergangsmetallionen aus waessriger loesung mit hilfe eines, kristallines uebergangsmetallaluminat enthaltenden, ionen austauscherharzes.
ES456179A1 (es) Procedimiento para la depuracion de resinas intercambiadorasde iones usadas en reactores nucleares.
CA2212578A1 (fr) Extraction de sel d'amine stable a la chaleur d'une resine echangeuse d'anions de type ii
EP0815939A3 (fr) Echangeur d'ions, procédé pour sa production et procédé pour enlever des anions multivalents utilisant cet échangeur d'ions
MY128388A (en) Method of regenerating ion exchange resin
HK1007289A1 (en) Apparatus for providing a regenerant solution to a regenerable liquid treatment medium bed
WO2000001487A3 (fr) Reduction de traces d'ions metalliques par une unite echangeuse d'ions
CA2266453A1 (fr) Procede de fabrication d'hydroxylamine
JP2003230840A5 (fr)
AU8888382A (en) Regenerating mixed-bed exchange resins
DE3479892D1 (en) Process for fluorinated ion exchange polymer precursor

Legal Events

Date Code Title Description
EEER Examination request
MKEX Expiry