CA2036731C - Process for the production of granulated dicalcium phosphate dihydrate - Google Patents
Process for the production of granulated dicalcium phosphate dihydrateInfo
- Publication number
- CA2036731C CA2036731C CA002036731A CA2036731A CA2036731C CA 2036731 C CA2036731 C CA 2036731C CA 002036731 A CA002036731 A CA 002036731A CA 2036731 A CA2036731 A CA 2036731A CA 2036731 C CA2036731 C CA 2036731C
- Authority
- CA
- Canada
- Prior art keywords
- dicalcium phosphate
- grain size
- calcium hydroxide
- granulated
- fine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000000034 method Methods 0.000 title claims abstract description 17
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 11
- RBLGLDWTCZMLRW-UHFFFAOYSA-K dicalcium;phosphate;dihydrate Chemical compound O.O.[Ca+2].[Ca+2].[O-]P([O-])([O-])=O RBLGLDWTCZMLRW-UHFFFAOYSA-K 0.000 title abstract description 24
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims abstract description 36
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims abstract description 22
- 239000000920 calcium hydroxide Substances 0.000 claims abstract description 22
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims abstract description 22
- 239000008187 granular material Substances 0.000 claims abstract description 20
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims abstract description 17
- 239000000463 material Substances 0.000 claims abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000007787 solid Substances 0.000 claims abstract description 7
- 238000006386 neutralization reaction Methods 0.000 claims abstract description 4
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 20
- 239000001506 calcium phosphate Substances 0.000 claims description 17
- 235000019739 Dicalciumphosphate Nutrition 0.000 claims description 13
- NEFBYIFKOOEVPA-UHFFFAOYSA-K dicalcium phosphate Chemical compound [Ca+2].[Ca+2].[O-]P([O-])([O-])=O NEFBYIFKOOEVPA-UHFFFAOYSA-K 0.000 claims description 13
- 229910000390 dicalcium phosphate Inorganic materials 0.000 claims description 12
- 229940038472 dicalcium phosphate Drugs 0.000 claims description 12
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 10
- 238000005469 granulation Methods 0.000 claims description 4
- 230000003179 granulation Effects 0.000 claims description 4
- 239000007858 starting material Substances 0.000 claims description 4
- 235000011116 calcium hydroxide Nutrition 0.000 description 17
- 235000011007 phosphoric acid Nutrition 0.000 description 17
- 229940095643 calcium hydroxide Drugs 0.000 description 14
- 239000007788 liquid Substances 0.000 description 11
- 238000006243 chemical reaction Methods 0.000 description 9
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 6
- 239000000843 powder Substances 0.000 description 6
- 235000011010 calcium phosphates Nutrition 0.000 description 5
- 238000009826 distribution Methods 0.000 description 5
- 238000002156 mixing Methods 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 5
- 239000000428 dust Substances 0.000 description 4
- 239000002002 slurry Substances 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 229910000389 calcium phosphate Inorganic materials 0.000 description 3
- 239000001569 carbon dioxide Substances 0.000 description 3
- 229910002092 carbon dioxide Inorganic materials 0.000 description 3
- 239000011230 binding agent Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000009969 flowable effect Effects 0.000 description 2
- 239000001488 sodium phosphate Substances 0.000 description 2
- 229910000162 sodium phosphate Inorganic materials 0.000 description 2
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 2
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000002671 adjuvant Substances 0.000 description 1
- 239000007900 aqueous suspension Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- YYRMJZQKEFZXMX-UHFFFAOYSA-L calcium bis(dihydrogenphosphate) Chemical class [Ca+2].OP(O)([O-])=O.OP(O)([O-])=O YYRMJZQKEFZXMX-UHFFFAOYSA-L 0.000 description 1
- 229940043430 calcium compound Drugs 0.000 description 1
- 150000001674 calcium compounds Chemical class 0.000 description 1
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
- 239000000292 calcium oxide Substances 0.000 description 1
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 1
- 239000012876 carrier material Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000019691 monocalcium phosphate Nutrition 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 235000021317 phosphate Nutrition 0.000 description 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 239000000606 toothpaste Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 230000003245 working effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/32—Phosphates of magnesium, calcium, strontium, or barium
- C01B25/327—After-treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Geology (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Inorganic Chemistry (AREA)
- Environmental & Geological Engineering (AREA)
- Glanulating (AREA)
- Fodder In General (AREA)
- Cosmetics (AREA)
- Materials For Medical Uses (AREA)
- Medicinal Preparation (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Fertilizers (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE4006734A DE4006734C1 (OSRAM) | 1990-03-03 | 1990-03-03 | |
| DEP4006734.3 | 1990-03-03 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2036731A1 CA2036731A1 (en) | 1991-09-04 |
| CA2036731C true CA2036731C (en) | 1997-05-06 |
Family
ID=6401369
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA002036731A Expired - Fee Related CA2036731C (en) | 1990-03-03 | 1991-02-20 | Process for the production of granulated dicalcium phosphate dihydrate |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US5108728A (OSRAM) |
| EP (1) | EP0445593B1 (OSRAM) |
| JP (1) | JPH0748108A (OSRAM) |
| AT (1) | ATE104926T1 (OSRAM) |
| CA (1) | CA2036731C (OSRAM) |
| DE (2) | DE4006734C1 (OSRAM) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5785956A (en) * | 1996-06-07 | 1998-07-28 | Colgate Palmolive Company | Dual component dentifrice composition for dental fluoridation |
| GB9825033D0 (en) * | 1998-11-13 | 1999-01-13 | Nycomed Pharma As | Process |
| JP5112860B2 (ja) * | 2004-05-24 | 2013-01-09 | ニコメド ファーマ エイエス | カルシム含有化合物および糖アルコールを含む微粒状物 |
| CN103479582A (zh) * | 2005-02-03 | 2014-01-01 | 武田奈科明有限公司 | 制备含钙组合物的快速湿聚结方法 |
| EP1845949B1 (en) | 2005-02-03 | 2008-05-21 | Nycomed Pharma AS | Melt granulation of a composition containing a calcium-containing compound |
| MX2007010519A (es) † | 2005-03-04 | 2008-01-18 | Nycomed Pharma As | Proceso para la produccion de composiciones de calcio en un lecho fluido continuo. |
| US20070003611A1 (en) * | 2005-06-29 | 2007-01-04 | Sung-Tsuen Liu | Novel method of granulating calcium carbonate and products provided therefrom |
| US7273596B2 (en) * | 2005-08-10 | 2007-09-25 | J.M. Huber Corporation | Method of producing granulated anhydrous dicalcium phosphate |
| CN102872157A (zh) * | 2005-12-07 | 2013-01-16 | 奈科明制药有限公司 | 预先压实的含钙组合物 |
| WO2007065840A1 (de) * | 2005-12-07 | 2007-06-14 | Basf Se | Verfahren zum kontinuierlichen mischen von polymerpartikeln |
| UA95093C2 (uk) * | 2005-12-07 | 2011-07-11 | Нікомед Фарма Ас | Спосіб одержання кальцієвмісної сполуки |
| US7273521B1 (en) | 2006-04-28 | 2007-09-25 | J.M. Huber Corporation | Method of producing granulated calcium carbonate/calcium phosphate composite materials with very high calcium to phosphate mole ratios |
| KR20100108523A (ko) | 2007-11-19 | 2010-10-07 | 그라세 게엠베하 운트 캄파니 카게 | 내식성 입자 |
| AR074508A1 (es) * | 2008-12-08 | 2011-01-19 | Grace Gmbh & Co Kg | Particulas anticorrosivas |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1216264B (de) * | 1963-09-16 | 1966-05-12 | Knapsack Ag | Verfahren zur Herstellung von Dicalciumphosphatdihydrat |
| US3304249A (en) * | 1964-02-28 | 1967-02-14 | Katz Herbert | Method of stabilizing a fluidized bed using a glow discharge |
| GB1084062A (OSRAM) * | 1965-01-21 | |||
| US3467495A (en) * | 1965-12-23 | 1969-09-16 | Int Minerals & Chem Corp | Preparation of calcium phosphates |
| ES374610A1 (es) * | 1968-12-27 | 1972-01-01 | Knapsack Ag | Procedimiento para la preparacion de un pienso para anima- les. |
| US4166839A (en) * | 1974-03-19 | 1979-09-04 | Norsk Hydro A.S | Method for producing calcium phosphates |
| NO132685C (OSRAM) * | 1974-03-19 | 1977-05-24 | Norsk Hydro As | |
| IE52274B1 (en) * | 1980-12-12 | 1987-09-02 | Stauffer Chemical Co | A process of compacting fine particles of calcium phosphate and the compacts obtained thereby |
| US4675188A (en) * | 1985-08-02 | 1987-06-23 | Stauffer Chemical Company | Granular anhydrous dicalcium phosphate compositions suitable for direct compression tableting |
-
1990
- 1990-03-03 DE DE4006734A patent/DE4006734C1/de not_active Expired - Lifetime
-
1991
- 1991-02-20 CA CA002036731A patent/CA2036731C/en not_active Expired - Fee Related
- 1991-02-21 AT AT9191102530T patent/ATE104926T1/de not_active IP Right Cessation
- 1991-02-21 DE DE59101469T patent/DE59101469D1/de not_active Expired - Fee Related
- 1991-02-21 EP EP91102530A patent/EP0445593B1/de not_active Expired - Lifetime
- 1991-02-27 JP JP3031184A patent/JPH0748108A/ja active Pending
- 1991-03-01 US US07/662,967 patent/US5108728A/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| DE4006734C1 (OSRAM) | 1991-07-25 |
| CA2036731A1 (en) | 1991-09-04 |
| DE59101469D1 (de) | 1994-06-01 |
| EP0445593A1 (de) | 1991-09-11 |
| US5108728A (en) | 1992-04-28 |
| EP0445593B1 (de) | 1994-04-27 |
| ATE104926T1 (de) | 1994-05-15 |
| JPH0748108A (ja) | 1995-02-21 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request | ||
| MKLA | Lapsed |