CA1340947C - Method and device for producing pure elemental iodine - Google Patents
Method and device for producing pure elemental iodineInfo
- Publication number
- CA1340947C CA1340947C CA000613953A CA613953A CA1340947C CA 1340947 C CA1340947 C CA 1340947C CA 000613953 A CA000613953 A CA 000613953A CA 613953 A CA613953 A CA 613953A CA 1340947 C CA1340947 C CA 1340947C
- Authority
- CA
- Canada
- Prior art keywords
- iodine
- tfi2
- barrier
- solid
- source
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 title claims abstract description 168
- 239000011630 iodine Substances 0.000 title claims abstract description 167
- 229910052740 iodine Inorganic materials 0.000 title claims abstract description 167
- 238000000034 method Methods 0.000 title claims abstract description 23
- 230000004888 barrier function Effects 0.000 claims abstract description 64
- 239000007787 solid Substances 0.000 claims abstract description 60
- 239000000463 material Substances 0.000 claims abstract description 16
- 239000000203 mixture Substances 0.000 claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 25
- -1 polyethylene Polymers 0.000 claims description 16
- 230000000536 complexating effect Effects 0.000 claims description 14
- 150000001875 compounds Chemical class 0.000 claims description 12
- 239000002904 solvent Substances 0.000 claims description 10
- 239000004698 Polyethylene Substances 0.000 claims description 9
- 239000007788 liquid Substances 0.000 claims description 9
- 229920000573 polyethylene Polymers 0.000 claims description 9
- 239000000356 contaminant Substances 0.000 claims description 7
- 229930040373 Paraformaldehyde Natural products 0.000 claims description 4
- 229920006324 polyoxymethylene Polymers 0.000 claims description 4
- 230000004044 response Effects 0.000 claims description 4
- 229920003023 plastic Polymers 0.000 claims 4
- 239000004033 plastic Substances 0.000 claims 4
- 239000011343 solid material Substances 0.000 claims 4
- 229920001707 polybutylene terephthalate Polymers 0.000 claims 3
- 230000008569 process Effects 0.000 abstract description 3
- 235000013675 iodine Nutrition 0.000 description 119
- 239000000243 solution Substances 0.000 description 17
- PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 description 12
- 239000000047 product Substances 0.000 description 12
- 239000002671 adjuvant Substances 0.000 description 11
- NLKNQRATVPKPDG-UHFFFAOYSA-M potassium iodide Chemical compound [K+].[I-] NLKNQRATVPKPDG-UHFFFAOYSA-M 0.000 description 11
- 239000000126 substance Substances 0.000 description 10
- 239000002775 capsule Substances 0.000 description 5
- 239000012530 fluid Substances 0.000 description 5
- 230000003115 biocidal effect Effects 0.000 description 4
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 3
- 238000011109 contamination Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- QDHHCQZDFGDHMP-UHFFFAOYSA-N Chloramine Chemical compound ClN QDHHCQZDFGDHMP-UHFFFAOYSA-N 0.000 description 2
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 2
- 239000003086 colorant Substances 0.000 description 2
- 239000008139 complexing agent Substances 0.000 description 2
- 238000010276 construction Methods 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 239000012895 dilution Substances 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 210000004907 gland Anatomy 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 229940098465 tincture Drugs 0.000 description 2
- CPKVUHPKYQGHMW-UHFFFAOYSA-N 1-ethenylpyrrolidin-2-one;molecular iodine Chemical compound II.C=CN1CCCC1=O CPKVUHPKYQGHMW-UHFFFAOYSA-N 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- WHNWPMSKXPGLAX-UHFFFAOYSA-N N-Vinyl-2-pyrrolidone Chemical compound C=CN1CCCC1=O WHNWPMSKXPGLAX-UHFFFAOYSA-N 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 229920000153 Povidone-iodine Polymers 0.000 description 1
- 101100214488 Solanum lycopersicum TFT2 gene Proteins 0.000 description 1
- 206010052428 Wound Diseases 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000003139 biocide Substances 0.000 description 1
- 230000031018 biological processes and functions Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005538 encapsulation Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 230000002070 germicidal effect Effects 0.000 description 1
- 230000012010 growth Effects 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 150000004694 iodide salts Chemical class 0.000 description 1
- 150000002496 iodine Chemical class 0.000 description 1
- 150000002497 iodine compounds Chemical class 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 230000002262 irrigation Effects 0.000 description 1
- 238000003973 irrigation Methods 0.000 description 1
- 229920001684 low density polyethylene Polymers 0.000 description 1
- 239000004702 low-density polyethylene Substances 0.000 description 1
- 210000002751 lymph Anatomy 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 210000004877 mucosa Anatomy 0.000 description 1
- 231100000344 non-irritating Toxicity 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 1
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 description 1
- 239000001103 potassium chloride Substances 0.000 description 1
- 235000011164 potassium chloride Nutrition 0.000 description 1
- 229940069328 povidone Drugs 0.000 description 1
- 229960001621 povidone-iodine Drugs 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 230000001850 reproductive effect Effects 0.000 description 1
- 230000000452 restraining effect Effects 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- KKEYFWRCBNTPAC-UHFFFAOYSA-L terephthalate(2-) Chemical compound [O-]C(=O)C1=CC=C(C([O-])=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-L 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 231100000167 toxic agent Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 239000003440 toxic substance Substances 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/12—Iodine, e.g. iodophors; Compounds thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/36—Pervaporation; Membrane distillation; Liquid permeation
- B01D61/363—Vapour permeation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/13—Iodine; Hydrogen iodide
- C01B7/14—Iodine
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Water Supply & Treatment (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Organic Chemistry (AREA)
- Dentistry (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Plant Pathology (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Priority Applications (11)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CA000613953A CA1340947C (en) | 1989-09-28 | 1989-09-28 | Method and device for producing pure elemental iodine |
| US07/842,153 US5275736A (en) | 1989-09-28 | 1990-08-20 | Method and device for producing pure elemental iodine |
| BR909007705A BR9007705A (pt) | 1989-09-28 | 1990-08-20 | Metodo e dispositivo para producao de iodo elementar puro |
| PCT/CA1990/000265 WO1991004940A1 (en) | 1989-09-28 | 1990-08-20 | Method and device for producing pure elemental iodine |
| JP2511166A JPH05500354A (ja) | 1989-09-28 | 1990-08-20 | 純粋な元素ヨウ素の製造方法および装置 |
| AU61536/90A AU633616C (en) | 1989-09-28 | 1990-08-20 | Method and device for producing pure elemental iodine |
| CA002066673A CA2066673C (en) | 1989-09-28 | 1990-08-20 | Method and device for producing pure elemental iodine |
| HU9201028A HUT60696A (en) | 1989-09-28 | 1990-08-20 | Process and equipment for obtaining pure elementary iodine |
| EP90911944A EP0494150A1 (en) | 1989-09-28 | 1990-08-20 | Method and device for producing pure elemental iodine |
| NO921168A NO308697B1 (no) | 1989-09-28 | 1992-03-25 | FremgangsmÕte og anordning for fremstilling av rent elementært jod |
| FI921354A FI921354A0 (fi) | 1989-09-28 | 1992-03-27 | Foerfarande och anordning foer produktion av ren elementjod. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CA000613953A CA1340947C (en) | 1989-09-28 | 1989-09-28 | Method and device for producing pure elemental iodine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1340947C true CA1340947C (en) | 2000-04-04 |
Family
ID=4140750
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA000613953A Expired - Fee Related CA1340947C (en) | 1989-09-28 | 1989-09-28 | Method and device for producing pure elemental iodine |
Country Status (8)
| Country | Link |
|---|---|
| EP (1) | EP0494150A1 (fi) |
| JP (1) | JPH05500354A (fi) |
| BR (1) | BR9007705A (fi) |
| CA (1) | CA1340947C (fi) |
| FI (1) | FI921354A0 (fi) |
| HU (1) | HUT60696A (fi) |
| NO (1) | NO308697B1 (fi) |
| WO (1) | WO1991004940A1 (fi) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TW482651B (en) * | 1994-12-28 | 2002-04-11 | Baxter Int | Antimicrobial materials. |
| US5948385A (en) * | 1996-09-30 | 1999-09-07 | Baxter International Inc. | Antimicrobial materials |
| JP5209159B2 (ja) * | 1999-06-04 | 2013-06-12 | ボストン サイエンティフィック サイムド，インコーポレイテッド | 抗感染性装置およびその製造方法 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE559167C (de) * | 1931-12-12 | 1932-09-16 | Byk Guldenwerke Chem Fab Akt G | Reinigung von Jod durch Sublimation |
| US4769143A (en) * | 1987-02-17 | 1988-09-06 | Or-Tsurim | Device for purifying water |
-
1989
- 1989-09-28 CA CA000613953A patent/CA1340947C/en not_active Expired - Fee Related
-
1990
- 1990-08-20 HU HU9201028A patent/HUT60696A/hu unknown
- 1990-08-20 WO PCT/CA1990/000265 patent/WO1991004940A1/en not_active Application Discontinuation
- 1990-08-20 BR BR909007705A patent/BR9007705A/pt unknown
- 1990-08-20 EP EP90911944A patent/EP0494150A1/en not_active Withdrawn
- 1990-08-20 JP JP2511166A patent/JPH05500354A/ja active Pending
-
1992
- 1992-03-25 NO NO921168A patent/NO308697B1/no unknown
- 1992-03-27 FI FI921354A patent/FI921354A0/fi not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| HUT60696A (en) | 1992-10-28 |
| AU6153690A (en) | 1991-04-28 |
| HU9201028D0 (en) | 1992-08-28 |
| BR9007705A (pt) | 1992-07-21 |
| NO921168D0 (no) | 1992-03-25 |
| WO1991004940A1 (en) | 1991-04-18 |
| EP0494150A1 (en) | 1992-07-15 |
| JPH05500354A (ja) | 1993-01-28 |
| NO308697B1 (no) | 2000-10-16 |
| NO921168L (no) | 1992-05-29 |
| FI921354A (fi) | 1992-03-27 |
| FI921354A0 (fi) | 1992-03-27 |
| AU633616B2 (en) | 1993-02-04 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKLA | Lapsed |