CA1293235C - Fine powder of an acrylonitrile-type polymer and method for its production - Google Patents
Fine powder of an acrylonitrile-type polymer and method for its productionInfo
- Publication number
- CA1293235C CA1293235C CA000507789A CA507789A CA1293235C CA 1293235 C CA1293235 C CA 1293235C CA 000507789 A CA000507789 A CA 000507789A CA 507789 A CA507789 A CA 507789A CA 1293235 C CA1293235 C CA 1293235C
- Authority
- CA
- Canada
- Prior art keywords
- acrylonitrile
- particles
- type polymer
- particle size
- fine powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 229920000642 polymer Polymers 0.000 title claims abstract description 103
- 239000000843 powder Substances 0.000 title claims abstract description 59
- 238000000034 method Methods 0.000 title claims description 17
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- 239000002245 particle Substances 0.000 claims abstract description 131
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 claims abstract description 16
- 125000000542 sulfonic acid group Chemical group 0.000 claims abstract description 14
- 238000010298 pulverizing process Methods 0.000 claims description 23
- 239000011802 pulverized particle Substances 0.000 claims description 4
- 238000005054 agglomeration Methods 0.000 claims description 3
- 230000002776 aggregation Effects 0.000 claims description 3
- 239000007900 aqueous suspension Substances 0.000 claims description 3
- 238000010557 suspension polymerization reaction Methods 0.000 claims description 3
- 239000000945 filler Substances 0.000 description 15
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 9
- 239000011256 inorganic filler Substances 0.000 description 9
- 229910003475 inorganic filler Inorganic materials 0.000 description 9
- 238000006116 polymerization reaction Methods 0.000 description 9
- 239000011248 coating agent Substances 0.000 description 8
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 6
- 238000000576 coating method Methods 0.000 description 6
- 239000011247 coating layer Substances 0.000 description 5
- 239000002609 medium Substances 0.000 description 5
- 230000006866 deterioration Effects 0.000 description 4
- 238000009826 distribution Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000000178 monomer Substances 0.000 description 4
- 239000012766 organic filler Substances 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 3
- 239000010410 layer Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 229920002239 polyacrylonitrile Polymers 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 3
- 229920002554 vinyl polymer Polymers 0.000 description 3
- 239000005995 Aluminium silicate Substances 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- SOGAXMICEFXMKE-UHFFFAOYSA-N Butylmethacrylate Chemical compound CCCCOC(=O)C(C)=C SOGAXMICEFXMKE-UHFFFAOYSA-N 0.000 description 2
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 description 2
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 235000012211 aluminium silicate Nutrition 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 150000001768 cations Chemical class 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 2
- 229920000620 organic polymer Polymers 0.000 description 2
- 230000000379 polymerizing effect Effects 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 239000000741 silica gel Substances 0.000 description 2
- 229910002027 silica gel Inorganic materials 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 238000010558 suspension polymerization method Methods 0.000 description 2
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 2
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 1
- 239000004925 Acrylic resin Substances 0.000 description 1
- 229920000178 Acrylic resin Polymers 0.000 description 1
- 241000251468 Actinopterygii Species 0.000 description 1
- JIGUQPWFLRLWPJ-UHFFFAOYSA-N Ethyl acrylate Chemical compound CCOC(=O)C=C JIGUQPWFLRLWPJ-UHFFFAOYSA-N 0.000 description 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 239000012736 aqueous medium Substances 0.000 description 1
- 239000003125 aqueous solvent Substances 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 230000015271 coagulation Effects 0.000 description 1
- 238000005345 coagulation Methods 0.000 description 1
- 239000011362 coarse particle Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- -1 cyclohe~ane Chemical compound 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- FSQQTNAZHBEJLS-UPHRSURJSA-N maleamic acid Chemical compound NC(=O)\C=C/C(O)=O FSQQTNAZHBEJLS-UPHRSURJSA-N 0.000 description 1
- 125000005439 maleimidyl group Chemical class C1(C=CC(N1*)=O)=O 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000033116 oxidation-reduction process Effects 0.000 description 1
- PNJWIWWMYCMZRO-UHFFFAOYSA-N pent‐4‐en‐2‐one Natural products CC(=O)CC=C PNJWIWWMYCMZRO-UHFFFAOYSA-N 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 230000003746 surface roughness Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/12—Powdering or granulating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B9/00—Making granules
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/12—Powdering or granulating
- C08J3/122—Pulverisation by spraying
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/36—Coatings with pigments
- D21H19/38—Coatings with pigments characterised by the pigments
- D21H19/42—Coatings with pigments characterised by the pigments at least partly organic
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/50—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by form
- D21H21/52—Additives of definite length or shape
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2033/00—Use of polymers of unsaturated acids or derivatives thereof as moulding material
- B29K2033/18—Polymers of nitriles
- B29K2033/20—PAN, i.e. polyacrylonitrile
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2333/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers
- C08J2333/18—Homopolymers or copolymers of nitriles
- C08J2333/20—Homopolymers or copolymers of acrylonitrile
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Polymerisation Methods In General (AREA)
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP9871785 | 1985-05-09 | ||
JP98717/1985 | 1985-05-09 | ||
JP13151185 | 1985-06-17 | ||
JP131511/1985 | 1985-06-17 |
Publications (1)
Publication Number | Publication Date |
---|---|
CA1293235C true CA1293235C (en) | 1991-12-17 |
Family
ID=26439843
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA000507789A Expired - Lifetime CA1293235C (en) | 1985-05-09 | 1986-04-28 | Fine powder of an acrylonitrile-type polymer and method for its production |
Country Status (5)
Country | Link |
---|---|
JP (1) | JPS6289711A (enrdf_load_stackoverflow) |
AU (1) | AU583918B2 (enrdf_load_stackoverflow) |
CA (1) | CA1293235C (enrdf_load_stackoverflow) |
DE (1) | DE3615155A1 (enrdf_load_stackoverflow) |
GB (1) | GB2175591B (enrdf_load_stackoverflow) |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH075743B2 (ja) * | 1986-12-22 | 1995-01-25 | ダイキン工業株式会社 | テトラフルオロエチレン系共重合体粉末およびその製造法 |
AUPN388195A0 (en) * | 1995-06-29 | 1995-07-20 | Glover, Mark Richard | Water grinding of particulate material using high and ultra high pressure water processing |
AUPN829796A0 (en) * | 1996-02-23 | 1996-03-21 | Bengold Holdings Pty Ltd | Improved grinding method and apparatus for performing same |
DE19851676A1 (de) * | 1998-11-10 | 2000-05-11 | Bayer Ag | Thermoplastische Formmassen mit verbesserten mechanischen Eigenschaften |
FI19991742A7 (fi) * | 1999-06-24 | 2000-12-24 | Neste Chemicals Oy | Kuivana applikoituva polymeeripigmentti |
US7041781B2 (en) * | 2000-06-02 | 2006-05-09 | Bayer Aktiengesellschaft | Thermoplastic molding compounds with improved surface properties and improved structural homogeneity |
DE102005042607A1 (de) * | 2005-09-07 | 2007-03-08 | Basf Ag | Polymerisationsverfahren |
JP5773234B2 (ja) * | 2009-06-23 | 2015-09-02 | 東洋紡株式会社 | 有機系艶消し材 |
CN104761671A (zh) * | 2015-03-31 | 2015-07-08 | 东华大学 | 一种聚丙烯腈纳米乳胶粒子的制备方法 |
JP6115588B2 (ja) * | 2015-06-15 | 2017-04-19 | 東洋紡株式会社 | 有機系艶消し材 |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6026099A (ja) * | 1983-07-25 | 1985-02-08 | 株式会社リンレイ | 漂白剤 |
JPS6114201A (ja) * | 1984-06-29 | 1986-01-22 | Soken Kagaku Kk | 微粉末重合体の製造法 |
-
1986
- 1986-04-24 JP JP9563686A patent/JPS6289711A/ja active Granted
- 1986-04-28 CA CA000507789A patent/CA1293235C/en not_active Expired - Lifetime
- 1986-05-01 AU AU57077/86A patent/AU583918B2/en not_active Ceased
- 1986-05-05 DE DE19863615155 patent/DE3615155A1/de not_active Withdrawn
- 1986-05-06 GB GB8610974A patent/GB2175591B/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
GB8610974D0 (en) | 1986-06-11 |
JPS6289711A (ja) | 1987-04-24 |
GB2175591A (en) | 1986-12-03 |
AU583918B2 (en) | 1989-05-11 |
JPH0556762B2 (enrdf_load_stackoverflow) | 1993-08-20 |
GB2175591B (en) | 1989-01-25 |
AU5707786A (en) | 1986-11-13 |
DE3615155A1 (de) | 1986-11-13 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
US3669922A (en) | Process for the preparation of colored polymer powders of controlled charge and printing characteristics | |
EP0572128B1 (en) | A method of producing coated inorganic particles | |
US4254207A (en) | Process for producing spherical particles or crystalline polymers | |
CA1293235C (en) | Fine powder of an acrylonitrile-type polymer and method for its production | |
US3923704A (en) | Process for making porous polyester granules | |
US3326848A (en) | Spray dried latex toners | |
US5283151A (en) | Method for the preparation of electrostatographic toner of controlled shape by evaporative limited coalescence | |
JP2005509716A (ja) | 顔料配合インク組成物 | |
JPH0267341A (ja) | 無機質充填剤の調製方法 | |
EP0188200B1 (en) | Colored resin composition | |
EP1082376B1 (en) | Manufacturing methods, based on non aqueous dispersion techniques, to produce spherical polyester particles with narrow particle size distributions and tailorable mean particle sizes | |
US4267310A (en) | Process for producing spherical particles of crystalline polymers | |
US3661807A (en) | Soluble fluorescent materials and optical brighteners in solvent precipitation film compositions | |
JP2000103865A (ja) | 含フッ素重合体粉末の製造方法 | |
US3775357A (en) | Finely divided carbon black modified unmasticated polymers of vinyl monomers | |
JPH11268912A (ja) | 無機分散剤、懸濁重合用安定剤、重合体粒子、不飽和ポリエステル樹脂組成物及びトナー組成物 | |
CA1247367A (en) | Electrostatic recording material | |
JP3060522B2 (ja) | 樹脂粒子およびその製法 | |
GB1579233A (en) | Process for the production of powder-form hydrolysed ethylene/vinyl acetate copolymers | |
US4171274A (en) | Alteration of tesselated magnetic particles by fracture | |
GB2396925A (en) | Stencil master | |
JP4455752B2 (ja) | 着色樹脂球状微粒子の製造方法 | |
JPS63159480A (ja) | 粉体塗料 | |
JPH04211450A (ja) | 着色樹脂球状微粒子およびその製造方法 | |
JPS61258810A (ja) | アクリロニトリル系重合体微粉末 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
MKLA | Lapsed |