CA1233939A - Continuous extraction of polyphenylene sulfide - Google Patents
Continuous extraction of polyphenylene sulfideInfo
- Publication number
- CA1233939A CA1233939A CA000434393A CA434393A CA1233939A CA 1233939 A CA1233939 A CA 1233939A CA 000434393 A CA000434393 A CA 000434393A CA 434393 A CA434393 A CA 434393A CA 1233939 A CA1233939 A CA 1233939A
- Authority
- CA
- Canada
- Prior art keywords
- slurry
- polymer
- heat exchange
- temperature
- exchange medium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229920000069 polyphenylene sulfide Polymers 0.000 title description 21
- 238000000605 extraction Methods 0.000 title description 13
- 239000004734 Polyphenylene sulfide Substances 0.000 title 1
- 239000002002 slurry Substances 0.000 claims abstract description 48
- 229920000642 polymer Polymers 0.000 claims abstract description 40
- 238000000034 method Methods 0.000 claims abstract description 32
- -1 arylene sulfide Chemical compound 0.000 claims abstract description 31
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 30
- 239000012535 impurity Substances 0.000 claims abstract description 13
- 238000000926 separation method Methods 0.000 claims abstract description 6
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 12
- 239000000356 contaminant Substances 0.000 claims description 11
- 229910052783 alkali metal Inorganic materials 0.000 claims description 10
- ODPYDILFQYARBK-UHFFFAOYSA-N 7-thiabicyclo[4.1.0]hepta-1,3,5-triene Chemical group C1=CC=C2SC2=C1 ODPYDILFQYARBK-UHFFFAOYSA-N 0.000 claims description 6
- 239000011780 sodium chloride Substances 0.000 claims description 6
- 150000001340 alkali metals Chemical class 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims 2
- 239000002245 particle Substances 0.000 description 11
- 150000003839 salts Chemical class 0.000 description 6
- 150000002500 ions Chemical class 0.000 description 5
- 239000011541 reaction mixture Substances 0.000 description 5
- 238000010924 continuous production Methods 0.000 description 4
- 238000011084 recovery Methods 0.000 description 4
- PBKONEOXTCPAFI-UHFFFAOYSA-N 1,2,4-trichlorobenzene Chemical compound ClC1=CC=C(Cl)C(Cl)=C1 PBKONEOXTCPAFI-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 238000010923 batch production Methods 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 238000006116 polymerization reaction Methods 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 150000001491 aromatic compounds Chemical class 0.000 description 2
- 150000003857 carboxamides Chemical class 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000013529 heat transfer fluid Substances 0.000 description 2
- KWGKDLIKAYFUFQ-UHFFFAOYSA-M lithium chloride Chemical compound [Li+].[Cl-] KWGKDLIKAYFUFQ-UHFFFAOYSA-M 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 125000000843 phenylene group Chemical group C1(=C(C=CC=C1)*)* 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- 241000726103 Atta Species 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 description 1
- MKFMGYNOUJNFQD-UHFFFAOYSA-N OC(=O)CCCN(C)C1=CC=C(Cl)C=C1 Chemical compound OC(=O)CCCN(C)C1=CC=C(Cl)C=C1 MKFMGYNOUJNFQD-UHFFFAOYSA-N 0.000 description 1
- 206010037660 Pyrexia Diseases 0.000 description 1
- 229920013632 Ryton Polymers 0.000 description 1
- 239000004736 Ryton® Substances 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 229910001508 alkali metal halide Inorganic materials 0.000 description 1
- 150000008045 alkali metal halides Chemical class 0.000 description 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 150000007942 carboxylates Chemical class 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000002844 continuous effect Effects 0.000 description 1
- 238000011437 continuous method Methods 0.000 description 1
- 239000012809 cooling fluid Substances 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 229920006389 polyphenyl polymer Polymers 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 238000003809 water extraction Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
- C08G75/02—Polythioethers
- C08G75/0204—Polyarylenethioethers
- C08G75/0277—Post-polymerisation treatment
- C08G75/0281—Recovery or purification
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Extraction Or Liquid Replacement (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US41675682A | 1982-09-10 | 1982-09-10 | |
| US416,756 | 1982-09-10 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1233939A true CA1233939A (en) | 1988-03-08 |
Family
ID=23651185
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA000434393A Expired CA1233939A (en) | 1982-09-10 | 1983-08-11 | Continuous extraction of polyphenylene sulfide |
Country Status (6)
| Country | Link |
|---|---|
| EP (1) | EP0103261B1 (OSRAM) |
| JP (1) | JPS5949233A (OSRAM) |
| AT (1) | ATE125279T1 (OSRAM) |
| CA (1) | CA1233939A (OSRAM) |
| DE (1) | DE3382790T2 (OSRAM) |
| ES (1) | ES525489A0 (OSRAM) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0292211A3 (en) * | 1987-05-18 | 1989-06-14 | Imperial Chemical Industries Plc | Production and/or handling of polymers |
| ES2051811T3 (es) * | 1987-10-05 | 1994-07-01 | Phillips Petroleum Co | Metodo para recuperar poli(sulfuros de arileno) con liquidos vaporizados. |
| US4877850A (en) * | 1988-02-22 | 1989-10-31 | Phillips Petroleum Company | Buffer wash of polyarylene sulfides |
| JPH0386287A (ja) * | 1989-08-28 | 1991-04-11 | Idemitsu Petrochem Co Ltd | 粉粒状樹脂の洗浄方法およびその洗浄装置 |
| JP2010100701A (ja) * | 2008-10-22 | 2010-05-06 | Toray Ind Inc | 樹脂スラリーの処理方法 |
| JP5630258B2 (ja) * | 2010-12-27 | 2014-11-26 | 東レ株式会社 | ポリアリーレンスルフィド樹脂の製造方法 |
| US10029230B1 (en) | 2017-01-24 | 2018-07-24 | Chevron Phillips Chemical Company Lp | Flow in a slurry loop reactor |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3354129A (en) | 1963-11-27 | 1967-11-21 | Phillips Petroleum Co | Production of polymers from aromatic compounds |
| US3457242A (en) * | 1966-08-22 | 1969-07-22 | Phillips Petroleum Co | Arylene sulfide polymer recovery |
| US3478000A (en) * | 1967-11-20 | 1969-11-11 | Phillips Petroleum Co | Recovery of poly(arylene sulfides) |
| US3800845A (en) * | 1971-12-14 | 1974-04-02 | Phillips Petroleum Co | Solvent removal from poly(arylene sulfide) reaction slurry |
| US3956060A (en) * | 1971-12-30 | 1976-05-11 | Phillips Petroleum Company | Removal of reaction diluent from poly(arylene sulfide) reaction slurry |
| US3919177A (en) | 1973-11-19 | 1975-11-11 | Phillips Petroleum Co | P-phenylene sulfide polymers |
| US4025496A (en) * | 1975-10-10 | 1977-05-24 | Phillips Petroleum Company | Sequenced addition of components in poly(arylene sulfide) production |
| JPS55156342A (en) * | 1979-05-25 | 1980-12-05 | Hitachi Ltd | Resin sealed electronic parts |
| JPS57108135A (en) * | 1980-12-26 | 1982-07-06 | Asahi Glass Co Ltd | Method for removing common salt from polyphenylene sulfide resin |
-
1983
- 1983-07-27 JP JP58137434A patent/JPS5949233A/ja active Granted
- 1983-08-11 CA CA000434393A patent/CA1233939A/en not_active Expired
- 1983-09-06 DE DE3382790T patent/DE3382790T2/de not_active Expired - Lifetime
- 1983-09-06 EP EP83108780A patent/EP0103261B1/en not_active Expired - Lifetime
- 1983-09-06 AT AT83108780T patent/ATE125279T1/de active
- 1983-09-08 ES ES525489A patent/ES525489A0/es active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| ES8503011A1 (es) | 1985-02-01 |
| ATE125279T1 (de) | 1995-08-15 |
| DE3382790T2 (de) | 1995-11-30 |
| JPS5949233A (ja) | 1984-03-21 |
| EP0103261B1 (en) | 1995-07-19 |
| DE3382790D1 (de) | 1995-08-24 |
| EP0103261A3 (en) | 1984-11-07 |
| JPH0529649B2 (OSRAM) | 1993-05-06 |
| ES525489A0 (es) | 1985-02-01 |
| EP0103261A2 (en) | 1984-03-21 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEX | Expiry | ||
| MKEX | Expiry |
Effective date: 20050308 |