CA1209512A - Used oil re-refining - Google Patents
Used oil re-refiningInfo
- Publication number
- CA1209512A CA1209512A CA000447462A CA447462A CA1209512A CA 1209512 A CA1209512 A CA 1209512A CA 000447462 A CA000447462 A CA 000447462A CA 447462 A CA447462 A CA 447462A CA 1209512 A CA1209512 A CA 1209512A
- Authority
- CA
- Canada
- Prior art keywords
- oil
- heat
- distillate
- distillation
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000010913 used oil Substances 0.000 title claims abstract description 83
- 238000007670 refining Methods 0.000 title abstract description 13
- 239000003921 oil Substances 0.000 claims abstract description 108
- 238000000034 method Methods 0.000 claims abstract description 67
- 238000002791 soaking Methods 0.000 claims abstract description 58
- 239000000463 material Substances 0.000 claims abstract description 28
- 238000009835 boiling Methods 0.000 claims abstract description 18
- 239000010687 lubricating oil Substances 0.000 claims abstract description 16
- 239000012084 conversion product Substances 0.000 claims abstract description 14
- 238000004821 distillation Methods 0.000 claims description 59
- 230000008569 process Effects 0.000 claims description 50
- 239000010802 sludge Substances 0.000 claims description 44
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 31
- 229910052698 phosphorus Inorganic materials 0.000 claims description 31
- 239000011574 phosphorus Substances 0.000 claims description 31
- 150000004820 halides Chemical class 0.000 claims description 27
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 26
- 239000000047 product Substances 0.000 claims description 19
- 239000007789 gas Substances 0.000 claims description 17
- 239000002243 precursor Substances 0.000 claims description 11
- 239000002199 base oil Substances 0.000 claims description 10
- 230000015572 biosynthetic process Effects 0.000 claims description 9
- 239000000571 coke Substances 0.000 claims description 9
- 239000001257 hydrogen Substances 0.000 claims description 8
- 229910052739 hydrogen Inorganic materials 0.000 claims description 8
- 239000010409 thin film Substances 0.000 claims description 8
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 6
- 239000010408 film Substances 0.000 claims description 5
- 235000008733 Citrus aurantifolia Nutrition 0.000 claims description 4
- 235000011941 Tilia x europaea Nutrition 0.000 claims description 4
- 239000003610 charcoal Substances 0.000 claims description 4
- 239000004571 lime Substances 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 claims 1
- 239000010779 crude oil Substances 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 18
- 239000000446 fuel Substances 0.000 abstract description 17
- 239000002699 waste material Substances 0.000 abstract description 14
- 230000001627 detrimental effect Effects 0.000 abstract description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 39
- 239000002184 metal Substances 0.000 description 17
- 229910052751 metal Inorganic materials 0.000 description 17
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 16
- 239000003054 catalyst Substances 0.000 description 13
- 230000002829 reductive effect Effects 0.000 description 13
- 239000002253 acid Substances 0.000 description 11
- 239000000203 mixture Substances 0.000 description 11
- 239000004927 clay Substances 0.000 description 10
- 239000000654 additive Substances 0.000 description 9
- -1 dirt Substances 0.000 description 9
- 229910052736 halogen Inorganic materials 0.000 description 9
- 150000002367 halogens Chemical class 0.000 description 9
- 150000002739 metals Chemical class 0.000 description 9
- 229910052757 nitrogen Inorganic materials 0.000 description 8
- 238000012545 processing Methods 0.000 description 8
- 239000000356 contaminant Substances 0.000 description 7
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 7
- 239000003463 adsorbent Substances 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 5
- 230000008901 benefit Effects 0.000 description 5
- 150000001875 compounds Chemical class 0.000 description 5
- 230000007613 environmental effect Effects 0.000 description 5
- 238000007689 inspection Methods 0.000 description 5
- 230000035515 penetration Effects 0.000 description 5
- 239000007787 solid Substances 0.000 description 5
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- 239000010426 asphalt Substances 0.000 description 4
- 230000003247 decreasing effect Effects 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 229930195733 hydrocarbon Natural products 0.000 description 4
- 150000002430 hydrocarbons Chemical class 0.000 description 4
- 230000009467 reduction Effects 0.000 description 4
- 238000005292 vacuum distillation Methods 0.000 description 4
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 3
- 239000004215 Carbon black (E152) Substances 0.000 description 3
- 230000000996 additive effect Effects 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 3
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 3
- 229910052794 bromium Inorganic materials 0.000 description 3
- 238000004939 coking Methods 0.000 description 3
- 230000009849 deactivation Effects 0.000 description 3
- 238000000354 decomposition reaction Methods 0.000 description 3
- 150000002500 ions Chemical class 0.000 description 3
- 150000003018 phosphorus compounds Chemical class 0.000 description 3
- 230000000704 physical effect Effects 0.000 description 3
- 238000011084 recovery Methods 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 229910052717 sulfur Inorganic materials 0.000 description 3
- 239000011593 sulfur Substances 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
- CPELXLSAUQHCOX-UHFFFAOYSA-N Hydrogen bromide Chemical compound Br CPELXLSAUQHCOX-UHFFFAOYSA-N 0.000 description 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- 239000005864 Sulphur Substances 0.000 description 2
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical group ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 description 2
- 230000002411 adverse Effects 0.000 description 2
- 238000000998 batch distillation Methods 0.000 description 2
- 150000001649 bromium compounds Chemical class 0.000 description 2
- 150000001805 chlorine compounds Chemical class 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 239000002270 dispersing agent Substances 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 229910052750 molybdenum Inorganic materials 0.000 description 2
- 239000000178 monomer Substances 0.000 description 2
- 230000000737 periodic effect Effects 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- 230000004044 response Effects 0.000 description 2
- 239000004576 sand Substances 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 239000010454 slate Substances 0.000 description 2
- 125000000101 thioether group Chemical group 0.000 description 2
- UBOXGVDOUJQMTN-UHFFFAOYSA-N trichloroethylene Natural products ClCC(Cl)Cl UBOXGVDOUJQMTN-UHFFFAOYSA-N 0.000 description 2
- 239000010723 turbine oil Substances 0.000 description 2
- GNFTZDOKVXKIBK-UHFFFAOYSA-N 3-(2-methoxyethoxy)benzohydrazide Chemical compound COCCOC1=CC=CC(C(=O)NN)=C1 GNFTZDOKVXKIBK-UHFFFAOYSA-N 0.000 description 1
- 241000212384 Bifora Species 0.000 description 1
- 101100004287 Caenorhabditis elegans best-6 gene Proteins 0.000 description 1
- 241000543381 Cliftonia monophylla Species 0.000 description 1
- 239000005696 Diammonium phosphate Substances 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 230000002745 absorbent Effects 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000008186 active pharmaceutical agent Substances 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 235000019270 ammonium chloride Nutrition 0.000 description 1
- 239000002519 antifouling agent Substances 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000003190 augmentative effect Effects 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 229910017052 cobalt Inorganic materials 0.000 description 1
- 239000010941 cobalt Substances 0.000 description 1
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000010908 decantation Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000002939 deleterious effect Effects 0.000 description 1
- 239000002274 desiccant Substances 0.000 description 1
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 description 1
- 229910000388 diammonium phosphate Inorganic materials 0.000 description 1
- 235000019838 diammonium phosphate Nutrition 0.000 description 1
- 230000003467 diminishing effect Effects 0.000 description 1
- 238000011143 downstream manufacturing Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000002920 hazardous waste Substances 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 229910000042 hydrogen bromide Inorganic materials 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 230000003340 mental effect Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000002808 molecular sieve Substances 0.000 description 1
- 239000011733 molybdenum Substances 0.000 description 1
- 239000010705 motor oil Substances 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 238000013441 quality evaluation Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000012958 reprocessing Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 150000003568 thioethers Chemical class 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M175/00—Working-up used lubricants to recover useful products ; Cleaning
- C10M175/02—Working-up used lubricants to recover useful products ; Cleaning mineral-oil based
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Fats And Perfumes (AREA)
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US46710083A | 1983-02-16 | 1983-02-16 | |
| US06/467,032 US4512878A (en) | 1983-02-16 | 1983-02-16 | Used oil re-refining |
| US467,032 | 1983-02-16 | ||
| US467,100 | 1990-01-18 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1209512A true CA1209512A (en) | 1986-08-12 |
Family
ID=27041884
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA000447462A Expired CA1209512A (en) | 1983-02-16 | 1984-02-15 | Used oil re-refining |
Country Status (5)
| Country | Link |
|---|---|
| CA (1) | CA1209512A (enrdf_load_stackoverflow) |
| DE (1) | DE3405858C2 (enrdf_load_stackoverflow) |
| GR (1) | GR79510B (enrdf_load_stackoverflow) |
| MX (1) | MX165696B (enrdf_load_stackoverflow) |
| NO (1) | NO163906C (enrdf_load_stackoverflow) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US12122965B2 (en) | 2020-07-07 | 2024-10-22 | Haldor Topsøe A/S | Porous material for removing impurities in feedstocks |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL8402837A (nl) * | 1984-09-14 | 1986-04-01 | Kinetics Technology | Werkwijze voor het zuiveren en/of onschadelijk maken van een door halogeen-, stikstof- en/of zwavel (verbindingen) verontreinigde vloeibare koolwaterstofstroom. |
| DE3537384A1 (de) * | 1985-10-21 | 1987-04-23 | Goetze Ag | Verfahren zum reinigen von kuehlmittelschmierstoffen |
| DE3703110A1 (de) * | 1986-11-12 | 1987-10-08 | Christian Schoen | Verfahren zur kontinuierlichen aufbereitung von altoel |
| DE3839799A1 (de) * | 1988-11-25 | 1990-07-05 | Rwe Entsorgung Ag | Verfahren zur aufarbeitung kontaminierter oele |
| DE19837276B4 (de) * | 1998-08-18 | 2008-09-04 | ECO IMPACT Brüske Gesellschaft für Umwelttechnik und Apparatebau mbH | Verfahren und Vorrichtung zum Destillieren und Cracken von Altölen |
| DE102006057910A1 (de) * | 2006-12-08 | 2008-07-03 | Exad Gmbh | Verfahren zum Aufbereiten von Altölen und/oder Öl/Wassergemischen oder ähnlichen flüssigen Gemischen |
| EP3714026B1 (en) * | 2017-11-22 | 2022-01-12 | Itelyum Regeneration S.p.A. | Use of alumina in a plant for the regeneration of waste oils |
| CN109321350A (zh) * | 2018-11-06 | 2019-02-12 | 宁波中循环保科技有限公司 | 一种脱除废润滑油中添加剂的方法 |
| FI128237B (en) * | 2018-12-21 | 2020-01-15 | Neste Oyj | METHOD FOR UPGRADING GAME OILS |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3923643A (en) * | 1974-06-14 | 1975-12-02 | Shell Oil Co | Removal of lead and other suspended solids from used hydrocarbon lubricating oil |
| US3919076A (en) * | 1974-07-18 | 1975-11-11 | Pilot Res & Dev Co | Re-refining used automotive lubricating oil |
| US3930988A (en) * | 1975-02-24 | 1976-01-06 | Phillips Petroleum Company | Reclaiming used motor oil |
| US4033859A (en) * | 1975-04-24 | 1977-07-05 | Witco Chemical Corporation | Thermal treatment of used petroleum oils |
| IT1137280B (it) * | 1981-07-07 | 1986-09-03 | Assoreni E Snamprogetti Spa | Procedimento per recupero di oli esausti |
-
1984
- 1984-02-10 MX MX823784A patent/MX165696B/es unknown
- 1984-02-13 GR GR73793A patent/GR79510B/el unknown
- 1984-02-15 CA CA000447462A patent/CA1209512A/en not_active Expired
- 1984-02-15 NO NO840556A patent/NO163906C/no unknown
- 1984-02-15 DE DE19843405858 patent/DE3405858C2/de not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US12122965B2 (en) | 2020-07-07 | 2024-10-22 | Haldor Topsøe A/S | Porous material for removing impurities in feedstocks |
Also Published As
| Publication number | Publication date |
|---|---|
| DE3405858A1 (de) | 1984-08-16 |
| NO163906C (no) | 1990-08-15 |
| NO840556L (no) | 1984-08-17 |
| GR79510B (enrdf_load_stackoverflow) | 1984-10-30 |
| MX165696B (es) | 1992-12-01 |
| DE3405858C2 (de) | 1994-11-24 |
| NO163906B (no) | 1990-04-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEX | Expiry |