CA1094292A - Procede de decomposition thermique du chlorure d'aluminium hexa-hydrate par chauffage indirect - Google Patents
Procede de decomposition thermique du chlorure d'aluminium hexa-hydrate par chauffage indirectInfo
- Publication number
- CA1094292A CA1094292A CA284,678A CA284678A CA1094292A CA 1094292 A CA1094292 A CA 1094292A CA 284678 A CA284678 A CA 284678A CA 1094292 A CA1094292 A CA 1094292A
- Authority
- CA
- Canada
- Prior art keywords
- reactor
- gas
- calcination
- fluidized bed
- fact
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000001354 calcination Methods 0.000 claims abstract description 81
- 239000007787 solid Substances 0.000 claims abstract description 60
- 238000000034 method Methods 0.000 claims abstract description 40
- 238000000354 decomposition reaction Methods 0.000 claims abstract description 38
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims abstract description 27
- 239000000725 suspension Substances 0.000 claims abstract description 27
- 238000010438 heat treatment Methods 0.000 claims abstract description 21
- 239000007789 gas Substances 0.000 claims description 168
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 claims description 42
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 26
- 238000005243 fluidization Methods 0.000 claims description 18
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 13
- 239000001301 oxygen Substances 0.000 claims description 13
- 229910052760 oxygen Inorganic materials 0.000 claims description 13
- 239000000463 material Substances 0.000 claims description 8
- 239000002253 acid Substances 0.000 claims description 7
- 239000000446 fuel Substances 0.000 claims description 6
- 238000005979 thermal decomposition reaction Methods 0.000 claims description 5
- 238000000605 extraction Methods 0.000 claims description 4
- 150000001805 chlorine compounds Chemical group 0.000 claims description 3
- 230000007423 decrease Effects 0.000 claims description 3
- 230000003134 recirculating effect Effects 0.000 claims description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 2
- 229910052782 aluminium Inorganic materials 0.000 claims description 2
- JGDITNMASUZKPW-UHFFFAOYSA-K aluminium trichloride hexahydrate Chemical compound O.O.O.O.O.O.Cl[Al](Cl)Cl JGDITNMASUZKPW-UHFFFAOYSA-K 0.000 abstract description 8
- 229940009861 aluminum chloride hexahydrate Drugs 0.000 abstract description 7
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 229940063656 aluminum chloride Drugs 0.000 description 17
- 239000000047 product Substances 0.000 description 14
- 238000004064 recycling Methods 0.000 description 12
- 239000000428 dust Substances 0.000 description 11
- 238000001816 cooling Methods 0.000 description 10
- 238000006243 chemical reaction Methods 0.000 description 9
- 150000003839 salts Chemical class 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- 238000010521 absorption reaction Methods 0.000 description 6
- 238000002485 combustion reaction Methods 0.000 description 5
- 238000009434 installation Methods 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 239000002245 particle Substances 0.000 description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 4
- 239000012530 fluid Substances 0.000 description 4
- 239000010763 heavy fuel oil Substances 0.000 description 4
- 150000004687 hexahydrates Chemical class 0.000 description 3
- 238000011068 loading method Methods 0.000 description 3
- 238000013021 overheating Methods 0.000 description 3
- JTJMJGYZQZDUJJ-UHFFFAOYSA-N phencyclidine Chemical class C1CCCCN1C1(C=2C=CC=CC=2)CCCCC1 JTJMJGYZQZDUJJ-UHFFFAOYSA-N 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 239000011343 solid material Substances 0.000 description 3
- 239000012265 solid product Substances 0.000 description 3
- 238000010586 diagram Methods 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 239000013529 heat transfer fluid Substances 0.000 description 2
- 238000009834 vaporization Methods 0.000 description 2
- 230000008016 vaporization Effects 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- 102100026933 Myelin-associated neurite-outgrowth inhibitor Human genes 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- PPNXXZIBFHTHDM-UHFFFAOYSA-N aluminium phosphide Chemical compound P#[Al] PPNXXZIBFHTHDM-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 239000002737 fuel gas Substances 0.000 description 1
- 239000000295 fuel oil Substances 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000003758 nuclear fuel Substances 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000003507 refrigerant Substances 0.000 description 1
- 238000003303 reheating Methods 0.000 description 1
- 238000010079 rubber tapping Methods 0.000 description 1
- 239000012798 spherical particle Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
- C01F7/30—Preparation of aluminium oxide or hydroxide by thermal decomposition or by hydrolysis or oxidation of aluminium compounds
- C01F7/306—Thermal decomposition of hydrated chlorides, e.g. of aluminium trichloride hexahydrate
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S423/00—Chemistry of inorganic compounds
- Y10S423/09—Reaction techniques
- Y10S423/16—Fluidization
Landscapes
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEP2636854.7 | 1976-08-16 | ||
| DE2636854A DE2636854C2 (de) | 1976-08-16 | 1976-08-16 | Verfahren zur thermischen Spaltung von Aluminiumchloridhydrat |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1094292A true CA1094292A (fr) | 1981-01-27 |
Family
ID=5985573
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA284,678A Expired CA1094292A (fr) | 1976-08-16 | 1977-08-12 | Procede de decomposition thermique du chlorure d'aluminium hexa-hydrate par chauffage indirect |
Country Status (22)
| Country | Link |
|---|---|
| US (1) | US4091085A (enExample) |
| JP (1) | JPS5355498A (enExample) |
| AR (1) | AR219712A1 (enExample) |
| AU (1) | AU512098B2 (enExample) |
| BE (1) | BE857799A (enExample) |
| BR (1) | BR7705400A (enExample) |
| CA (1) | CA1094292A (enExample) |
| DD (1) | DD131086A5 (enExample) |
| DE (1) | DE2636854C2 (enExample) |
| DK (1) | DK361677A (enExample) |
| ES (1) | ES461616A1 (enExample) |
| FR (1) | FR2362082A1 (enExample) |
| GB (1) | GB1569412A (enExample) |
| IL (1) | IL52733A0 (enExample) |
| IT (1) | IT1114917B (enExample) |
| LU (1) | LU77965A1 (enExample) |
| MX (1) | MX147243A (enExample) |
| NL (1) | NL184776C (enExample) |
| NZ (1) | NZ184916A (enExample) |
| PL (1) | PL113235B1 (enExample) |
| SE (1) | SE417701B (enExample) |
| ZA (1) | ZA774912B (enExample) |
Families Citing this family (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2805906C2 (de) * | 1978-02-13 | 1986-08-14 | Aluminium Pechiney, Lyon | Verfahren zur thermischen Spaltung von Aluminiumchloridhydrat |
| JPS5813505U (ja) * | 1981-07-17 | 1983-01-27 | 日本電信電話株式会社 | マルチコア光フアイバ |
| US4402932A (en) * | 1982-05-07 | 1983-09-06 | The United States Of America As Represented By The Secretary Of The Interior | Thermal decomposition of aluminum chloride hexahydrate |
| US4584178A (en) * | 1984-11-16 | 1986-04-22 | Quantum Teechnologies, Inc. | Apparatus for the manufacture of hypochlorous acid |
| DE10260745A1 (de) * | 2002-12-23 | 2004-07-01 | Outokumpu Oyj | Verfahren und Anlage zur thermischen Behandlung von körnigen Feststoffen |
| DE10260738A1 (de) * | 2002-12-23 | 2004-07-15 | Outokumpu Oyj | Verfahren und Anlage zur Förderung von feinkörnigen Feststoffen |
| DE10260737B4 (de) * | 2002-12-23 | 2005-06-30 | Outokumpu Oyj | Verfahren und Anlage zur Wärmebehandlung von titanhaltigen Feststoffen |
| DE10260733B4 (de) * | 2002-12-23 | 2010-08-12 | Outokumpu Oyj | Verfahren und Anlage zur Wärmebehandlung von eisenoxidhaltigen Feststoffen |
| DE10260731B4 (de) | 2002-12-23 | 2005-04-14 | Outokumpu Oyj | Verfahren und Anlage zur Wärmebehandlung von eisenoxidhaltigen Feststoffen |
| DE10260739B3 (de) * | 2002-12-23 | 2004-09-16 | Outokumpu Oy | Verfahren und Anlage zur Herstellung von Metalloxid aus Metallverbindungen |
| DE10260741A1 (de) * | 2002-12-23 | 2004-07-08 | Outokumpu Oyj | Verfahren und Anlage zur Wärmebehandlung von feinkörnigen Feststoffen |
| DE10260734B4 (de) * | 2002-12-23 | 2005-05-04 | Outokumpu Oyj | Verfahren und Anlage zur Herstellung von Schwelkoks |
| DE102004042430A1 (de) * | 2004-08-31 | 2006-03-16 | Outokumpu Oyj | Wirbelschichtreaktor zum thermischen Behandeln von wirbelfähigen Substanzen in einem mikrowellenbeheizten Wirbelbett |
| DE102004049364A1 (de) * | 2004-10-08 | 2006-04-20 | Kerr-Mcgee Pigments Gmbh | Wirbelschichtreaktor und Verfahren zur Durchführung von Wilbelschichtreaktionen |
| JP2014508863A (ja) | 2011-03-18 | 2014-04-10 | オーバイト アルミナ インコーポレイテッド | アルミニウム含有材料から希土類元素を回収する方法 |
| IN2014DN03007A (enExample) | 2011-09-16 | 2015-05-08 | Orbite Aluminae Inc | |
| US9023301B2 (en) | 2012-01-10 | 2015-05-05 | Orbite Aluminae Inc. | Processes for treating red mud |
| CA2903512C (en) | 2012-03-29 | 2017-12-05 | Orbite Technologies Inc. | Processes for treating fly ashes |
| DE102016103100A1 (de) * | 2016-02-23 | 2017-08-24 | Outotec (Finland) Oy | Verfahren und Vorrichtung zur thermischen Behandlung von körnigen Feststoffen |
| CN108751244B (zh) * | 2018-07-06 | 2024-04-09 | 北京航天石化技术装备工程有限公司 | 一种结晶铝盐焙烧制备工业级氧化铝的集成装置 |
| KR20220024213A (ko) * | 2019-06-07 | 2022-03-03 | 메트소 오토텍 핀란드 오이 | 염화알루미늄 수화물을 산화알루미늄으로 열분해하는 방법 및 설비 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA788920A (en) * | 1968-07-02 | Rohrbach Rudolf | Process for heat treating material | |
| US2539263A (en) * | 1942-10-28 | 1951-01-23 | Standard Oil Dev Co | Contacting finely divided solids with gases |
| US3130008A (en) * | 1949-11-23 | 1964-04-21 | Cabot Corp | Method of preparing metallic oxides by hydrolysis of metallic halides |
| US2780525A (en) * | 1953-10-08 | 1957-02-05 | Cabot Godfrey L Inc | Process and apparatus for the production of aluminum oxide from aluminum chloride |
| US3144303A (en) * | 1960-08-30 | 1964-08-11 | Du Pont | Fluidization process |
| DE1767628C3 (de) * | 1968-05-30 | 1985-03-14 | Metallgesellschaft Ag, 6000 Frankfurt | Verfahren zur Durchführung endothermer Prozesse |
| JPS501700B1 (enExample) * | 1969-06-21 | 1975-01-21 | ||
| US3648380A (en) * | 1970-05-28 | 1972-03-14 | Aluminum Co Of America | Fluidized bed level control |
| DE2106306C3 (de) * | 1971-02-10 | 1974-12-19 | Metallgesellschaft Ag, 6000 Frankfurt | Verfahren zur Herstellung von Aluminiumfluorid |
| DE2261083C3 (de) * | 1972-12-14 | 1979-05-31 | Metallgesellschaft Ag, 6000 Frankfurt | Verfahren zur thermischen Spaltung von Metallchloriden |
-
1976
- 1976-08-16 DE DE2636854A patent/DE2636854C2/de not_active Expired
-
1977
- 1977-06-13 FR FR7718893A patent/FR2362082A1/fr active Granted
- 1977-08-05 AU AU27905/77A patent/AU512098B2/en not_active Expired
- 1977-08-11 US US05/823,644 patent/US4091085A/en not_active Expired - Lifetime
- 1977-08-12 AR AR268780A patent/AR219712A1/es active
- 1977-08-12 CA CA284,678A patent/CA1094292A/fr not_active Expired
- 1977-08-12 DD DD7700200553A patent/DD131086A5/xx unknown
- 1977-08-12 IT IT26665/77A patent/IT1114917B/it active
- 1977-08-12 NZ NZ184916A patent/NZ184916A/xx unknown
- 1977-08-12 LU LU77965A patent/LU77965A1/xx unknown
- 1977-08-15 SE SE7709199A patent/SE417701B/xx not_active IP Right Cessation
- 1977-08-15 IL IL52733A patent/IL52733A0/xx not_active IP Right Cessation
- 1977-08-15 ZA ZA00774912A patent/ZA774912B/xx unknown
- 1977-08-15 MX MX170233A patent/MX147243A/es unknown
- 1977-08-15 BR BR7705400A patent/BR7705400A/pt unknown
- 1977-08-15 GB GB34216/77A patent/GB1569412A/en not_active Expired
- 1977-08-15 JP JP9772177A patent/JPS5355498A/ja active Granted
- 1977-08-15 PL PL1977200286A patent/PL113235B1/pl unknown
- 1977-08-15 DK DK361677A patent/DK361677A/da unknown
- 1977-08-16 BE BE180179A patent/BE857799A/xx not_active IP Right Cessation
- 1977-08-16 NL NLAANVRAGE7709058,A patent/NL184776C/xx not_active IP Right Cessation
- 1977-08-16 ES ES461616A patent/ES461616A1/es not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| FR2362082B1 (enExample) | 1981-10-02 |
| DE2636854A1 (de) | 1978-02-23 |
| JPS5355498A (en) | 1978-05-19 |
| NZ184916A (en) | 1980-02-21 |
| FR2362082A1 (fr) | 1978-03-17 |
| IL52733A0 (en) | 1977-10-31 |
| SE7709199L (sv) | 1978-02-17 |
| DD131086A5 (de) | 1978-05-31 |
| US4091085A (en) | 1978-05-23 |
| LU77965A1 (enExample) | 1978-04-27 |
| JPS5635605B2 (enExample) | 1981-08-18 |
| BR7705400A (pt) | 1978-06-06 |
| BE857799A (fr) | 1978-02-16 |
| PL200286A1 (pl) | 1978-04-10 |
| NL184776B (nl) | 1989-06-01 |
| AU512098B2 (en) | 1980-09-25 |
| ZA774912B (en) | 1978-09-27 |
| MX147243A (es) | 1982-10-28 |
| AU2790577A (en) | 1979-02-22 |
| DK361677A (da) | 1978-02-17 |
| NL7709058A (nl) | 1978-02-20 |
| AR219712A1 (es) | 1980-09-15 |
| SE417701B (sv) | 1981-04-06 |
| DE2636854C2 (de) | 1986-08-21 |
| IT1114917B (it) | 1986-02-03 |
| ES461616A1 (es) | 1978-06-16 |
| GB1569412A (en) | 1980-06-18 |
| NL184776C (nl) | 1989-11-01 |
| PL113235B1 (en) | 1980-11-29 |
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| BE499540A (enExample) |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEX | Expiry |