CA1053132A - Apparatus, composition and method for detecting free water in hydrocarbon fuels - Google Patents
Apparatus, composition and method for detecting free water in hydrocarbon fuelsInfo
- Publication number
- CA1053132A CA1053132A CA216,433A CA216433A CA1053132A CA 1053132 A CA1053132 A CA 1053132A CA 216433 A CA216433 A CA 216433A CA 1053132 A CA1053132 A CA 1053132A
- Authority
- CA
- Canada
- Prior art keywords
- vial
- free water
- cannula
- receptacle
- dye
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 34
- 229930195733 hydrocarbon Natural products 0.000 title claims abstract description 26
- 150000002430 hydrocarbons Chemical class 0.000 title claims abstract description 26
- 239000004215 Carbon black (E152) Substances 0.000 title claims abstract description 16
- 238000000034 method Methods 0.000 title claims abstract description 5
- 239000000446 fuel Substances 0.000 title abstract description 38
- 239000000203 mixture Substances 0.000 title abstract description 19
- 239000007787 solid Substances 0.000 claims abstract description 23
- 239000003153 chemical reaction reagent Substances 0.000 claims abstract description 21
- 239000002245 particle Substances 0.000 claims abstract description 11
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract description 10
- 229910000019 calcium carbonate Inorganic materials 0.000 claims abstract description 5
- 241000720913 Fuchsia Species 0.000 claims description 9
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 claims description 8
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 claims description 4
- 239000001095 magnesium carbonate Substances 0.000 claims description 4
- 229910000021 magnesium carbonate Inorganic materials 0.000 claims description 4
- 239000000126 substance Substances 0.000 claims description 4
- AYJRCSIUFZENHW-DEQYMQKBSA-L barium(2+);oxomethanediolate Chemical compound [Ba+2].[O-][14C]([O-])=O AYJRCSIUFZENHW-DEQYMQKBSA-L 0.000 claims description 3
- 238000005070 sampling Methods 0.000 claims description 2
- 229940092690 barium sulfate Drugs 0.000 claims 2
- 238000005192 partition Methods 0.000 claims 2
- 239000011521 glass Substances 0.000 abstract description 8
- 238000001514 detection method Methods 0.000 abstract description 5
- 239000007788 liquid Substances 0.000 abstract description 3
- 240000007108 Fuchsia magellanica Species 0.000 abstract 1
- 239000000523 sample Substances 0.000 description 11
- 230000035945 sensitivity Effects 0.000 description 10
- 238000012360 testing method Methods 0.000 description 7
- 239000000463 material Substances 0.000 description 5
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 3
- 239000004753 textile Substances 0.000 description 2
- NSMXQKNUPPXBRG-SECBINFHSA-N (R)-lisofylline Chemical compound O=C1N(CCCC[C@H](O)C)C(=O)N(C)C2=C1N(C)C=N2 NSMXQKNUPPXBRG-SECBINFHSA-N 0.000 description 1
- SQHWUYVHKRVCMD-UHFFFAOYSA-N 2-n,2-n-dimethyl-10-phenylphenazin-10-ium-2,8-diamine;chloride Chemical compound [Cl-].C12=CC(N(C)C)=CC=C2N=C2C=CC(N)=CC2=[N+]1C1=CC=CC=C1 SQHWUYVHKRVCMD-UHFFFAOYSA-N 0.000 description 1
- XPYQFIISZQCINN-QVXDJYSKSA-N 4-amino-1-[(2r,3e,4s,5r)-3-(fluoromethylidene)-4-hydroxy-5-(hydroxymethyl)oxolan-2-yl]pyrimidin-2-one;hydrate Chemical compound O.O=C1N=C(N)C=CN1[C@H]1C(=C/F)/[C@H](O)[C@@H](CO)O1 XPYQFIISZQCINN-QVXDJYSKSA-N 0.000 description 1
- ALJHHTHBYJROOG-UHFFFAOYSA-N 7-(dimethylamino)phenothiazin-3-one Chemical compound C1=CC(=O)C=C2SC3=CC(N(C)C)=CC=C3N=C21 ALJHHTHBYJROOG-UHFFFAOYSA-N 0.000 description 1
- 229920001213 Polysorbate 20 Polymers 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfate Natural products OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
- 241000153282 Theope Species 0.000 description 1
- 229910052788 barium Inorganic materials 0.000 description 1
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000000256 polyoxyethylene sorbitan monolaurate Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000000284 resting effect Effects 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N31/00—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
- G01N31/22—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using chemical indicators
- G01N31/222—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using chemical indicators for investigating moisture content
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/26—Oils; Viscous liquids; Paints; Inks
- G01N33/28—Oils, i.e. hydrocarbon liquids
- G01N33/2835—Specific substances contained in the oils or fuels
- G01N33/2847—Water in oils
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- Pathology (AREA)
- Immunology (AREA)
- General Physics & Mathematics (AREA)
- General Health & Medical Sciences (AREA)
- Physics & Mathematics (AREA)
- Engineering & Computer Science (AREA)
- Medicinal Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Food Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Biophysics (AREA)
- Molecular Biology (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Optical Measuring Cells (AREA)
- Spectrometry And Color Measurement (AREA)
- Investigating Or Analysing Materials By The Use Of Chemical Reactions (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CA307,697A CA1059410A (en) | 1974-01-02 | 1978-07-19 | Packaged composition useful for detecting free water in hydrocarbon fuels |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US429973A US3873271A (en) | 1974-01-02 | 1974-01-02 | Method and apparatus for detecting free water in hydrocarbon fuels |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1053132A true CA1053132A (en) | 1979-04-24 |
Family
ID=23705522
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA216,433A Expired CA1053132A (en) | 1974-01-02 | 1974-12-19 | Apparatus, composition and method for detecting free water in hydrocarbon fuels |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US3873271A (de) |
| JP (1) | JPS5819988B2 (de) |
| CA (1) | CA1053132A (de) |
| DE (2) | DE2461585C2 (de) |
| GB (2) | GB1486779A (de) |
Families Citing this family (39)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3976572A (en) * | 1974-01-04 | 1976-08-24 | Michael Ebert | Aircraft fuel contaminant tester |
| CH585403A5 (de) * | 1974-05-10 | 1977-02-28 | Battelle Memorial Institute | |
| GB1583943A (en) * | 1976-05-12 | 1981-02-04 | Mobil Oil Corp | Ditection of water in an oil |
| US4151256A (en) * | 1977-05-12 | 1979-04-24 | Mobil Oil Corporation | Water-in-oil detection device |
| DE2828088A1 (de) * | 1978-06-27 | 1980-01-10 | Riedel De Haen Ag | Vorrichtung zur kontaminationsfreien probenahme von fluessigkeiten |
| US4272245A (en) * | 1978-12-04 | 1981-06-09 | Transidyne General Corporation | Method and apparatus for electro-chemical measurement |
| US4231752A (en) * | 1979-02-28 | 1980-11-04 | Mobil Oil Corporation | Method of determining salt water in oils |
| US4257775A (en) * | 1979-03-26 | 1981-03-24 | Mobil Oil Corporation | Determination of water content in various systems |
| US4198207A (en) * | 1979-03-26 | 1980-04-15 | Mobil Oil Corporation | Determination of water content in presence of oils |
| FR2521300A1 (fr) * | 1982-02-10 | 1983-08-12 | Primagaz Cie Gaz Petrole | Dispositif de detection de la presence de liquides aqueux susceptibles de contenir de la soude, dans du gaz de petrole liquefie |
| US4537747A (en) * | 1983-03-16 | 1985-08-27 | Chemetrics, Inc. | Disposable device for sampling and diluting |
| US4596780A (en) * | 1983-03-16 | 1986-06-24 | Chemetrics, Inc. | Process for sampling and diluting |
| US4699885A (en) * | 1983-05-02 | 1987-10-13 | Melpolder Frank W | Composition and probe for detection of water |
| US4578357A (en) * | 1983-06-27 | 1986-03-25 | Atlantic Richfield Company | Stabilized water indicating paste composition |
| US4717671A (en) * | 1983-06-27 | 1988-01-05 | Pony Industries, Inc. | Stabilized water indicating paste composition |
| US4557899A (en) * | 1984-10-15 | 1985-12-10 | Hach Company | Water-in-oil testing apparatus |
| US4668634A (en) * | 1985-09-16 | 1987-05-26 | Marquest Medical Products, Inc. | Syringe tonometric apparatus and method |
| US4929562A (en) * | 1986-08-20 | 1990-05-29 | The Regents Of The University Of California | Method and apparatus for detecting gem-polyhalogenated hydrocarbons |
| DE3709773A1 (de) * | 1987-03-25 | 1988-10-06 | Josef Dr Ing Koehler | Vorrichtung zur dosierung und mischung von kleinen stoffmengen |
| JPH0269758U (de) * | 1988-11-16 | 1990-05-28 | ||
| JPH02168158A (ja) * | 1988-12-22 | 1990-06-28 | Shigeru Nakagawa | 液体検査具 |
| US5286453A (en) * | 1992-04-02 | 1994-02-15 | Pope Carolyn M | Device for dispensing a biological fluid from a sealed vacuum tube |
| US5491345A (en) * | 1994-10-03 | 1996-02-13 | Associated Universities, Inc. | Sealed vacuum canister and method for pick-up and containment of material |
| US6376250B1 (en) | 2000-08-17 | 2002-04-23 | Nabil J. Mohtadi | Composition and probe for detection of water |
| US8409508B2 (en) | 2002-04-23 | 2013-04-02 | Biofire Diagnostics, Inc. | Sample withdrawal and dispensing device |
| US7407625B1 (en) * | 2004-04-28 | 2008-08-05 | Phase Dynamics, Inc. | Volume-differential water assay system using hydrophilic gel |
| US7354768B1 (en) * | 2004-04-28 | 2008-04-08 | Phase Dynamics, Inc. | Volume-differential assay using hydrophilic gel |
| US9945839B2 (en) | 2012-11-30 | 2018-04-17 | Rarecyte, Inc. | Apparatus, system, and method for collecting a target material |
| US9217697B2 (en) * | 2012-11-30 | 2015-12-22 | Rarecyte, Inc. | Apparatus, system, and method for collecting a target material |
| US9533303B2 (en) | 2012-11-30 | 2017-01-03 | Rarecyte, Inc. | Apparatus, system, and method for collecting a target material |
| US10054524B2 (en) | 2012-11-30 | 2018-08-21 | Rarecyte, Inc. | Apparatus, system and method for collecting a target material |
| US9039999B2 (en) | 2012-11-30 | 2015-05-26 | Rarecyte, Inc. | Apparatus, system, and method for collecting a target material |
| US9956555B2 (en) | 2012-11-30 | 2018-05-01 | Rarecyte, Inc. | Apparatus, system, and method for collecting a target material |
| US9539570B2 (en) | 2012-11-30 | 2017-01-10 | Rarecyte, Inc. | Apparatus, system, and method for collecting a target material |
| US9513291B2 (en) | 2012-11-30 | 2016-12-06 | Rarecyte, Inc. | Apparatus, system, and method for collecting a target material |
| WO2014089174A2 (en) * | 2012-12-06 | 2014-06-12 | Aerodesigns, Inc. | Aerosol dispenser with edible cartridge |
| US9557313B2 (en) * | 2013-09-28 | 2017-01-31 | Alan James Fougere | System for pre-treating a filter used in a small-scale water separometer |
| US20160243544A1 (en) * | 2013-11-14 | 2016-08-25 | Abon Biopharm (Hangzhou) Co., Ltd. | A device and method for using the device |
| US9638680B2 (en) | 2014-01-13 | 2017-05-02 | Council Of Scientific & Industrial Research | Composition for the colorimetric detection of water in hydrocarbon fuels and a process for the preparation thereof |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2429694A (en) * | 1944-03-29 | 1947-10-28 | Little Inc A | Method and equipment for indicating the water content of a gas |
| CH431139A (de) * | 1965-01-19 | 1967-02-28 | Bayer Ag | Pyrolyse- und Reaktionskammer für Gaschromatographie |
| US3505020A (en) * | 1967-05-25 | 1970-04-07 | Exxon Research Engineering Co | Method and composition for detecting free water |
| CA928181A (en) * | 1968-06-28 | 1973-06-12 | Gilford Instrument Laboratories | Fluid sampling method and apparatus |
| US3634038A (en) * | 1969-09-10 | 1972-01-11 | Gordon A Rampy | Device for the quantitative colorimetric analysis of fluids |
| JPS5014144A (de) * | 1973-06-08 | 1975-02-14 |
-
1974
- 1974-01-02 US US429973A patent/US3873271A/en not_active Expired - Lifetime
- 1974-12-19 CA CA216,433A patent/CA1053132A/en not_active Expired
- 1974-12-19 JP JP49145072A patent/JPS5819988B2/ja not_active Expired
- 1974-12-23 GB GB55376/74A patent/GB1486779A/en not_active Expired
- 1974-12-23 GB GB12058/77A patent/GB1486780A/en not_active Expired
- 1974-12-27 DE DE2461585A patent/DE2461585C2/de not_active Expired
- 1974-12-27 DE DE2463212A patent/DE2463212C2/de not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5099795A (de) | 1975-08-07 |
| US3873271A (en) | 1975-03-25 |
| DE2461585C2 (de) | 1986-01-09 |
| JPS5819988B2 (ja) | 1983-04-21 |
| DE2463212C2 (de) | 1987-05-07 |
| GB1486779A (en) | 1977-09-21 |
| DE2461585A1 (de) | 1975-07-10 |
| GB1486780A (en) | 1977-09-21 |
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