BRPI1106997A2 - composição adesiva, método para ligar dois ou mais substratos, e, conjunto ligado - Google Patents
composição adesiva, método para ligar dois ou mais substratos, e, conjunto ligadoInfo
- Publication number
- BRPI1106997A2 BRPI1106997A2 BRPI1106997A BRPI1106997A BRPI1106997A2 BR PI1106997 A2 BRPI1106997 A2 BR PI1106997A2 BR PI1106997 A BRPI1106997 A BR PI1106997A BR PI1106997 A BRPI1106997 A BR PI1106997A BR PI1106997 A2 BRPI1106997 A2 BR PI1106997A2
- Authority
- BR
- Brazil
- Prior art keywords
- substrates
- adhesive composition
- bonding
- monomeric
- bonded assembly
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/10—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step
- C08G18/12—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step using two or more compounds having active hydrogen in the first polymerisation step
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/48—Polyethers
- C08G18/4829—Polyethers containing at least three hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/65—Low-molecular-weight compounds having active hydrogen with high-molecular-weight compounds having active hydrogen
- C08G18/66—Compounds of groups C08G18/42, C08G18/48, or C08G18/52
- C08G18/6666—Compounds of group C08G18/48 or C08G18/52
- C08G18/667—Compounds of group C08G18/48 or C08G18/52 with compounds of group C08G18/32 or polyamines of C08G18/38
- C08G18/6674—Compounds of group C08G18/48 or C08G18/52 with compounds of group C08G18/32 or polyamines of C08G18/38 with compounds of group C08G18/3203
- C08G18/6677—Compounds of group C08G18/48 or C08G18/52 with compounds of group C08G18/32 or polyamines of C08G18/38 with compounds of group C08G18/3203 having at least three hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
- C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
- C08G18/7657—Polyisocyanates or polyisothiocyanates cyclic aromatic containing two or more aromatic rings
- C08G18/7664—Polyisocyanates or polyisothiocyanates cyclic aromatic containing two or more aromatic rings containing alkylene polyphenyl groups
- C08G18/7671—Polyisocyanates or polyisothiocyanates cyclic aromatic containing two or more aromatic rings containing alkylene polyphenyl groups containing only one alkylene bisphenyl group
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J175/00—Adhesives based on polyureas or polyurethanes; Adhesives based on derivatives of such polymers
- C09J175/04—Polyurethanes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/0838—Manufacture of polymers in the presence of non-reactive compounds
- C08G18/0842—Manufacture of polymers in the presence of non-reactive compounds in the presence of liquid diluents
- C08G18/0847—Manufacture of polymers in the presence of non-reactive compounds in the presence of liquid diluents in the presence of solvents for the polymers
- C08G18/0852—Manufacture of polymers in the presence of non-reactive compounds in the presence of liquid diluents in the presence of solvents for the polymers the solvents being organic
- C08G18/0857—Manufacture of polymers in the presence of non-reactive compounds in the presence of liquid diluents in the presence of solvents for the polymers the solvents being organic the solvent being a polyol
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/16—Catalysts
- C08G18/18—Catalysts containing secondary or tertiary amines or salts thereof
- C08G18/1825—Catalysts containing secondary or tertiary amines or salts thereof having hydroxy or primary amino groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/16—Catalysts
- C08G18/18—Catalysts containing secondary or tertiary amines or salts thereof
- C08G18/20—Heterocyclic amines; Salts thereof
- C08G18/2009—Heterocyclic amines; Salts thereof containing one heterocyclic ring
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/68—Polyesters containing atoms other than carbon, hydrogen and oxygen
- C08G63/685—Polyesters containing atoms other than carbon, hydrogen and oxygen containing nitrogen
- C08G63/6854—Polyesters containing atoms other than carbon, hydrogen and oxygen containing nitrogen derived from polycarboxylic acids and polyhydroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2367/00—Characterised by the use of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Derivatives of such polymers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/05—Alcohols; Metal alcoholates
- C08K5/053—Polyhydroxylic alcohols
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/10—Esters; Ether-esters
- C08K5/101—Esters; Ether-esters of monocarboxylic acids
- C08K5/103—Esters; Ether-esters of monocarboxylic acids with polyalcohols
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J175/00—Adhesives based on polyureas or polyurethanes; Adhesives based on derivatives of such polymers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2477/00—Presence of polyamide
- C09J2477/006—Presence of polyamide in the substrate
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31551—Of polyamidoester [polyurethane, polyisocyanate, polycarbamate, etc.]
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Polyurethanes Or Polyureas (AREA)
Abstract
composição adesiva, l\1étodo para ligar dois ou mais substratos, e, conjunto ligado. é provida uma composição adesiva, que compreende: (a)um componente de poliisocianato, que compreende: (i) difenil diisocianato de 4,4'-metileno monomérico, e (ii) um pré-polímero funcional de isocianato, que é o produto de reação de uma mistura de reagente de pré-polímero, que compreende: (a) difenil diisocianato de 4,4'-metileno monomérico, e (b) um ou mais polióis, em que a quantidade de difenil diisocianato de 2,2'-metileno monomérico na referida mistura de reagente de pré-polímero é de 1%, ou menos, em peso, com base no peso da referida mistura de reagente de pré- polímero; em que a quantidade de difenil diisocianato de 2,2'-metileno monomérico no referido componente de poliisocianato é de 1 %, ou menos, em peso, com base no peso do referido componente de isocianato; e, (b) um componente de poliol, que compreende um ou mais polióis. é também provido um método de ligação de dois ou mais substratos, que compreende colocar uma tal composição adesiva em contanto com ambos os referidos dois ou mais substratos. é ainda provido um conjunto ligado, que compreende dois ou mais substratos, ligados de um modo conjunto por uma tal composição adesiva.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201061425444P | 2010-12-21 | 2010-12-21 | |
US201161500919P | 2011-06-24 | 2011-06-24 |
Publications (2)
Publication Number | Publication Date |
---|---|
BRPI1106997A2 true BRPI1106997A2 (pt) | 2018-02-27 |
BRPI1106997B1 BRPI1106997B1 (pt) | 2020-04-07 |
Family
ID=45218267
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BRPI1106997A BRPI1106997B1 (pt) | 2010-12-21 | 2011-12-19 | composição adesiva, método para ligar dois ou mais substratos, e, conjunto ligado |
Country Status (5)
Country | Link |
---|---|
US (1) | US8835009B2 (pt) |
EP (1) | EP2468787A1 (pt) |
JP (1) | JP5604407B2 (pt) |
CN (1) | CN102585751B (pt) |
BR (1) | BRPI1106997B1 (pt) |
Families Citing this family (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP5642047B2 (ja) * | 2010-12-21 | 2014-12-17 | ローム アンド ハース カンパニーRohm And Haas Company | 接着剤組成物 |
JP6161866B2 (ja) * | 2010-12-21 | 2017-07-12 | ローム アンド ハース カンパニーRohm And Haas Company | 接着剤組成物 |
JP5472525B1 (ja) * | 2013-01-22 | 2014-04-16 | 東洋インキScホールディングス株式会社 | 接着剤組成物、並びに積層体およびその製造方法 |
US20170334183A1 (en) * | 2015-03-20 | 2017-11-23 | Dic Corporation | Solvent-free laminating adhesive, cured product of same, polyol composition for lamination adhesives, and multilayer film |
AU2015389306B2 (en) | 2015-03-27 | 2018-04-26 | Mitsubishi Electric Corporation | Step-up device and converter device |
JP5812219B1 (ja) | 2015-04-17 | 2015-11-11 | 東洋インキScホールディングス株式会社 | 接着剤組成物およびそれを用いた積層体 |
AU2017368512B2 (en) * | 2016-12-02 | 2019-12-19 | Dic Corporation | Reactive adhesive, multilayer film, and packaging |
CN110831993A (zh) | 2017-05-30 | 2020-02-21 | 陶氏环球技术有限责任公司 | 双组分无溶剂粘着剂组合物 |
US11732080B2 (en) | 2017-06-15 | 2023-08-22 | Ddp Specialty Electronics Materials Us, Inc. | Compositions containing hydrophobic modified isocyanate functional prepolymer containing adhesives |
CN109181620B (zh) * | 2018-08-22 | 2021-07-02 | 黎明化工研究设计院有限责任公司 | 一种可粘接时间长室温固化耐候性聚氨酯胶黏剂 |
US11981767B2 (en) | 2018-11-16 | 2024-05-14 | Dow Global Technologies Llc | Solventless adhesive composition and process for making and use in forming a laminate |
US11746266B2 (en) | 2020-10-01 | 2023-09-05 | The Dow Chemical Company | Adhesive composition |
WO2022185115A1 (en) * | 2021-03-04 | 2022-09-09 | Uflex Limited | An adhesive composition and a process for its preparation |
Family Cites Families (21)
Publication number | Priority date | Publication date | Assignee | Title |
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US4405531A (en) | 1975-11-10 | 1983-09-20 | Monsanto Company | Salts of N-phosphonomethylglycine |
DE2917314B1 (de) | 1979-04-28 | 1980-09-25 | Haeger & Kaessner Gmbh | Verfahren zur Herstellung elastischer,wetterbestaendiger Flaechengebilde |
DE3306559A1 (de) | 1983-02-25 | 1984-08-30 | Henkel KGaA, 4000 Düsseldorf | Verfahren zur herstellung von polyurethan-praepolymeren mit endstaendigen isocyanatgruppen und vermindertem restmonomergehalt |
DE3401129A1 (de) | 1984-01-14 | 1985-07-18 | Henkel KGaA, 4000 Düsseldorf | Verfahren zur herstellung gemischter polyurethan-prepolymerer |
DE4232015A1 (de) | 1992-09-24 | 1994-03-31 | Bayer Ag | Lösungsmittelfreie Zweikomponentenpolyurethanklebstoffsysteme |
JP3519135B2 (ja) * | 1994-08-30 | 2004-04-12 | 三洋化成工業株式会社 | 多孔質材の接着方法 |
DE19603330C1 (de) | 1996-01-31 | 1997-06-05 | Bayer Ag | Verfahren zur Herstellung von Holzwerkstoffen mit Polyisocyanat-Bindemitteln unter Mitverwendung von latenten, wärmeaktivierbaren Katalysatoren |
US6784242B2 (en) | 1997-11-11 | 2004-08-31 | Henkel Kommanditgesellschaft Auf Aktien | Polyurethane binding agents having a low content of highly volatile monomers |
DE59814397D1 (de) * | 1997-11-11 | 2009-11-12 | Henkel Ag & Co Kgaa | Verfahren zur Herstellung eines Polyurethanbindemittels mit einem niedrigen Gehalt an leichtflüchtigen Monomeren |
JP2002249745A (ja) | 2001-02-27 | 2002-09-06 | Mitsui Takeda Chemicals Inc | 2液硬化型無溶剤系接着剤組成物 |
US6884904B2 (en) * | 2001-04-12 | 2005-04-26 | Air Products And Chemicals, Inc. | MDI-based polyurethane prepolymer with low monomeric MDI content |
US7019102B2 (en) * | 2004-06-18 | 2006-03-28 | Henkel Kommanditgesellschaft Auf Aktien | Blocked polyurethane prepolymers useful in coating compositions |
DE102004035764A1 (de) * | 2004-07-23 | 2006-03-16 | Bayer Materialscience Ag | Niedrigviskose Polyurethan-Prepolymere auf Basis von 2,4'-MDI |
US20060078741A1 (en) | 2004-10-12 | 2006-04-13 | Ramalingam Balasubramaniam Jr | Laminating adhesives containing microencapsulated catalysts |
JP2007284520A (ja) * | 2006-04-14 | 2007-11-01 | Agc Polymer Material Co Ltd | 二液型ポリウレタン防水材組成物 |
US20100136347A1 (en) | 2006-08-07 | 2010-06-03 | Simons J Brandon Simons | Two component solventless polyurethane laminating adhesives based on 1,4:3,6 dianhydrohexitols |
DE102006059464A1 (de) | 2006-12-14 | 2008-06-19 | Henkel Kgaa | Polyurethan-Kaschierklebstoff |
JP5577013B2 (ja) * | 2007-06-06 | 2014-08-20 | 三井化学株式会社 | 無溶剤型ラミネート接着剤および複合フィルムの製造方法 |
JP4948507B2 (ja) | 2007-12-19 | 2012-06-06 | ローム アンド ハース カンパニー | ラミネート接着剤 |
EP2130641A1 (en) | 2008-06-03 | 2009-12-09 | Dow Global Technologies Inc. | Polyurethane Adhesive Composition |
JP5642047B2 (ja) * | 2010-12-21 | 2014-12-17 | ローム アンド ハース カンパニーRohm And Haas Company | 接着剤組成物 |
-
2011
- 2011-11-15 JP JP2011249202A patent/JP5604407B2/ja not_active Expired - Fee Related
- 2011-11-18 US US13/300,071 patent/US8835009B2/en not_active Expired - Fee Related
- 2011-11-21 EP EP20110189868 patent/EP2468787A1/en not_active Withdrawn
- 2011-12-19 BR BRPI1106997A patent/BRPI1106997B1/pt not_active IP Right Cessation
- 2011-12-20 CN CN201110453337.4A patent/CN102585751B/zh not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
CN102585751B (zh) | 2014-06-25 |
JP2012131980A (ja) | 2012-07-12 |
CN102585751A (zh) | 2012-07-18 |
US8835009B2 (en) | 2014-09-16 |
US20120156505A1 (en) | 2012-06-21 |
BRPI1106997B1 (pt) | 2020-04-07 |
EP2468787A1 (en) | 2012-06-27 |
JP5604407B2 (ja) | 2014-10-08 |
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