BRPI0403754A - método para controlar congelamento-concentração progressivo - Google Patents

método para controlar congelamento-concentração progressivo

Info

Publication number
BRPI0403754A
BRPI0403754A BRPI0403754-5A BRPI0403754A BRPI0403754A BR PI0403754 A BRPI0403754 A BR PI0403754A BR PI0403754 A BRPI0403754 A BR PI0403754A BR PI0403754 A BRPI0403754 A BR PI0403754A
Authority
BR
Brazil
Prior art keywords
target liquid
liquid flow
volume
flow path
growth rate
Prior art date
Application number
BRPI0403754-5A
Other languages
English (en)
Inventor
Kazuo Kagitani
Kiro Hayakawa
Original Assignee
Kagome Kk
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kagome Kk filed Critical Kagome Kk
Publication of BRPI0403754A publication Critical patent/BRPI0403754A/pt
Publication of BRPI0403754B1 publication Critical patent/BRPI0403754B1/pt

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0004—Crystallisation cooling by heat exchange
    • B01D9/0013—Crystallisation cooling by heat exchange by indirect heat exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0063—Control or regulation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/02—Crystallisation from solutions
    • B01D9/04—Crystallisation from solutions concentrating solutions by removing frozen solvent therefrom

Landscapes

  • Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Non-Alcoholic Beverages (AREA)
  • Physical Water Treatments (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
  • Control Of Non-Electrical Variables (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Sorption Type Refrigeration Machines (AREA)
  • Paper (AREA)

Abstract

"MéTODO PARA CONTROLAR CONGELAMENTO-CONCENTRAçãO PROGRESSIVO". Em um método para controlar congelamento-concentração progressivo pela circulação de meio refrigerante através de uma rota de fluxo de meio refrigerante enquanto circulando um líquido-alvo para congelamento-concentração através de uma rota de fluxo de líquido-alvo de modo a formar gradativamente cristais de gelo sobre superfícies de parede da rota de fluxo de líquido-alvo, um dispositivo de detecção de expansão de volume é usado para detectar expansão de volume do líquido-alvo e espessura dos cristais de gelo na rota de fluxo de líquido-alvo é obtido a partir da expansão de volume detectada por este dispositivo de detecção de expansão de volume. A vazão do líquido-alvo e a velocidade de crescimento da frente de gelo na rota de fluxo de líquido-alvo são controladas para se tornarem iguais, respectivamente, a um valor de vazão estabelecido e a um valor de velocidade de crescimento estabelecido, pela execução de operações de tipos específicos baseadas na espessura do cristal assim obtida, como pelo cálculo do diâmetro interno dos cristais de gelo, cálculo de um volume de fluxo requerido do líquido-alvo na rota de fluxo de líquido-alvo a partir do diâmetro interno calculado e da vazão estabelecida, e pelo ajuste do volume de circulação do líquido-alvo, de modo que o volume de fluxo medido do líquido-alvo se tome igual ao volume de fluxo requerido, e pelo cálculo da velocidade de crescimento real da frente de gelo a partir da espessura de cristal obtida e pelo ajuste de temperatura e/ou volume de circulação do meio refrigerante, de modo que a velocidade de crescimento real calculada se torne igual ao valor de velocidade de crescimento estabelecido.
BRPI0403754-5A 2003-09-08 2004-09-03 mÉtodo para controlar congelamento-concentraÇço progressivo. BRPI0403754B1 (pt)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2003314975A JP4429665B2 (ja) 2003-09-08 2003-09-08 前進凍結濃縮制御方法

Publications (2)

Publication Number Publication Date
BRPI0403754A true BRPI0403754A (pt) 2006-05-02
BRPI0403754B1 BRPI0403754B1 (pt) 2013-05-28

Family

ID=34131925

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0403754-5A BRPI0403754B1 (pt) 2003-09-08 2004-09-03 mÉtodo para controlar congelamento-concentraÇço progressivo.

Country Status (9)

Country Link
US (1) US7017367B2 (pt)
EP (1) EP1512449B1 (pt)
JP (1) JP4429665B2 (pt)
CN (1) CN100371046C (pt)
AT (1) ATE522262T1 (pt)
AU (1) AU2004205268B2 (pt)
BR (1) BRPI0403754B1 (pt)
ES (1) ES2370242T3 (pt)
PT (1) PT1512449E (pt)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PL1675484T3 (pl) * 2003-10-15 2011-09-30 Thomas Lutz Ubiór
CN100450572C (zh) * 2006-05-23 2009-01-14 青岛大学 一种界面渐进冷冻浓缩方法
JP4909145B2 (ja) * 2007-03-26 2012-04-04 カゴメ株式会社 前進凍結濃縮方法
GB2452918B (en) * 2007-09-18 2013-03-13 Scottish & Newcastle Plc Control system
CN101664214B (zh) * 2009-09-15 2012-08-22 华南理工大学 超声协同养晶的果汁冷冻浓缩方法与设备
JP6121661B2 (ja) * 2012-07-03 2017-04-26 石川県 界面前進凍結濃縮装置及び界面前進凍結濃縮法
EP3040108B1 (en) 2013-08-29 2021-02-17 Meiji Co., Ltd. Production method for concentrated product using membrane-concentration method and freeze-concentration method
CN105658293A (zh) 2013-08-29 2016-06-08 株式会社明治 采用冷冻浓缩法的浓缩制品的制造方法
CN108283824B (zh) * 2018-04-27 2023-10-20 韶关学院 含传热缓冲层的管式循环冷冻浓缩装置及其冷冻浓缩方法
CN108477441B (zh) * 2018-05-28 2024-09-13 新疆农业大学 一种连续冷冻制备浓缩果汁的装置及方法
WO2020037128A1 (en) * 2018-08-15 2020-02-20 The Regents Of The University Of Michigan Freeze concentration for urine-based fertilizer production
CN109248466A (zh) * 2018-11-13 2019-01-22 常宁市沿江锌业有限责任公司 一种真空冷却浓酸硫酸锌的方法
US11897822B2 (en) 2019-11-07 2024-02-13 The Regents Of The University Of Michigan Reciprocating freeze concentration for urine-based fertilizer production

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3354083A (en) * 1964-02-20 1967-11-21 Dept Of Chemical Engineering Separation of fresh water from aqueous solutions
US3347058A (en) * 1966-06-21 1967-10-17 Struthers Scientific Int Corp Concentration of extracts by freezing
US3328972A (en) * 1966-08-09 1967-07-04 Struthers Scientific Int Corp Concentration of extracts by freezing
US3616653A (en) * 1967-10-04 1971-11-02 Donald F Othmer Refrigeration in cycles of freezing and melting
US4551159A (en) * 1979-04-03 1985-11-05 Vladimir Goldstein Ice making machine and method
US4291550A (en) * 1980-02-14 1981-09-29 Chicago Bridge & Iron Company Fluidized bed crystallization apparatus and method
US5035733A (en) * 1987-07-17 1991-07-30 Sunwell Engineering Company Ltd. Ice storage and distribution unit
US5139549A (en) * 1991-04-05 1992-08-18 Chicago Bridge & Iron Technical Services Company Apparatus and method for cooling using aqueous ice slurry
US5394706A (en) * 1993-05-20 1995-03-07 Waterworks International, Inc. Freeze crystallization for the removal of water from a solution of dissolved solids
DE19834781A1 (de) * 1998-08-01 2000-02-17 Integral Energietechnik Gmbh Verfahren zur Bestimmung wechselnder Eiskonzentrationen in Binäreisvolumen
WO2003006898A1 (en) * 2001-06-20 2003-01-23 3L Filters Ltd. Apparatus for producing potable water and slush from sea water or brine
JP3775737B2 (ja) * 2002-03-19 2006-05-17 カゴメ株式会社 野菜・果実ジュースの凍結濃縮方法とその装置

Also Published As

Publication number Publication date
US7017367B2 (en) 2006-03-28
JP4429665B2 (ja) 2010-03-10
EP1512449A1 (en) 2005-03-09
ATE522262T1 (de) 2011-09-15
AU2004205268A1 (en) 2005-03-24
EP1512449B1 (en) 2011-08-31
CN100371046C (zh) 2008-02-27
US20050050917A1 (en) 2005-03-10
JP2005081215A (ja) 2005-03-31
CN1593248A (zh) 2005-03-16
AU2004205268B2 (en) 2009-10-01
PT1512449E (pt) 2011-11-03
BRPI0403754B1 (pt) 2013-05-28
ES2370242T3 (es) 2011-12-13

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Legal Events

Date Code Title Description
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 03/09/2004, OBSERVADAS AS CONDICOES LEGAIS.

B21F Lapse acc. art. 78, item iv - on non-payment of the annual fees in time

Free format text: REFERENTE A 11A ANUIDADE.

B24J Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12)

Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2322 DE 07-07-2015 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013.