BR112019015540B1 - Mistura que contém 3,4-dimetilpirazol, seu processo de produção, seus usos e processo para a produção de pó, grânulos, chips, comprimidos ou extrudado de fertilizantes que contêm nitrogênio amoniacal estabilizado - Google Patents
Mistura que contém 3,4-dimetilpirazol, seu processo de produção, seus usos e processo para a produção de pó, grânulos, chips, comprimidos ou extrudado de fertilizantes que contêm nitrogênio amoniacal estabilizado Download PDFInfo
- Publication number
- BR112019015540B1 BR112019015540B1 BR112019015540-6A BR112019015540A BR112019015540B1 BR 112019015540 B1 BR112019015540 B1 BR 112019015540B1 BR 112019015540 A BR112019015540 A BR 112019015540A BR 112019015540 B1 BR112019015540 B1 BR 112019015540B1
- Authority
- BR
- Brazil
- Prior art keywords
- weight
- mixture
- fertilizer
- dimethylpyrazole
- phosphoric acid
- Prior art date
Links
- 239000003337 fertilizer Substances 0.000 title claims abstract description 111
- 239000000203 mixture Substances 0.000 title claims abstract description 88
- VQTVFIMEENGCJA-UHFFFAOYSA-N 3,4-dimethyl-1H-pyrazole Chemical compound CC=1C=NNC=1C VQTVFIMEENGCJA-UHFFFAOYSA-N 0.000 title claims abstract description 44
- XKMRRTOUMJRJIA-UHFFFAOYSA-N ammonia nh3 Chemical compound N.N XKMRRTOUMJRJIA-UHFFFAOYSA-N 0.000 title claims description 28
- 239000008187 granular material Substances 0.000 title claims description 20
- 239000000843 powder Substances 0.000 title claims description 9
- 238000000034 method Methods 0.000 title claims description 8
- 238000004519 manufacturing process Methods 0.000 title description 6
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims abstract description 92
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims abstract description 46
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 36
- 238000007792 addition Methods 0.000 claims description 19
- 239000011248 coating agent Substances 0.000 claims description 10
- 238000000576 coating method Methods 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 9
- 238000009472 formulation Methods 0.000 claims description 7
- 239000000126 substance Substances 0.000 claims description 4
- 239000003086 colorant Substances 0.000 claims description 3
- 239000007921 spray Substances 0.000 claims description 3
- 238000005470 impregnation Methods 0.000 claims description 2
- 230000000087 stabilizing effect Effects 0.000 claims 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 abstract description 2
- LXKCHCXZBPLTAE-UHFFFAOYSA-N 3,4-dimethyl-1H-pyrazole phosphate Chemical compound OP(O)(O)=O.CC1=CNN=C1C LXKCHCXZBPLTAE-UHFFFAOYSA-N 0.000 description 27
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical class N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 18
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 16
- 239000000243 solution Substances 0.000 description 16
- 239000003112 inhibitor Substances 0.000 description 15
- 150000003839 salts Chemical class 0.000 description 10
- 239000007787 solid Substances 0.000 description 10
- 229910052500 inorganic mineral Inorganic materials 0.000 description 9
- 239000011707 mineral Substances 0.000 description 9
- 229910021529 ammonia Inorganic materials 0.000 description 8
- 229910052757 nitrogen Inorganic materials 0.000 description 8
- 238000003860 storage Methods 0.000 description 7
- 238000004090 dissolution Methods 0.000 description 6
- 150000003217 pyrazoles Chemical class 0.000 description 6
- 239000004615 ingredient Substances 0.000 description 5
- 229910002651 NO3 Inorganic materials 0.000 description 4
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 4
- 239000000654 additive Substances 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- 239000000725 suspension Substances 0.000 description 4
- 239000002253 acid Substances 0.000 description 3
- 238000002425 crystallisation Methods 0.000 description 3
- 230000008025 crystallization Effects 0.000 description 3
- 230000008021 deposition Effects 0.000 description 3
- 238000010790 dilution Methods 0.000 description 3
- 239000012895 dilution Substances 0.000 description 3
- 238000009826 distribution Methods 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 2
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 230000002028 premature Effects 0.000 description 2
- -1 pyrazole compound Chemical class 0.000 description 2
- 239000002689 soil Substances 0.000 description 2
- KKEOZWYTZSNYLJ-UHFFFAOYSA-O triazanium;nitrate;sulfate Chemical compound [NH4+].[NH4+].[NH4+].[O-][N+]([O-])=O.[O-]S([O-])(=O)=O KKEOZWYTZSNYLJ-UHFFFAOYSA-O 0.000 description 2
- 238000009827 uniform distribution Methods 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 1
- 235000019484 Rapeseed oil Nutrition 0.000 description 1
- UFONUKZQWFSQLP-UHFFFAOYSA-N [N].NC#N Chemical compound [N].NC#N UFONUKZQWFSQLP-UHFFFAOYSA-N 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 239000013011 aqueous formulation Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000004202 carbamide Substances 0.000 description 1
- 235000013877 carbamide Nutrition 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000010981 drying operation Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000001863 plant nutrition Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/90—Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting the nitrification of ammonium compounds or urea in the soil
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B17/00—Other phosphatic fertilisers, e.g. soft rock phosphates, bone meal
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C1/00—Ammonium nitrate fertilisers
- C05C1/02—Granulation; Pelletisation; Stabilisation; Colouring
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
- C05G5/23—Solutions
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/30—Layered or coated, e.g. dust-preventing coatings
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/20—Reduction of greenhouse gas [GHG] emissions in agriculture, e.g. CO2
- Y02P60/21—Dinitrogen oxide [N2O], e.g. using aquaponics, hydroponics or efficiency measures
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pest Control & Pesticides (AREA)
- Soil Sciences (AREA)
- Fertilizers (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102017201608.6 | 2017-02-01 | ||
| DE102017201608.6A DE102017201608A1 (de) | 2017-02-01 | 2017-02-01 | 3,4-Dimethylpyrazol enthaltende Mischung und ihre Verwendung |
| PCT/EP2018/052200 WO2018141708A1 (de) | 2017-02-01 | 2018-01-30 | 3,4-dimethylpyrazol enthaltende mischung und ihre verwendung |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| BR112019015540A2 BR112019015540A2 (pt) | 2020-03-17 |
| BR112019015540B1 true BR112019015540B1 (pt) | 2024-01-02 |
Family
ID=61132428
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BR112019015540-6A BR112019015540B1 (pt) | 2017-02-01 | 2018-01-30 | Mistura que contém 3,4-dimetilpirazol, seu processo de produção, seus usos e processo para a produção de pó, grânulos, chips, comprimidos ou extrudado de fertilizantes que contêm nitrogênio amoniacal estabilizado |
Country Status (21)
| Country | Link |
|---|---|
| US (1) | US20190359538A1 (ko) |
| EP (1) | EP3577094B1 (ko) |
| JP (1) | JP7034168B2 (ko) |
| KR (1) | KR102542410B1 (ko) |
| CN (1) | CN110392675B (ko) |
| AR (1) | AR110793A1 (ko) |
| AU (1) | AU2018216906B2 (ko) |
| BR (1) | BR112019015540B1 (ko) |
| CA (1) | CA3050837A1 (ko) |
| CL (1) | CL2019002168A1 (ko) |
| CO (1) | CO2019008385A2 (ko) |
| DE (1) | DE102017201608A1 (ko) |
| DK (1) | DK3577094T3 (ko) |
| ES (1) | ES2879356T3 (ko) |
| MX (1) | MX2019008959A (ko) |
| MY (1) | MY193157A (ko) |
| PT (1) | PT3577094T (ko) |
| RU (1) | RU2771500C2 (ko) |
| UA (1) | UA125307C2 (ko) |
| WO (1) | WO2018141708A1 (ko) |
| ZA (1) | ZA201904957B (ko) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2019035069A1 (en) * | 2017-08-18 | 2019-02-21 | Basf Se | PROCESS FOR THE PREPARATION OF ENHANCED 3,4-DIMETHYL-1-H-PYRAZOLE PHOSPHATE FORMULATIONS |
| CN109665927B (zh) * | 2019-02-15 | 2021-11-19 | 金正大生态工程集团股份有限公司 | 一种稳定的硝化抑制剂及其制备方法与应用 |
| EP4015488A1 (en) | 2020-12-21 | 2022-06-22 | Yara International ASA | Method for producing an ammonium-based solid, particulate composition comprising an additive |
| CN113773159A (zh) * | 2021-06-28 | 2021-12-10 | 武威金仓生物科技有限公司 | 一种液体配方组合物及其应用 |
Family Cites Families (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3276510A (en) * | 1966-10-04 | Concentration op phosphoric acid | ||
| UA5668A1 (uk) * | 1990-06-06 | 1994-12-28 | Державний Науково-Дослідний І Проектний Інститут Метанолу Та Продуктів Органічного Синтезу | Спосіб стабілізації рідких комплексних добрив |
| JP3374922B2 (ja) | 1991-05-09 | 2003-02-10 | 日産化学工業株式会社 | 複素環式第３級アミンの製造方法 |
| DE4128828A1 (de) | 1991-08-30 | 1993-03-04 | Basf Ag | Ammonium- oder harnstoffhaltige duengemittel und verfahren zu ihrer herstellung |
| RU2046116C1 (ru) * | 1993-07-05 | 1995-10-20 | Государственный научно-исследовательский и проектный институт азотной промышленности и продуктов органического синтеза | Способ ингибирования нитрификации аммонийного азота удобрений в почве |
| DE19631764A1 (de) * | 1996-08-06 | 1998-02-12 | Basf Ag | Neue Nitrifikationsinhibitoren sowie die Verwendung von Polysäuren zur Behandlung von Mineraldüngemitteln die einen Nitrifikationsinhibitor enthalten |
| DE19831656A1 (de) | 1998-07-15 | 2000-01-20 | Basf Ag | Verfahren zur Herstellung von Pyrazolen |
| US6689181B2 (en) * | 2000-11-15 | 2004-02-10 | Honeywell International Inc. | Ammonium sulfate nitrate |
| DE10164103C1 (de) | 2001-12-24 | 2003-01-30 | Compo Gmbh & Co Kg | Verfahren zur Herstellung von Mineraldüngemitteln |
| CN100424051C (zh) * | 2005-06-01 | 2008-10-08 | 中国科学院沈阳应用生态研究所 | 一种缓控释含氮肥料及其制备方法 |
| CN101244964A (zh) * | 2007-02-14 | 2008-08-20 | 中国科学院沈阳应用生态研究所 | 一种生化抑制剂组合型缓释尿素及其制备方法 |
| AU2015227474A1 (en) * | 2008-03-28 | 2015-10-08 | Ballance Agri-Nutrients Limited | Particulate nitrification inhibitor systems |
| DE102009060150B4 (de) | 2009-12-23 | 2013-06-06 | K+S Aktiengesellschaft | Verfahren zur Herstellung von Säureadditionssalzen von Pyrazolen |
| CN102558054A (zh) * | 2011-12-21 | 2012-07-11 | 深圳中航资源有限公司 | 3,4-二甲基吡唑磷酸盐的制备方法 |
| CL2013002188A1 (es) * | 2013-07-30 | 2014-02-28 | Tivar Helicopteros Asesorias E Inversiones Ltda | Metodo para la elaboracion de una composicion que comprende el compuesto dimetilpirazol fosfato, para mejorar la eficiencia de la aplicacion de fertilizantes nitrogenados amoniacales o el amonio del suelo, que comprende mezclar acido fosforico con 3,5-dimetil-pirazol, agitar la mezcla, agregar agua, y aminoacidos; y dicha composicion. |
| EP3639667A1 (en) | 2013-11-26 | 2020-04-22 | Mcknight, Gary, David | Nitrification inhibitors designed for urea and manure based fertilisers |
| BR112016013578B1 (pt) * | 2013-12-13 | 2022-02-08 | Eurochem Agro Gmbh | Mistura fertilizante contendo inibidor de nitrificação e processos para sua produção e para a fertilização de solos |
| CN105315107A (zh) * | 2015-12-04 | 2016-02-10 | 魏占波 | 一种适用于酸性土壤的专用肥 |
| EP3472122B1 (en) * | 2016-06-18 | 2022-03-09 | Milliken & Company | Compositions suitable for use in making fertilizers, methods for making such compositions, and method for making fertilizers using the same |
-
2017
- 2017-02-01 DE DE102017201608.6A patent/DE102017201608A1/de active Pending
-
2018
- 2018-01-30 DK DK18702478.1T patent/DK3577094T3/da active
- 2018-01-30 CN CN201880009772.8A patent/CN110392675B/zh active Active
- 2018-01-30 MY MYPI2019004388A patent/MY193157A/en unknown
- 2018-01-30 UA UAA201909526A patent/UA125307C2/uk unknown
- 2018-01-30 MX MX2019008959A patent/MX2019008959A/es unknown
- 2018-01-30 ES ES18702478T patent/ES2879356T3/es active Active
- 2018-01-30 RU RU2019127413A patent/RU2771500C2/ru active
- 2018-01-30 US US16/481,670 patent/US20190359538A1/en active Pending
- 2018-01-30 CA CA3050837A patent/CA3050837A1/en active Pending
- 2018-01-30 JP JP2019541744A patent/JP7034168B2/ja active Active
- 2018-01-30 AU AU2018216906A patent/AU2018216906B2/en active Active
- 2018-01-30 BR BR112019015540-6A patent/BR112019015540B1/pt active IP Right Grant
- 2018-01-30 WO PCT/EP2018/052200 patent/WO2018141708A1/de active Search and Examination
- 2018-01-30 EP EP18702478.1A patent/EP3577094B1/de active Active
- 2018-01-30 KR KR1020197025502A patent/KR102542410B1/ko active IP Right Grant
- 2018-01-30 PT PT187024781T patent/PT3577094T/pt unknown
- 2018-01-31 AR ARP180100233A patent/AR110793A1/es active IP Right Grant
-
2019
- 2019-07-29 ZA ZA2019/04957A patent/ZA201904957B/en unknown
- 2019-07-31 CO CO2019008385A patent/CO2019008385A2/es unknown
- 2019-08-01 CL CL2019002168A patent/CL2019002168A1/es unknown
Also Published As
| Publication number | Publication date |
|---|---|
| RU2019127413A3 (ko) | 2021-05-27 |
| UA125307C2 (uk) | 2022-02-16 |
| RU2019127413A (ru) | 2021-03-02 |
| EP3577094B1 (de) | 2021-05-19 |
| CO2019008385A2 (es) | 2019-10-31 |
| CN110392675B (zh) | 2023-02-28 |
| KR20190113881A (ko) | 2019-10-08 |
| AU2018216906A1 (en) | 2019-08-22 |
| US20190359538A1 (en) | 2019-11-28 |
| ES2879356T3 (es) | 2021-11-22 |
| CA3050837A1 (en) | 2018-08-09 |
| CN110392675A (zh) | 2019-10-29 |
| EP3577094A1 (de) | 2019-12-11 |
| AU2018216906B2 (en) | 2022-12-01 |
| AR110793A1 (es) | 2019-05-02 |
| BR112019015540A2 (pt) | 2020-03-17 |
| DK3577094T3 (da) | 2021-07-26 |
| JP2020514228A (ja) | 2020-05-21 |
| RU2771500C2 (ru) | 2022-05-05 |
| DE102017201608A1 (de) | 2018-08-02 |
| WO2018141708A1 (de) | 2018-08-09 |
| KR102542410B1 (ko) | 2023-06-13 |
| JP7034168B2 (ja) | 2022-03-11 |
| PT3577094T (pt) | 2021-07-19 |
| MX2019008959A (es) | 2019-09-10 |
| MY193157A (en) | 2022-09-26 |
| CL2019002168A1 (es) | 2019-10-25 |
| ZA201904957B (en) | 2020-05-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B350 | Update of information on the portal [chapter 15.35 patent gazette] | ||
| B06W | Patent application suspended after preliminary examination (for patents with searches from other patent authorities) chapter 6.23 patent gazette] | ||
| B15K | Others concerning applications: alteration of classification |
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