BR112017022395A2 - método para preparação de um agente de direcionamento de estrutura, e, composição - Google Patents
método para preparação de um agente de direcionamento de estrutura, e, composiçãoInfo
- Publication number
- BR112017022395A2 BR112017022395A2 BR112017022395A BR112017022395A BR112017022395A2 BR 112017022395 A2 BR112017022395 A2 BR 112017022395A2 BR 112017022395 A BR112017022395 A BR 112017022395A BR 112017022395 A BR112017022395 A BR 112017022395A BR 112017022395 A2 BR112017022395 A2 BR 112017022395A2
- Authority
- BR
- Brazil
- Prior art keywords
- ammonium salt
- organic ammonium
- directing agent
- counterion
- preparing
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 2
- 150000003863 ammonium salts Chemical class 0.000 abstract 4
- 230000015572 biosynthetic process Effects 0.000 abstract 2
- 239000003795 chemical substances by application Substances 0.000 abstract 2
- QAOWNCQODCNURD-UHFFFAOYSA-M hydrogensulfate Chemical compound OS([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-M 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 abstract 2
- 239000002808 molecular sieve Substances 0.000 abstract 2
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 abstract 2
- 238000003786 synthesis reaction Methods 0.000 abstract 2
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 abstract 1
- 230000003301 hydrolyzing effect Effects 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 150000003242 quaternary ammonium salts Chemical class 0.000 abstract 1
- 230000008685 targeting Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B39/00—Halogenation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
- C01B39/04—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof using at least one organic template directing agent, e.g. an ionic quaternary ammonium compound or an aminated compound
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
- C01B39/30—Erionite or offretite type, e.g. zeolite T
- C01B39/305—Erionite or offretite type, e.g. zeolite T using at least one organic template directing agent
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/04—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups
- C07C209/14—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups
- C07C209/20—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups with formation of quaternary ammonium compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D211/00—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings
- C07D211/04—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D211/06—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having no double bonds between ring members or between ring members and non-ring members
- C07D211/08—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having no double bonds between ring members or between ring members and non-ring members with hydrocarbon or substituted hydrocarbon radicals directly attached to ring carbon atoms
- C07D211/10—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having no double bonds between ring members or between ring members and non-ring members with hydrocarbon or substituted hydrocarbon radicals directly attached to ring carbon atoms with radicals containing only carbon and hydrogen atoms attached to ring carbon atoms
- C07D211/14—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having no double bonds between ring members or between ring members and non-ring members with hydrocarbon or substituted hydrocarbon radicals directly attached to ring carbon atoms with radicals containing only carbon and hydrogen atoms attached to ring carbon atoms with hydrocarbon or substituted hydrocarbon radicals attached to the ring nitrogen atom
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
- C07D295/02—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements
- C07D295/037—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements with quaternary ring nitrogen atoms
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
- C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
- C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Catalysts (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
- Hydrogenated Pyridines (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
Abstract
é provido um método para preparação de um agente de direcionamento de estrutura (das) para síntese de peneira molecular cristalina compreendendo as etapas de (a) hidrolisar contraíon de sulfato de analquila de um sal quaternário de amônia para produzir um sal orgânico de amônia tendo um contraíon de sulfato de hidrogênio; e (b) colocar o sal orgânico de amônia tendo o contraíon de sulfato de hidrogênio em contato com uma fonte de hidróxido em solução para formar um sal orgânico de amônia tendo um contraíon de hidróxido, em que o sal orgânico de amônia é um agente de direcionamento de estrutura (sda) para síntese de peneira molecular cristalina.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201562150015P | 2015-04-20 | 2015-04-20 | |
PCT/US2016/028326 WO2016172128A1 (en) | 2015-04-20 | 2016-04-20 | Method for preparing structured directing agent |
Publications (1)
Publication Number | Publication Date |
---|---|
BR112017022395A2 true BR112017022395A2 (pt) | 2018-07-10 |
Family
ID=56015084
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR112017022395A BR112017022395A2 (pt) | 2015-04-20 | 2016-04-20 | método para preparação de um agente de direcionamento de estrutura, e, composição |
Country Status (10)
Country | Link |
---|---|
US (2) | US20180016231A9 (pt) |
EP (1) | EP3286163A1 (pt) |
JP (1) | JP7304133B2 (pt) |
KR (1) | KR20170140281A (pt) |
CN (2) | CN116574050A (pt) |
BR (1) | BR112017022395A2 (pt) |
DE (1) | DE102016107257A1 (pt) |
GB (1) | GB2542876B (pt) |
RU (1) | RU2764578C2 (pt) |
WO (1) | WO2016172128A1 (pt) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107285334B (zh) * | 2017-07-26 | 2019-05-10 | 中触媒新材料股份有限公司 | 一种固相合成aei型分子筛的方法及催化剂 |
KR102610289B1 (ko) * | 2017-10-27 | 2023-12-05 | 셰브런 유.에스.에이.인크. | 분자체 ssz-112, 이의 합성 및 용도 |
WO2020193987A1 (en) * | 2019-03-28 | 2020-10-01 | Johnson Matthey Public Limited Company | Molecular sieve intergrowths of cha and aft having an "sfw-gme tail", methods of preparation and use |
CN111960433A (zh) * | 2020-08-10 | 2020-11-20 | 中触媒新材料股份有限公司 | 用含双环状基团季铵鎓模板剂合成的cha型分子筛及催化剂制备与应用 |
WO2024073458A1 (en) * | 2022-09-29 | 2024-04-04 | Basf Corporation | Methods for preparing molecular sieves using 1,1-diethyl-2,6-dimethylpiperidin-1-ium and molecular sieves prepared therefrom |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1297955A (pt) * | 1969-05-19 | 1972-11-29 | ||
US5645812A (en) * | 1993-10-01 | 1997-07-08 | Chevron U.S.A. Inc. | Zeolite ZSM-11 and a process for preparing zeolite ZSM-11 using a 3,5-dimethylpiperidinium templating agent |
US5958370A (en) * | 1997-12-11 | 1999-09-28 | Chevron U.S.A. Inc. | Zeolite SSZ-39 |
CN1228310C (zh) * | 2003-07-04 | 2005-11-23 | 兰溪市钱塘合成新材料有限公司 | 一种制备氢氧化四烷基铵的方法 |
JP2005047836A (ja) * | 2003-07-30 | 2005-02-24 | Koei Chem Co Ltd | 1−アルキル−3−ピペリジンエステル類の製造方法 |
DE102004010662A1 (de) * | 2004-03-04 | 2005-09-22 | Basf Ag | Verfahren zur Herstellung von Verbindungen mit quaternären sp2-hybridisierten Stickstoffatomen |
BRPI0511500A (pt) * | 2004-05-28 | 2008-01-08 | Basf Ag | processo para a preparação de um composto de amÈnio quaternário, uso de uma solução de hidróxido de tetrametilamÈnio de alta pureza, e solução aquosa de hidróxido de tetrametilamÈnio de alta pureza |
CN1960964A (zh) * | 2004-05-28 | 2007-05-09 | 巴斯福股份公司 | 制备季铵化合物的方法 |
US20080033209A1 (en) * | 2004-08-24 | 2008-02-07 | Basf Aktiengsellschaft | Method For High-Purity Quaternary Ammonium Compounds |
ITMI20061231A1 (it) * | 2006-06-26 | 2007-12-27 | Eni Spa | Proxcesso e materiali zeolitici per la separazione di gas |
MY163927A (en) * | 2010-06-16 | 2017-11-15 | Takeda Pharmaceuticals Co | Crystal of amide compound |
KR102256341B1 (ko) * | 2013-03-27 | 2021-05-27 | 존슨 맛쎄이 퍼블릭 리미티드 컴파니 | 1-아다만틸트리메틸암모늄 수산화물의 제조 방법 |
KR102299906B1 (ko) * | 2013-08-28 | 2021-09-09 | 존슨 맛쎄이 퍼블릭 리미티드 컴파니 | 주형제의 제조방법 |
-
2016
- 2016-04-18 GB GB1606735.7A patent/GB2542876B/en active Active
- 2016-04-20 RU RU2017140039A patent/RU2764578C2/ru active
- 2016-04-20 EP EP16723567.0A patent/EP3286163A1/en active Pending
- 2016-04-20 KR KR1020177033049A patent/KR20170140281A/ko not_active Application Discontinuation
- 2016-04-20 JP JP2017554464A patent/JP7304133B2/ja active Active
- 2016-04-20 CN CN202310745603.3A patent/CN116574050A/zh active Pending
- 2016-04-20 WO PCT/US2016/028326 patent/WO2016172128A1/en active Application Filing
- 2016-04-20 DE DE102016107257.5A patent/DE102016107257A1/de active Pending
- 2016-04-20 US US15/133,811 patent/US20180016231A9/en not_active Abandoned
- 2016-04-20 BR BR112017022395A patent/BR112017022395A2/pt not_active Application Discontinuation
- 2016-04-20 CN CN201680022966.2A patent/CN107531629A/zh active Pending
-
2018
- 2018-05-01 US US15/967,859 patent/US20180244618A1/en not_active Abandoned
Also Published As
Publication number | Publication date |
---|---|
US20160304457A1 (en) | 2016-10-20 |
CN116574050A (zh) | 2023-08-11 |
WO2016172128A1 (en) | 2016-10-27 |
RU2764578C2 (ru) | 2022-01-18 |
RU2017140039A (ru) | 2019-05-20 |
EP3286163A1 (en) | 2018-02-28 |
GB2542876B (en) | 2019-10-23 |
JP2018513095A (ja) | 2018-05-24 |
RU2017140039A3 (pt) | 2019-10-01 |
GB2542876A (en) | 2017-04-05 |
CN107531629A (zh) | 2018-01-02 |
KR20170140281A (ko) | 2017-12-20 |
DE102016107257A1 (de) | 2016-10-20 |
US20180244618A1 (en) | 2018-08-30 |
JP7304133B2 (ja) | 2023-07-06 |
US20180016231A9 (en) | 2018-01-18 |
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Legal Events
Date | Code | Title | Description |
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B06U | Preliminary requirement: requests with searches performed by other patent offices: procedure suspended [chapter 6.21 patent gazette] | ||
B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
B09B | Patent application refused [chapter 9.2 patent gazette] | ||
B12B | Appeal against refusal [chapter 12.2 patent gazette] |