BR112017000120B1 - kit de partes estável para o armazenamento para fornecer uma composição dental - Google Patents

Info

Publication number

BR112017000120B1

BR112017000120B1 BR112017000120-9A BR112017000120A BR112017000120B1 BR 112017000120 B1 BR112017000120 B1 BR 112017000120B1 BR 112017000120 A BR112017000120 A BR 112017000120A BR 112017000120 B1 BR112017000120 B1 BR 112017000120B1

Authority

BR

Brazil

Prior art keywords

weight

composition

acid

kit

component

Prior art date

2014-07-10

Links

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• Global Dossier
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• 239000000203 mixture Substances 0.000 title claims abstract description 244
• 238000003860 storage Methods 0.000 title claims description 14
• -1 iron ion Chemical class 0.000 claims abstract description 73
• CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims abstract description 68
• 239000011668 ascorbic acid Substances 0.000 claims abstract description 35
• 229960005070 ascorbic acid Drugs 0.000 claims abstract description 35
• 235000010323 ascorbic acid Nutrition 0.000 claims abstract description 34
• 150000001451 organic peroxides Chemical class 0.000 claims abstract description 27
• 239000000945 filler Substances 0.000 claims abstract description 26
• 229910052723 transition metal Inorganic materials 0.000 claims abstract description 25
• 150000003624 transition metals Chemical class 0.000 claims abstract description 25
• 150000003839 salts Chemical class 0.000 claims abstract description 22
• 229910052802 copper Inorganic materials 0.000 claims abstract description 21
• 239000010949 copper Substances 0.000 claims abstract description 21
• RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims abstract description 18
• 229910052742 iron Inorganic materials 0.000 claims abstract description 10
• MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims abstract description 9
• 230000002378 acidificating effect Effects 0.000 claims description 45
• 125000000217 alkyl group Chemical group 0.000 claims description 19
• 239000007788 liquid Substances 0.000 claims description 17
• UMGDCJDMYOKAJW-UHFFFAOYSA-N thiourea Chemical compound NC(N)=S UMGDCJDMYOKAJW-UHFFFAOYSA-N 0.000 claims description 12
• 125000003118 aryl group Chemical group 0.000 claims description 11
• 239000000843 powder Substances 0.000 claims description 11
• XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Natural products NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 9
• 150000002148 esters Chemical class 0.000 claims description 7
• 125000002877 alkyl aryl group Chemical group 0.000 claims description 6
• HNYOPLTXPVRDBG-UHFFFAOYSA-N barbituric acid Chemical compound O=C1CC(=O)NC(=O)N1 HNYOPLTXPVRDBG-UHFFFAOYSA-N 0.000 claims description 6
• DOUHZFSGSXMPIE-UHFFFAOYSA-N hydroxidooxidosulfur(.) Chemical compound [O]SO DOUHZFSGSXMPIE-UHFFFAOYSA-N 0.000 claims description 6
• RVBUGGBMJDPOST-UHFFFAOYSA-N 2-thiobarbituric acid Chemical compound O=C1CC(=O)NC(=S)N1 RVBUGGBMJDPOST-UHFFFAOYSA-N 0.000 claims description 5
• 125000000753 cycloalkyl group Chemical group 0.000 claims description 5
• YEOCHZFPBYUXMC-UHFFFAOYSA-L copper benzoate Chemical compound [Cu+2].[O-]C(=O)C1=CC=CC=C1.[O-]C(=O)C1=CC=CC=C1 YEOCHZFPBYUXMC-UHFFFAOYSA-L 0.000 claims description 4
• 229910052725 zinc Inorganic materials 0.000 claims description 4
• 150000001879 copper Chemical class 0.000 claims description 3
• OPQARKPSCNTWTJ-UHFFFAOYSA-L copper(ii) acetate Chemical compound [Cu+2].CC([O-])=O.CC([O-])=O OPQARKPSCNTWTJ-UHFFFAOYSA-L 0.000 claims description 3
• 229910052804 chromium Inorganic materials 0.000 claims description 2
• 229940120693 copper naphthenate Drugs 0.000 claims description 2
• ORTQZVOHEJQUHG-UHFFFAOYSA-L copper(II) chloride Chemical compound Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 claims description 2
• SEVNKWFHTNVOLD-UHFFFAOYSA-L copper;3-(4-ethylcyclohexyl)propanoate;3-(3-ethylcyclopentyl)propanoate Chemical compound [Cu+2].CCC1CCC(CCC([O-])=O)C1.CCC1CCC(CCC([O-])=O)CC1 SEVNKWFHTNVOLD-UHFFFAOYSA-L 0.000 claims description 2
• 229910052759 nickel Inorganic materials 0.000 claims description 2
• 229910052719 titanium Inorganic materials 0.000 claims description 2
• 229910052720 vanadium Inorganic materials 0.000 claims description 2
• WFVZAFMKEMBBOU-UHFFFAOYSA-N copper;1-phenylpentane-1,3-dione Chemical compound [Cu].CCC(=O)CC(=O)C1=CC=CC=C1.CCC(=O)CC(=O)C1=CC=CC=C1 WFVZAFMKEMBBOU-UHFFFAOYSA-N 0.000 claims 1
• 229910052748 manganese Inorganic materials 0.000 claims 1
• 239000000853 adhesive Substances 0.000 abstract description 49
• 239000002253 acid Substances 0.000 abstract description 44
• 239000012966 redox initiator Substances 0.000 abstract description 16
• XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract description 12
• 238000004519 manufacturing process Methods 0.000 abstract 1
• NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 36
• 230000001070 adhesive effect Effects 0.000 description 30
• 150000001875 compounds Chemical class 0.000 description 29
• 239000006072 paste Substances 0.000 description 25
• VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 22
• 239000003999 initiator Substances 0.000 description 21
• 239000000463 material Substances 0.000 description 21
• 239000002245 particle Substances 0.000 description 21
• 239000000126 substance Substances 0.000 description 21
• 238000002156 mixing Methods 0.000 description 19
• 239000000178 monomer Substances 0.000 description 18
• 239000003795 chemical substances by application Substances 0.000 description 17
• 239000005548 dental material Substances 0.000 description 16
• 238000000034 method Methods 0.000 description 16
• 210000004268 dentin Anatomy 0.000 description 15
• 238000005530 etching Methods 0.000 description 15
• 230000005855 radiation Effects 0.000 description 14
• 239000000654 additive Substances 0.000 description 13
• 210000003298 dental enamel Anatomy 0.000 description 13
• 150000001252 acrylic acid derivatives Chemical class 0.000 description 12
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• 239000000975 dye Substances 0.000 description 12
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• 230000003750 conditioning effect Effects 0.000 description 11
• 210000001519 tissue Anatomy 0.000 description 11
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 11
• 229910001868 water Inorganic materials 0.000 description 11
• 239000003479 dental cement Substances 0.000 description 10
• 239000011347 resin Substances 0.000 description 10
• 229920005989 resin Polymers 0.000 description 10
• IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 9
• 238000006243 chemical reaction Methods 0.000 description 9
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• 238000009472 formulation Methods 0.000 description 9
• 238000006116 polymerization reaction Methods 0.000 description 9
• 239000000047 product Substances 0.000 description 9
• XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical group I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 description 8
• 230000007246 mechanism Effects 0.000 description 8
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• 238000011049 filling Methods 0.000 description 7
• 150000002978 peroxides Chemical class 0.000 description 7
• 230000008569 process Effects 0.000 description 7
• KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 6
• PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 6
• NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical group OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 6
• QTBSBXVTEAMEQO-UHFFFAOYSA-N acetic acid Substances CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
• 229910052794 bromium Inorganic materials 0.000 description 6
• 125000004432 carbon atom Chemical group C* 0.000 description 6
• 239000003054 catalyst Substances 0.000 description 6
• 229910052801 chlorine Inorganic materials 0.000 description 6
• 230000000052 comparative effect Effects 0.000 description 6
• MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 6
• 125000000524 functional group Chemical group 0.000 description 6
• 239000011521 glass Substances 0.000 description 6
• 150000002432 hydroperoxides Chemical class 0.000 description 6
• 150000002576 ketones Chemical class 0.000 description 6
• 230000001235 sensitizing effect Effects 0.000 description 6
• 239000000377 silicon dioxide Substances 0.000 description 6
• LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 5
• BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 5
• 229910003439 heavy metal oxide Inorganic materials 0.000 description 5
• 238000005259 measurement Methods 0.000 description 5
• 229910001512 metal fluoride Inorganic materials 0.000 description 5
• 229910000077 silane Inorganic materials 0.000 description 5
• 239000002904 solvent Substances 0.000 description 5
• 150000003512 tertiary amines Chemical class 0.000 description 5
• 238000012360 testing method Methods 0.000 description 5
• IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
• OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
• QSJXEFYPDANLFS-UHFFFAOYSA-N Diacetyl Chemical group CC(=O)C(C)=O QSJXEFYPDANLFS-UHFFFAOYSA-N 0.000 description 4
• RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
• JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 description 4
• 229910019142 PO4 Inorganic materials 0.000 description 4
• AMFGWXWBFGVCKG-UHFFFAOYSA-N Panavia opaque Chemical compound C1=CC(OCC(O)COC(=O)C(=C)C)=CC=C1C(C)(C)C1=CC=C(OCC(O)COC(=O)C(C)=C)C=C1 AMFGWXWBFGVCKG-UHFFFAOYSA-N 0.000 description 4
• 241000183024 Populus tremula Species 0.000 description 4
• WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 4
• MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 4
• 125000003545 alkoxy group Chemical group 0.000 description 4
• 235000019400 benzoyl peroxide Nutrition 0.000 description 4
• 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 description 4
• 239000007767 bonding agent Substances 0.000 description 4
• 229930006711 bornane-2,3-dione Natural products 0.000 description 4
• 150000001732 carboxylic acid derivatives Chemical group 0.000 description 4
• 125000004122 cyclic group Chemical group 0.000 description 4
• 239000011350 dental composite resin Substances 0.000 description 4
• 229910052731 fluorine Inorganic materials 0.000 description 4
• 150000002222 fluorine compounds Chemical class 0.000 description 4
• 150000004820 halides Chemical class 0.000 description 4
• 239000004615 ingredient Substances 0.000 description 4
• 229910052751 metal Inorganic materials 0.000 description 4
• 239000002184 metal Substances 0.000 description 4
• 239000007800 oxidant agent Substances 0.000 description 4
• 229910052760 oxygen Inorganic materials 0.000 description 4
• 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 4
• NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 4
• 239000010452 phosphate Substances 0.000 description 4
• 230000000704 physical effect Effects 0.000 description 4
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• 230000002829 reductive effect Effects 0.000 description 4
• 239000012756 surface treatment agent Substances 0.000 description 4
• VNQXSTWCDUXYEZ-UHFFFAOYSA-N 1,7,7-trimethylbicyclo[2.2.1]heptane-2,3-dione Chemical compound C1CC2(C)C(=O)C(=O)C1C2(C)C VNQXSTWCDUXYEZ-UHFFFAOYSA-N 0.000 description 3
• CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 3
• OMPJBNCRMGITSC-UHFFFAOYSA-N Benzoylperoxide Chemical compound C=1C=CC=CC=1C(=O)OOC(=O)C1=CC=CC=C1 OMPJBNCRMGITSC-UHFFFAOYSA-N 0.000 description 3
• 239000004322 Butylated hydroxytoluene Substances 0.000 description 3
• NLZUEZXRPGMBCV-UHFFFAOYSA-N Butylhydroxytoluene Chemical compound CC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 NLZUEZXRPGMBCV-UHFFFAOYSA-N 0.000 description 3
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
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• 238000003917 TEM image Methods 0.000 description 3
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• BTLXPCBPYBNQNR-UHFFFAOYSA-N 1-hydroxyanthraquinone Chemical compound O=C1C2=CC=CC=C2C(=O)C2=C1C=CC=C2O BTLXPCBPYBNQNR-UHFFFAOYSA-N 0.000 description 2
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• NTMDDSQESSRCTM-UHFFFAOYSA-N 10-phosphonooxydecyl prop-2-enoate Chemical compound OP(O)(=O)OCCCCCCCCCCOC(=O)C=C NTMDDSQESSRCTM-UHFFFAOYSA-N 0.000 description 2
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• IBDVWXAVKPRHCU-UHFFFAOYSA-N 2-(2-methylprop-2-enoyloxy)ethyl 3-oxobutanoate Chemical compound CC(=O)CC(=O)OCCOC(=O)C(C)=C IBDVWXAVKPRHCU-UHFFFAOYSA-N 0.000 description 2
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• UEKHZPDUBLCUHN-UHFFFAOYSA-N 2-[[3,5,5-trimethyl-6-[2-(2-methylprop-2-enoyloxy)ethoxycarbonylamino]hexyl]carbamoyloxy]ethyl 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OCCOC(=O)NCCC(C)CC(C)(C)CNC(=O)OCCOC(=O)C(C)=C UEKHZPDUBLCUHN-UHFFFAOYSA-N 0.000 description 2
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