BR112013022304A2 - processo para a recuperação contínua de ácido (met) acrílico e aparelho para o processo - Google Patents

processo para a recuperação contínua de ácido (met) acrílico e aparelho para o processo

Info

Publication number
BR112013022304A2
BR112013022304A2 BR112013022304A BR112013022304A BR112013022304A2 BR 112013022304 A2 BR112013022304 A2 BR 112013022304A2 BR 112013022304 A BR112013022304 A BR 112013022304A BR 112013022304 A BR112013022304 A BR 112013022304A BR 112013022304 A2 BR112013022304 A2 BR 112013022304A2
Authority
BR
Brazil
Prior art keywords
meth
acrylic acid
mixed gas
recovery
continuous
Prior art date
Application number
BR112013022304A
Other languages
English (en)
Other versions
BR112013022304B1 (pt
Inventor
Dong-Hyun Cho
Hyun-Kyu Kim
Jun-Seok Ko
Se-Won Baek
Original Assignee
Lg Chemical Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Lg Chemical Ltd filed Critical Lg Chemical Ltd
Publication of BR112013022304A2 publication Critical patent/BR112013022304A2/pt
Publication of BR112013022304B1 publication Critical patent/BR112013022304B1/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J15/00—Chemical processes in general for reacting gaseous media with non-particulate solids, e.g. sheet material; Apparatus specially adapted therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C57/00—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
    • C07C57/02—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
    • C07C57/03—Monocarboxylic acids
    • C07C57/04—Acrylic acid; Methacrylic acid

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

processo para a recuperação contínua de ácido (met) acrílico e aparelho para o processo a presente invenção refere-se a um método e aparelho para a recuperação contínua de ácido (met)acrílico, e masi especificamente a um método de recuperação contínua de ácido (met)acrílico, incluindo: conduzir a oxidação em fase gasosa de pelo menos um composto selecionado a partir do grupo que consiste em propano, propileno, butano, ibutileno, t-butileno, e (met)acroleína, na presença de um catalisador, para obter um gás misto contendo ácido (met)acrílico; resfriar subitamente o gás misto contendo ácido (met)acrílico para remover os subprodutos de alto ponto de ebulição no gás misto contendo ácido (met)acrílico; contatar o gás misto contendo ácido (met)acrílico sem subprodutos de alto ponto de ebulição com a água ou uma solução aquosa para obter uma solução aquosa contendo ácido (met)acrílico; e purificar a solução aquosa contendo ácido (met)acrílico para obter o ácido (met)acrílico. ométodo de recuperação contínua de ácido (met)acrílico de acordo com a presente invenção pode reduzir significativamente o consumo de energia e recuperar continuamente o ácido (met)acrílico de alta pureza com excelente eficiência de produção, comparado aos métodos de recuperação anteriores.
BR112013022304A 2011-03-11 2012-03-12 método de recuperação contínua de ácido (met)acrílico BR112013022304B1 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR20110021818 2011-03-11
PCT/KR2012/001784 WO2012124956A2 (ko) 2011-03-11 2012-03-12 (메트)아크릴산의 연속 회수 방법 및 회수 장치

Publications (2)

Publication Number Publication Date
BR112013022304A2 true BR112013022304A2 (pt) 2016-12-06
BR112013022304B1 BR112013022304B1 (pt) 2020-01-28

Family

ID=46831192

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112013022304A BR112013022304B1 (pt) 2011-03-11 2012-03-12 método de recuperação contínua de ácido (met)acrílico

Country Status (6)

Country Link
US (2) US8716525B2 (pt)
JP (1) JP5765863B2 (pt)
KR (1) KR101535496B1 (pt)
CN (1) CN103391914B (pt)
BR (1) BR112013022304B1 (pt)
WO (1) WO2012124956A2 (pt)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103193618B (zh) * 2013-03-20 2015-11-25 中国石油集团东北炼化工程有限公司吉林设计院 丙烷一步法制丙烯酸生产中的丙烯酸洗涤改进工艺
CN103193617B (zh) * 2013-03-25 2016-08-10 中国石油集团东北炼化工程有限公司吉林设计院 丙烷一步法制丙烯酸生产中的尾气循环工艺
US10093551B2 (en) * 2014-09-23 2018-10-09 Basf Se Process and plant for treatment of secondary components obtained in acrolein and/or (meth)acrylic acid production
KR102079775B1 (ko) 2016-11-25 2020-02-20 주식회사 엘지화학 (메트)아크릴산의 연속 회수 방법 및 장치
KR102319305B1 (ko) * 2016-12-06 2021-10-28 주식회사 엘지화학 (메트)아크릴산의 회수 방법 및 장치
WO2024049101A1 (ko) * 2022-08-30 2024-03-07 주식회사 엘지화학 고순도 (메트)아크릴산의 제조방법

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4260821A (en) * 1979-03-15 1981-04-07 Halcon Research And Development Corp. Minimizing polymerization during recovery of methacrylic acid
JPS58126831A (ja) * 1982-01-22 1983-07-28 Nippon Shokubai Kagaku Kogyo Co Ltd メタクリル酸の捕集方法
JP2504777B2 (ja) * 1987-06-27 1996-06-05 三井東圧化学株式会社 反応ガスの急冷方法
DE19627850A1 (de) * 1996-07-10 1998-01-15 Basf Ag Verfahren zur Herstellung von Acrylsäure und Methacrylsäure
DE19631645A1 (de) * 1996-08-05 1998-02-12 Basf Ag Verfahren zur Herstellung von Acrylsäure
DE19838817A1 (de) * 1998-08-26 2000-03-02 Basf Ag Verfahren zur kontinuierlichen Gewinnung von (Meth)acrylsäure
DE60005870T2 (de) * 1999-03-05 2004-08-19 Rohm And Haas Co. Verfahren zur Herstellung von Acrylsäure
BR0008823B1 (pt) * 1999-03-06 2010-11-03 processo para a preparação de ácido acrìlico.
MY122671A (en) 1999-03-06 2006-04-29 Basf Ag Fractional condensation of a product gas mixture containing acrylic acid
US6737546B2 (en) * 2001-11-13 2004-05-18 Lurgi Ag Extraction process for recovery of acrylic acid
MY135762A (en) 2002-01-09 2008-06-30 Basf Ag Method for producing acrylic acid
JP4658104B2 (ja) * 2003-06-05 2011-03-23 株式会社日本触媒 アクリル酸の製造方法
US7183428B2 (en) * 2003-06-05 2007-02-27 Nippon Shokubai Co., Inc. Method for production of acrylic acid
KR100584677B1 (ko) * 2003-08-04 2006-05-29 주식회사 엘지화학 고효율의 아크릴산 제조 방법
KR100581766B1 (ko) * 2004-02-20 2006-05-22 주식회사 엘지화학 아크릴산의 제조 방법
JP2005336065A (ja) * 2004-05-25 2005-12-08 Mitsubishi Chemicals Corp （メタ）アクロレイン又は（メタ）アクリル酸の製造方法
JP2005336099A (ja) * 2004-05-27 2005-12-08 Asahi Kasei Chemicals Corp （メタ）アクリル酸又は／及び（メタ）アクロレインを含む反応ガスの冷却方法
DE602005021361D1 (de) * 2004-08-02 2010-07-01 Lg Chemical Ltd Verfahren zur herstellung von (meth)acrylsäure
JP5368673B2 (ja) 2006-01-20 2013-12-18 株式会社日本触媒 （メタ）アクリル酸の製造方法
MY144918A (en) * 2007-01-26 2011-11-30 Basf Se Process for preparing acrylic acid
JP5358582B2 (ja) * 2007-10-23 2013-12-04 エルジー・ケム・リミテッド （メタ）アクリル酸回収方法および（メタ）アクリル酸回収装置

Also Published As

Publication number Publication date
WO2012124956A2 (ko) 2012-09-20
CN103391914B (zh) 2016-01-20
JP2014500860A (ja) 2014-01-16
WO2012124956A3 (ko) 2012-12-27
US20140105792A1 (en) 2014-04-17
BR112013022304B1 (pt) 2020-01-28
CN103391914A (zh) 2013-11-13
US9005532B2 (en) 2015-04-14
JP5765863B2 (ja) 2015-08-19
KR101535496B1 (ko) 2015-07-09
US8716525B2 (en) 2014-05-06
KR20120103520A (ko) 2012-09-19
US20130317253A1 (en) 2013-11-28

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Legal Events

Date Code Title Description
B07A Technical examination (opinion): publication of technical examination (opinion) [chapter 7.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 12/03/2012, OBSERVADAS AS CONDICOES LEGAIS.