BR0017083A - Processo para recuperar ácido tereftálico bruto (cta) - Google Patents

Processo para recuperar ácido tereftálico bruto (cta)

Info

Publication number
BR0017083A
BR0017083A BR0017083-6A BR0017083A BR0017083A BR 0017083 A BR0017083 A BR 0017083A BR 0017083 A BR0017083 A BR 0017083A BR 0017083 A BR0017083 A BR 0017083A
Authority
BR
Brazil
Prior art keywords
solid portion
pressure
drum
paste
terephthalic acid
Prior art date
Application number
BR0017083-6A
Other languages
English (en)
Inventor
Luciano Piras
Sergio Schena
Michelle Chiarelli
Luigi Soro
Original Assignee
Inca Internat S P A
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Inca Internat S P A filed Critical Inca Internat S P A
Publication of BR0017083A publication Critical patent/BR0017083A/pt

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/47Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

"PROCESSO PARA RECUPERAR áCIDO TEREFTáLICO BRUTO (CTA)". A presente invenção refere-se a um processo para a preparação de ácido tereftálico bruto que compreende primeiro introduzir uma pasta contendo ácido tereftálico cristalizado com impurezas em um licor mão de ácido carboxílico alifático em um filtro rotativo compreendendo uma carcaça e um tambor rotativo, sendo que o tambor rotativo é submetido a um diferencial de pressão uniforme ao longo do tambor inteiro, e dentro do tambor a uma pressão aproximadamente igual à pressão atmosférica ou maior, sendo então filtrada a dita pasta; e finalmente é recolhida pelo menos alguma da porção sólida. Outros aspectos da invenção incluem adicionar continuamente a pasta original ao filtro rotativo e lavar a porção sólida com ácido carboxílico alifático adicional, água ou uma combinação de ambos. A porção sólida pode então ser transferida para um tanque de reempastamento que está à mesma pressão que a pressão no ponto onde a porção sólida foi recolhida. A presente invenção também se refere a um processo para a preparação de ácido tereftálico bruto que compreende primeiramente introduzir uma pasta contendo ácido tereftálico cristalizado com impurezas em um licor mãe de ácido carboxílico alifático em um filtro rotativo compreendendo uma carcaça e um tambor rotativo, sendo que o tambor rotativo é submetido a um diferencial de pressão uniforme ao longo do tambor inteiro, sendo a dita pasta em seguida filtrada, sendo a porção sólida lavada com água; e sendo finalmente recolhida pelo menos alguma da dita porção sólida. Outros aspectos da invenção incluem adicionar continuamente a pasta original ao filtro rotativo e lavá-la adicionalmente com o licor mãe de ácido carboxílico alifático. O interior do tambor pode estar a uma pressão menor que, maior que, ou igual à pressão atmosférica. A porção sólida pode então ser transferida para um tanque de reempastamento que esteja à mesma pressão que a pressão no ponto onde a porção sólida foi recolhida.
BR0017083-6A 2000-01-25 2000-11-30 Processo para recuperar ácido tereftálico bruto (cta) BR0017083A (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US17784200P 2000-01-25 2000-01-25
PCT/IB2000/001888 WO2001055075A2 (en) 2000-01-25 2000-11-30 Process for the recovery of crude terephthalic acid (cta)

Publications (1)

Publication Number Publication Date
BR0017083A true BR0017083A (pt) 2002-11-05

Family

ID=22650174

Family Applications (1)

Application Number Title Priority Date Filing Date
BR0017083-6A BR0017083A (pt) 2000-01-25 2000-11-30 Processo para recuperar ácido tereftálico bruto (cta)

Country Status (10)

Country Link
US (1) US20030004372A1 (pt)
EP (1) EP1409445A2 (pt)
KR (1) KR20020076266A (pt)
CN (1) CN1424996A (pt)
AU (1) AU2001217248A1 (pt)
BR (1) BR0017083A (pt)
CA (1) CA2398041A1 (pt)
MX (1) MXPA02007258A (pt)
RU (1) RU2002122766A (pt)
WO (1) WO2001055075A2 (pt)

Families Citing this family (44)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7276625B2 (en) 2002-10-15 2007-10-02 Eastman Chemical Company Process for production of a carboxylic acid/diol mixture suitable for use in polyester production
US7074954B2 (en) * 2002-12-09 2006-07-11 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
US7132566B2 (en) * 2003-09-22 2006-11-07 Eastman Chemical Company Process for the purification of a crude carboxylic acid slurry
US7161027B2 (en) 2002-12-09 2007-01-09 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
EP1569888A1 (en) * 2002-12-09 2005-09-07 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
US7193109B2 (en) 2003-03-06 2007-03-20 Eastman Chemical Company Process for production of a carboxylic acid/diol mixture suitable for use in polyester production
US7452522B2 (en) 2003-06-05 2008-11-18 Eastman Chemical Company Extraction process for removal of impurities from an oxidizer purge stream in the synthesis of carboxylic acid
US7494641B2 (en) 2003-06-05 2009-02-24 Eastman Chemical Company Extraction process for removal of impurities from an oxidizer purge stream in the synthesis of carboxylic acid
US7381386B2 (en) 2003-06-05 2008-06-03 Eastman Chemical Company Extraction process for removal of impurities from mother liquor in the synthesis of carboxylic acid
US7410632B2 (en) 2003-06-05 2008-08-12 Eastman Chemical Company Extraction process for removal of impurities from mother liquor in the synthesis of carboxylic acid
US7282151B2 (en) * 2003-06-05 2007-10-16 Eastman Chemical Company Process for removal of impurities from mother liquor in the synthesis of carboxylic acid using pressure filtration
US7351396B2 (en) 2003-06-05 2008-04-01 Eastman Chemical Company Extraction process for removal of impurities from an aqueous mixture
US20050059709A1 (en) * 2003-09-15 2005-03-17 Meythaler Jay M. Treatment of a neuropathy with rapid release aminopyridine
US7214760B2 (en) * 2004-01-15 2007-05-08 Eastman Chemical Company Process for production of a carboxylic acid/diol mixture suitable for use in polyester production
CN1264802C (zh) * 2004-07-08 2006-07-19 艾博特(厦门)设备工程有限公司 一种制备纯度达到99.98%以上的纯对苯二甲酸的方法
US7888530B2 (en) 2004-09-02 2011-02-15 Eastman Chemical Company Optimized production of aromatic dicarboxylic acids
US20070238899A9 (en) 2004-09-02 2007-10-11 Robert Lin Optimized production of aromatic dicarboxylic acids
US7615663B2 (en) * 2004-09-02 2009-11-10 Eastman Chemical Company Optimized production of aromatic dicarboxylic acids
US7959879B2 (en) 2004-09-02 2011-06-14 Grupo Petrotemex, S.A. De C.V. Optimized production of aromatic dicarboxylic acids
US7273559B2 (en) 2004-10-28 2007-09-25 Eastman Chemical Company Process for removal of impurities from an oxidizer purge stream
US7291270B2 (en) 2004-10-28 2007-11-06 Eastman Chemical Company Process for removal of impurities from an oxidizer purge stream
US7569722B2 (en) 2005-08-11 2009-08-04 Eastman Chemical Company Process for removal of benzoic acid from an oxidizer purge stream
US7402694B2 (en) 2005-08-11 2008-07-22 Eastman Chemical Company Process for removal of benzoic acid from an oxidizer purge stream
CN100522915C (zh) * 2005-12-27 2009-08-05 艾博特(厦门)设备工程有限公司 一种用来分离粗对苯二甲酸(cta)的方法
US20070179312A1 (en) * 2006-02-02 2007-08-02 O'meadhra Ruairi Seosamh Process for the purification of a crude carboxylic axid slurry
US7847121B2 (en) * 2006-03-01 2010-12-07 Eastman Chemical Company Carboxylic acid production process
US7863483B2 (en) * 2006-03-01 2011-01-04 Eastman Chemical Company Carboxylic acid production process
US7880032B2 (en) 2006-03-01 2011-02-01 Eastman Chemical Company Versatile oxidation byproduct purge process
US8697906B2 (en) * 2006-03-01 2014-04-15 Grupo Petrotemex, S.A. De C.V. Methods and apparatus for producing a low-moisture carboxylic acid wet cake
US7897808B2 (en) 2006-03-01 2011-03-01 Eastman Chemical Company Versatile oxidation byproduct purge process
US8173835B2 (en) * 2006-03-01 2012-05-08 Grupo Petrotemex, S.A. De C.V. Method and apparatus for drying carboxylic acid
US20070203359A1 (en) 2006-03-01 2007-08-30 Philip Edward Gibson Versatile oxidation byproduct purge process
US7462736B2 (en) * 2006-03-01 2008-12-09 Eastman Chemical Company Methods and apparatus for isolating carboxylic acid
US20070208199A1 (en) * 2006-03-01 2007-09-06 Kenny Randolph Parker Methods and apparatus for isolating carboxylic acid
US7863481B2 (en) 2006-03-01 2011-01-04 Eastman Chemical Company Versatile oxidation byproduct purge process
DE102006058163A1 (de) * 2006-12-09 2008-06-19 Lurgi Ag Verfahren und Anlage zur Herstellung von Roh-Terephthalsäure
US8455680B2 (en) 2008-01-15 2013-06-04 Eastman Chemical Company Carboxylic acid production process employing solvent from esterification of lignocellulosic material
US8614350B2 (en) 2008-01-15 2013-12-24 Eastman Chemical Company Carboxylic acid production process employing solvent from esterification of lignocellulosic material
GB201016049D0 (en) * 2010-09-24 2010-11-10 Davy Process Techn Ltd Process and system
RU2687433C2 (ru) * 2013-12-31 2019-05-13 Бипи Корпорейшен Норт Америка Инк. Сепарация твердого вещества от жидкости при помощи ротационного напорного фильтра без сушки
CN104860813B (zh) * 2014-04-24 2017-04-26 因温斯特技术公司 用于芳族羧酸的过滤机
EP3098215B1 (de) * 2015-05-29 2020-07-01 BOKELA Ingenieurgesellschaft für Mechanische Verfahrenstechnik mbH Verfahren und vorrichtung zum behandeln von terephtalsäure
CN109400466B (zh) * 2018-11-12 2021-05-18 天华化工机械及自动化研究设计院有限公司 一种提高粗对苯二甲酸浆料进料浓度的方法及增浓装置
CN113087081B (zh) * 2021-04-14 2022-04-26 南京依柯卡特排放技术股份有限公司 一种基于陶瓷膜技术pta精制母液回收方法

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5200557A (en) * 1991-04-12 1993-04-06 Amoco Corporation Process for preparation of crude terephthalic acid suitable for reduction to prepare purified terephthalic acid
JPH06327915A (ja) * 1993-05-24 1994-11-29 Mitsui Petrochem Ind Ltd スラリーから結晶を回収する方法及び装置

Also Published As

Publication number Publication date
CA2398041A1 (en) 2001-08-02
KR20020076266A (ko) 2002-10-09
US20030004372A1 (en) 2003-01-02
WO2001055075A3 (en) 2002-03-14
RU2002122766A (ru) 2004-01-10
EP1409445A2 (en) 2004-04-21
CN1424996A (zh) 2003-06-18
AU2001217248A1 (en) 2001-08-07
MXPA02007258A (es) 2004-07-30
WO2001055075A2 (en) 2001-08-02

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Legal Events

Date Code Title Description
B11A Dismissal acc. art.33 of ipl - examination not requested within 36 months of filing
B11Y Definitive dismissal - extension of time limit for request of examination expired [chapter 11.1.1 patent gazette]