BE587140A - - Google Patents
Info
- Publication number
- BE587140A BE587140A BE587140DA BE587140A BE 587140 A BE587140 A BE 587140A BE 587140D A BE587140D A BE 587140DA BE 587140 A BE587140 A BE 587140A
- Authority
- BE
- Belgium
- Prior art keywords
- reagent
- sodium
- metallic
- boron
- compound
- Prior art date
Links
- 239000003153 chemical reaction reagent Substances 0.000 claims description 30
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 15
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 8
- 150000001875 compounds Chemical class 0.000 claims description 8
- 239000011734 sodium Substances 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 7
- 229910052783 alkali metal Inorganic materials 0.000 claims description 6
- 150000001340 alkali metals Chemical class 0.000 claims description 6
- 229910052708 sodium Inorganic materials 0.000 claims description 6
- 229910000497 Amalgam Inorganic materials 0.000 claims description 4
- 125000000217 alkyl group Chemical group 0.000 claims description 4
- 125000004432 carbon atom Chemical group C* 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 3
- 229910000799 K alloy Inorganic materials 0.000 claims description 3
- 229910000528 Na alloy Inorganic materials 0.000 claims description 3
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 3
- 229910000573 alkali metal alloy Inorganic materials 0.000 claims description 3
- 125000003118 aryl group Chemical group 0.000 claims description 3
- UORVGPXVDQYIDP-UHFFFAOYSA-N borane Chemical compound B UORVGPXVDQYIDP-UHFFFAOYSA-N 0.000 claims description 3
- 229910052739 hydrogen Inorganic materials 0.000 claims description 3
- 239000001257 hydrogen Substances 0.000 claims description 3
- 229910052751 metal Inorganic materials 0.000 claims description 3
- 239000002184 metal Substances 0.000 claims description 3
- 239000011591 potassium Substances 0.000 claims description 3
- 229910000085 borane Inorganic materials 0.000 claims description 2
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 claims description 2
- 229910052794 bromium Inorganic materials 0.000 claims description 2
- 229910052801 chlorine Inorganic materials 0.000 claims description 2
- 239000000460 chlorine Substances 0.000 claims description 2
- 125000005843 halogen group Chemical group 0.000 claims description 2
- 239000007788 liquid Substances 0.000 claims description 2
- 239000012299 nitrogen atmosphere Substances 0.000 claims description 2
- 239000007787 solid Substances 0.000 claims description 2
- 125000001246 bromo group Chemical group Br* 0.000 claims 1
- 125000001309 chloro group Chemical group Cl* 0.000 claims 1
- 239000000047 product Substances 0.000 description 6
- 150000001412 amines Chemical class 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 229910052700 potassium Inorganic materials 0.000 description 2
- 230000035484 reaction time Effects 0.000 description 2
- JHJLBTNAGRQEKS-UHFFFAOYSA-M sodium bromide Chemical compound [Na+].[Br-] JHJLBTNAGRQEKS-UHFFFAOYSA-M 0.000 description 2
- OTALAIHBWQBQHL-UHFFFAOYSA-N 4-methyl-N-(4-methylanilino)boranylaniline Chemical compound C1(=CC=C(C=C1)NBNC1=CC=C(C=C1)C)C OTALAIHBWQBQHL-UHFFFAOYSA-N 0.000 description 1
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 1
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 1
- NSLOMGGRFATYNP-UHFFFAOYSA-N C(C(C)C)N(CC(C)C)BN(CC(C)C)CC(C)C Chemical compound C(C(C)C)N(CC(C)C)BN(CC(C)C)CC(C)C NSLOMGGRFATYNP-UHFFFAOYSA-N 0.000 description 1
- ULBRGKLBLWDYKU-UHFFFAOYSA-N C(CCCCC)N(CCCCCC)BN(CCCCCC)CCCCCC Chemical compound C(CCCCC)N(CCCCCC)BN(CCCCCC)CCCCCC ULBRGKLBLWDYKU-UHFFFAOYSA-N 0.000 description 1
- HGOQSYBROZLZBH-UHFFFAOYSA-N C1(=CC=CC2=CC=CC=C12)NBNC1=CC=CC2=CC=CC=C12 Chemical compound C1(=CC=CC2=CC=CC=C12)NBNC1=CC=CC2=CC=CC=C12 HGOQSYBROZLZBH-UHFFFAOYSA-N 0.000 description 1
- YJOSBSRFQCDEDL-UHFFFAOYSA-N C1(=CC=CC=C1)N(C1=CC=CC=C1)BN(C1=CC=CC=C1)C1=CC=CC=C1 Chemical compound C1(=CC=CC=C1)N(C1=CC=CC=C1)BN(C1=CC=CC=C1)C1=CC=CC=C1 YJOSBSRFQCDEDL-UHFFFAOYSA-N 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 description 1
- XJIYHCPFTOPMLP-UHFFFAOYSA-N N-(diethylaminoboranyl)-N-ethylethanamine Chemical compound C(C)N(CC)BN(CC)CC XJIYHCPFTOPMLP-UHFFFAOYSA-N 0.000 description 1
- 229910001508 alkali metal halide Inorganic materials 0.000 description 1
- 150000008045 alkali metal halides Chemical class 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 125000003277 amino group Chemical group 0.000 description 1
- UORVGPXVDQYIDP-BJUDXGSMSA-N borane Chemical compound [10BH3] UORVGPXVDQYIDP-BJUDXGSMSA-N 0.000 description 1
- 229910052796 boron Inorganic materials 0.000 description 1
- 150000001639 boron compounds Chemical class 0.000 description 1
- 230000005587 bubbling Effects 0.000 description 1
- ZOCHARZZJNPSEU-UHFFFAOYSA-N diboron Chemical compound B#B ZOCHARZZJNPSEU-UHFFFAOYSA-N 0.000 description 1
- 125000002147 dimethylamino group Chemical group [H]C([H])([H])N(*)C([H])([H])[H] 0.000 description 1
- YPTUAQWMBNZZRN-UHFFFAOYSA-N dimethylaminoboron Chemical compound [B]N(C)C YPTUAQWMBNZZRN-UHFFFAOYSA-N 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- 229910052740 iodine Inorganic materials 0.000 description 1
- 239000011630 iodine Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- FNQHCCZDHSHINU-UHFFFAOYSA-N n-(dimethylaminoboranyl)-n-methylmethanamine Chemical compound CN(C)BN(C)C FNQHCCZDHSHINU-UHFFFAOYSA-N 0.000 description 1
- UBDPZBLACZIAPS-UHFFFAOYSA-N n-[bromo(dimethylamino)boranyl]-n-methylmethanamine Chemical compound CN(C)B(Br)N(C)C UBDPZBLACZIAPS-UHFFFAOYSA-N 0.000 description 1
- VYAJQQLLLCSMJL-UHFFFAOYSA-N n-[chloro(dimethylamino)boranyl]-n-methylmethanamine Chemical compound CN(C)B(Cl)N(C)C VYAJQQLLLCSMJL-UHFFFAOYSA-N 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- BITYAPCSNKJESK-UHFFFAOYSA-N potassiosodium Chemical compound [Na].[K] BITYAPCSNKJESK-UHFFFAOYSA-N 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000005292 vacuum distillation Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
- C07F5/02—Boron compounds
- C07F5/022—Boron compounds without C-boron linkages
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BE587140A true BE587140A (d) |
Family
ID=191657
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BE587140D BE587140A (d) |
Country Status (1)
| Country | Link |
|---|---|
| BE (1) | BE587140A (d) |
-
0
- BE BE587140D patent/BE587140A/fr unknown
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