BE568697A - - Google Patents
Info
- Publication number
- BE568697A BE568697A BE568697DA BE568697A BE 568697 A BE568697 A BE 568697A BE 568697D A BE568697D A BE 568697DA BE 568697 A BE568697 A BE 568697A
- Authority
- BE
- Belgium
- Prior art keywords
- emi
- distillation
- water
- solvent
- petroleum ether
- Prior art date
Links
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 16
- 239000003208 petroleum Substances 0.000 claims description 9
- 239000002904 solvent Substances 0.000 claims description 6
- 238000004821 distillation Methods 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- XHFGWHUWQXTGAT-UHFFFAOYSA-N dimethylamine hydrochloride Natural products CNC(C)C XHFGWHUWQXTGAT-UHFFFAOYSA-N 0.000 claims description 3
- IQDGSYLLQPDQDV-UHFFFAOYSA-N dimethylazanium;chloride Chemical compound Cl.CNC IQDGSYLLQPDQDV-UHFFFAOYSA-N 0.000 claims description 3
- FWMUJAIKEJWSSY-UHFFFAOYSA-N sulfur dichloride Chemical compound ClSCl FWMUJAIKEJWSSY-UHFFFAOYSA-N 0.000 claims description 3
- 150000001805 chlorine compounds Chemical class 0.000 claims description 2
- 239000012230 colorless oil Substances 0.000 claims description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims 2
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims 2
- 229910052938 sodium sulfate Inorganic materials 0.000 claims 2
- 235000011152 sodium sulphate Nutrition 0.000 claims 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims 1
- 239000003096 antiparasitic agent Substances 0.000 claims 1
- 229940125687 antiparasitic agent Drugs 0.000 claims 1
- 125000004432 carbon atom Chemical group C* 0.000 claims 1
- 230000007935 neutral effect Effects 0.000 claims 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims 1
- 235000017557 sodium bicarbonate Nutrition 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 239000003921 oil Substances 0.000 description 2
- OJMIONKXNSYLSR-UHFFFAOYSA-N phosphorous acid Chemical compound OP(O)O OJMIONKXNSYLSR-UHFFFAOYSA-N 0.000 description 2
- NGNBDVOYPDDBFK-UHFFFAOYSA-N 2-[2,4-di(pentan-2-yl)phenoxy]acetyl chloride Chemical compound CCCC(C)C1=CC=C(OCC(Cl)=O)C(C(C)CCC)=C1 NGNBDVOYPDDBFK-UHFFFAOYSA-N 0.000 description 1
- 241000238631 Hexapoda Species 0.000 description 1
- 241001454295 Tetranychidae Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 230000036760 body temperature Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000005457 ice water Substances 0.000 description 1
- 230000000749 insecticidal effect Effects 0.000 description 1
- -1 ligroin Chemical compound 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- AQSJGOWTSHOLKH-UHFFFAOYSA-N phosphite(3-) Chemical class [O-]P([O-])[O-] AQSJGOWTSHOLKH-UHFFFAOYSA-N 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000009885 systemic effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/16—Esters of thiophosphoric acids or thiophosphorous acids
- C07F9/165—Esters of thiophosphoric acids
- C07F9/1658—Esters of thiopolyphosphoric acids or anhydrides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEF23316A DE1141131B (de) | 1957-06-24 | 1957-06-24 | Schaedlingsbekaempfungsmittel |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BE568697A true BE568697A (it) |
Family
ID=7090792
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BE568697D BE568697A (it) | 1957-06-24 |
Country Status (4)
| Country | Link |
|---|---|
| BE (1) | BE568697A (it) |
| CH (1) | CH377326A (it) |
| DE (1) | DE1141131B (it) |
| FR (1) | FR1198264A (it) |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE896644C (de) * | 1944-07-09 | 1953-11-12 | Bayer Ag | Verfahren zur Herstellung von Pyrothiophosphorsaeuretetraalkylestern |
| DE820001C (de) * | 1949-09-07 | 1951-11-08 | Bayer Ag | Verfahren zur Herstellung von Thiopyrophosphorsaeureestern |
| US2705694A (en) * | 1952-06-24 | 1955-04-05 | Exxon Research Engineering Co | Insecticidal compositions comprising diethyl thiophosphoric acid disulfide |
-
0
- BE BE568697D patent/BE568697A/fr unknown
-
1957
- 1957-06-24 DE DEF23316A patent/DE1141131B/de active Pending
-
1958
- 1958-06-06 CH CH6030658A patent/CH377326A/de unknown
- 1958-06-17 FR FR1198264D patent/FR1198264A/fr not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| CH377326A (de) | 1964-05-15 |
| FR1198264A (fr) | 1959-12-07 |
| DE1141131B (de) | 1962-12-13 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CA1101872A (fr) | Procede de preparation de nouveaux derives de la pyrrolidine | |
| US3250798A (en) | 2,3,4,5,6-pentachloro-benzylidene malononitrile | |
| EP0233432B1 (fr) | Composés polyfluoroalkylthio-méthyliques, leurs procédés de préparation et leurs applications comme agents tensio-actifs ou précurseurs de ces derniers | |
| BE568697A (it) | ||
| CH389318A (fr) | Utilisation de nouveaux esters phosphoriques comme pesticides | |
| US2192894A (en) | Insecticide | |
| CH624089A5 (it) | ||
| US4003940A (en) | Alkynyl phenylphenol divalent aliphatic sulfites | |
| US4576935A (en) | Dihalovinylphenyl phosphates and their use as pesticides | |
| BE563341A (it) | ||
| CH392483A (fr) | Procédé de préparation de nouveaux esters d'acides 4-halo-3-sulfamoyl-benzoïques | |
| EP0376801B1 (fr) | Acétates, thioacétates et acétamides de polyfluoroalkyle substitués, leur procédé de préparation et leurs applications | |
| US3259647A (en) | Phenylalkanoates | |
| US4377531A (en) | Method for the alkylation of phenylacetonitriles | |
| BE659396A (it) | ||
| CH651575A5 (fr) | Halogenures d'acides s-alcoyle alcoylphosphonothioiques et procede pour leur preparation. | |
| BE633233A (it) | ||
| BE644164A (it) | ||
| BE581035A (it) | ||
| BE591579A (it) | ||
| CH382723A (fr) | Procédé de préparation de composés carbonylés | |
| CH467807A (fr) | Procédé de préparation de S-(2-halogéno-1-(N-phtalimido)éthyl) phosphorothioates, à activité insecticide | |
| JPS63313766A (ja) | ２，２−ビス−（２−パーフルオロアルキルエチルチオ）−アセトアルデヒド | |
| BE710777A (it) | ||
| BE466644A (it) |