AU2011210818B2 - Methods to treat mixtures of glycosides to obtain one or more of these glycosides in more pure form - Google Patents

Methods to treat mixtures of glycosides to obtain one or more of these glycosides in more pure form Download PDF

Info

Publication number
AU2011210818B2
AU2011210818B2 AU2011210818A AU2011210818A AU2011210818B2 AU 2011210818 B2 AU2011210818 B2 AU 2011210818B2 AU 2011210818 A AU2011210818 A AU 2011210818A AU 2011210818 A AU2011210818 A AU 2011210818A AU 2011210818 B2 AU2011210818 B2 AU 2011210818B2
Authority
AU
Australia
Prior art keywords
reb
slurry
rebaudioside
glycosides
aging
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
AU2011210818A
Other languages
English (en)
Other versions
AU2011210818A1 (en
Inventor
Aron Erickson
John Joseph Hahn
Allan S. Myerson
Andrew Keith Ohmes
Troy Allen Rhonemus
Kern M. Storo
Christopher Austin Tyler
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Cargill Inc
Original Assignee
Cargill Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Cargill Inc filed Critical Cargill Inc
Publication of AU2011210818A1 publication Critical patent/AU2011210818A1/en
Application granted granted Critical
Publication of AU2011210818B2 publication Critical patent/AU2011210818B2/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/30—Artificial sweetening agents
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H15/00—Compounds containing hydrocarbon or substituted hydrocarbon radicals directly attached to hetero atoms of saccharide radicals
    • C07H15/20—Carbocyclic rings
    • C07H15/24—Condensed ring systems having three or more rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H15/00—Compounds containing hydrocarbon or substituted hydrocarbon radicals directly attached to hetero atoms of saccharide radicals
    • C07H15/20—Carbocyclic rings
    • C07H15/24—Condensed ring systems having three or more rings
    • C07H15/256—Polyterpene radicals
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
    • A23L2/52—Adding ingredients
    • A23L2/60—Sweeteners
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/30—Artificial sweetening agents
    • A23L27/33—Artificial sweetening agents containing sugars or derivatives
    • A23L27/36—Terpene glycosides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H1/00—Processes for the preparation of sugar derivatives
    • C07H1/06—Separation; Purification
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Nutrition Science (AREA)
  • Food Science & Technology (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Biochemistry (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • Saccharide Compounds (AREA)
  • Seasonings (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Processing Of Solid Wastes (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Compounds Of Unknown Constitution (AREA)
AU2011210818A 2010-01-28 2011-01-27 Methods to treat mixtures of glycosides to obtain one or more of these glycosides in more pure form Expired - Fee Related AU2011210818B2 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US29916010P 2010-01-28 2010-01-28
US61/299,160 2010-01-28
PCT/US2011/022741 WO2011094423A1 (en) 2010-01-28 2011-01-27 Methods to treat mixtures of glycosides to obtain one or more of these glycosides in more pure form

Publications (2)

Publication Number Publication Date
AU2011210818A1 AU2011210818A1 (en) 2012-08-23
AU2011210818B2 true AU2011210818B2 (en) 2014-10-30

Family

ID=44319766

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2011210818A Expired - Fee Related AU2011210818B2 (en) 2010-01-28 2011-01-27 Methods to treat mixtures of glycosides to obtain one or more of these glycosides in more pure form

Country Status (14)

Country Link
US (2) US9024012B2 (cg-RX-API-DMAC10.html)
EP (1) EP2528455A4 (cg-RX-API-DMAC10.html)
JP (1) JP2013518118A (cg-RX-API-DMAC10.html)
KR (1) KR20120117895A (cg-RX-API-DMAC10.html)
CN (2) CN102811627A (cg-RX-API-DMAC10.html)
AR (1) AR080051A1 (cg-RX-API-DMAC10.html)
AU (1) AU2011210818B2 (cg-RX-API-DMAC10.html)
BR (1) BR112012018791A2 (cg-RX-API-DMAC10.html)
CA (1) CA2788359C (cg-RX-API-DMAC10.html)
MX (1) MX337550B (cg-RX-API-DMAC10.html)
PE (1) PE20121696A1 (cg-RX-API-DMAC10.html)
PY (1) PY1102598A (cg-RX-API-DMAC10.html)
RU (1) RU2012136639A (cg-RX-API-DMAC10.html)
WO (1) WO2011094423A1 (cg-RX-API-DMAC10.html)

Families Citing this family (34)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010146463A2 (en) 2009-06-16 2010-12-23 Cpc (Tianjin) Fine Chemicals Co., Ltd. Process for rebaudioside d
WO2011094423A1 (en) * 2010-01-28 2011-08-04 Cargill, Incorporated Methods to treat mixtures of glycosides to obtain one or more of these glycosides in more pure form
US20150344512A1 (en) 2011-12-19 2015-12-03 Purecircle Usa Inc. Methods of purifying steviol glycosides and uses of the same
US9578895B2 (en) 2010-08-23 2017-02-28 Epc (Beijing) Natural Products Co., Ltd. Rebaudioside A and stevioside compositions
CN103314000B (zh) 2010-11-19 2018-07-27 嘉吉公司 使用具有大孔中性吸附树脂的吸附-脱附色谱用于富集衍生自甜叶菊的糖苷组合物中的新蛇菊苷b和/或新蛇菊苷d的方法
US9510611B2 (en) * 2010-12-13 2016-12-06 Purecircle Sdn Bhd Stevia composition to improve sweetness and flavor profile
US8962698B2 (en) 2011-01-28 2015-02-24 Tate & Lyle Ingredients Americas Llc Rebaudioside-mogroside V blends
MX341180B (es) 2011-01-28 2016-08-09 Tate & Lyle Ingredients Americas Llc Mezclas de stevia conteniendo rebaudiosido b.
PL2672840T3 (pl) 2011-02-10 2019-12-31 Purecircle Usa Kompozycja stewii
US9795156B2 (en) 2011-03-17 2017-10-24 E.P.C (Beijing) Plant Pharmaceutical Technology Co., Ltd Rebaudioside B and derivatives
PL3513663T3 (pl) * 2011-09-06 2025-09-08 Pepsico, Inc. Słodziki z rebaudiozydem d i produkty spożywcze słodzone rebaudiozydem d
CA3152828A1 (en) 2011-12-19 2013-06-27 The Coca-Cola Company Methods for purifying steviol glycosides and uses of the same
GB201217700D0 (en) 2012-08-01 2012-11-14 Tate & Lyle Ingredients Sweetener compositions containing rebaudioside B
BR112015006543A2 (pt) 2012-09-25 2017-07-04 Cargill Inc misturas de esteviosídeos
US20140171519A1 (en) 2012-12-19 2014-06-19 Indra Prakash Compositions and methods for improving rebaudioside x solubility
EP2934181B1 (en) 2012-12-19 2019-09-25 The Coca-Cola Company Compositions and methods for improving rebaudioside x solubility
EP3003058B2 (en) 2013-06-07 2023-06-28 Purecircle Usa Inc. Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier
US10905146B2 (en) 2013-07-12 2021-02-02 The Coca-Cola Company Compositions for improving rebaudioside M solubility
CN103709215B (zh) * 2013-12-31 2016-01-06 天津北洋百川生物技术有限公司 一种从甜菊糖结晶母液糖中提取莱鲍迪甙d的方法
US10264811B2 (en) 2014-05-19 2019-04-23 Epc Natural Products Co., Ltd. Stevia sweetener with improved solubility
US10357052B2 (en) 2014-06-16 2019-07-23 Sweet Green Fields USA LLC Rebaudioside A and stevioside with improved solubilities
US10485256B2 (en) 2014-06-20 2019-11-26 Sweet Green Fields International Co., Limited Stevia sweetener with improved solubility with a cyclodextrin
EP3017708B1 (en) * 2014-10-24 2018-05-02 Red Bull GmbH Sweetening composition
CA2968280A1 (en) * 2014-11-24 2016-06-02 Cargill, Incorporated Glycoside compositions
AU2016264732A1 (en) 2015-05-20 2017-11-30 Cargill, Incorporated Glycoside compositions
CN105037458B (zh) 2015-07-23 2018-12-28 诸城市浩天药业有限公司 一种甜菊糖d苷晶型a、其制备方法及其应用
US11251343B2 (en) * 2017-02-08 2022-02-15 Current Lighting Solutions, Llc LED design of lower CCT utilizing PFS phosphor
WO2019071187A1 (en) 2017-10-06 2019-04-11 Cargill, Incorporated STABILIZED GLYCOSIDE COMPOSITIONS OF STEVIOL AND USES THEREOF
CN109456371A (zh) * 2018-10-16 2019-03-12 桂林莱茵生物科技股份有限公司 一种高效甜菊糖苷混合物的制备方法
BR112021019948A2 (pt) 2019-04-06 2021-12-14 Cargill Inc Intensificador de solubilidade de glicosídeo de esteviol, solução aquosa de glicosídeo de esteviol, e, bebida não alcoólica
BR112021019811A2 (pt) 2019-04-06 2021-12-07 Cargill Inc Composição de glicosídeo de esteviol, bebida, métodos para reduzir um atributo sensorial indesejável de uma solução aquosa de glicosídeo de esteviol, para reduzir a persistência de doçura de um componente de glicosídeo de esteviol em uma composição comestível e para reduzir o amargor de um componente de glicosídeo de esteviol em uma composição comestível, e, soluções aquosa de glicosídeo de esteviol com reduzida persistência de doçura e aquosa de glicosídeo de esteviol com reduzido amargor
JP2020031640A (ja) * 2019-10-04 2020-03-05 カーギル インコーポレイテッド 配糖体混合物
US12662504B2 (en) 2019-12-27 2026-06-23 Suntory Holdings Limited High-solubility rebaudioside D complex
WO2022132971A1 (en) * 2020-12-16 2022-06-23 Corn Products Development, Inc. Method for purifying a crude composition comprising one or more steviol glycosides

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20060083838A1 (en) * 2004-10-18 2006-04-20 Sweet Aloha Farms, L.L.C. High yield method of producing pure rebaudioside A
US20070082103A1 (en) * 2005-10-11 2007-04-12 Stevian Biotechnology Corporation Sdn. Bhd Process for manufacturing a sweetner and use thereof
US20070292582A1 (en) * 2006-06-19 2007-12-20 The Coca-Cola Company Rebaudioside A Composition and Method for Purifying Rebaudioside A
WO2008091547A2 (en) * 2007-01-22 2008-07-31 Cargill, Incorporated Method of producing purified rebaudioside a compositions using solvent/antisolvent crystallization
WO2010118218A1 (en) * 2009-04-09 2010-10-14 Cargill, Incorporated Sweetener composition comprising high solubility form of rebaudioside a and method of making

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS51142570A (en) 1975-06-04 1976-12-08 Morita Kagaku Kogyo Method of imparting sweetness to food or pharmaceutical agent
JPS5262300A (en) 1975-11-13 1977-05-23 Ajinomoto Co Inc Isolation of bibaudioside-a by crystallization
JPS56121453A (en) 1980-02-27 1981-09-24 Ajinomoto Co Inc Separation of stevioside and rebaudioside a
JPS56121454A (en) 1980-02-27 1981-09-24 Ajinomoto Co Inc Separation of stevioside and rebaudioside a by crystallization
US4361697A (en) 1981-05-21 1982-11-30 F. K. Suzuki International, Inc. Extraction, separation and recovery of diterpene glycosides from Stevia rebaudiana plants
US4599403A (en) * 1985-10-07 1986-07-08 Harold Levy Method for recovery of stevioside
DE3788351D1 (de) 1987-07-21 1994-01-13 Roger H Giovanetto Verfahren zur Gewinnung von Steviosiden aus pflanzlichem Rohmaterial.
JP3111203B2 (ja) 1987-12-26 2000-11-20 中里 隆憲 ステビア新品種に属する植物
US5962678A (en) * 1996-09-13 1999-10-05 Alberta Research Council Method of extracting selected sweet glycosides from the Stevia rebaudiana plant
CN1243835A (zh) 1998-08-05 2000-02-09 黑龙江垦区海林甜菊糖有限责任公司 莱苞迪甙a提取方法
WO2006038221A1 (en) * 2004-10-04 2006-04-13 Council Of Scientific And Industrial Research Process for production of steviosides from stevia rebaudiana bertoni
US7838044B2 (en) * 2004-12-21 2010-11-23 Purecircle Sdn Bhd Extraction, separation and modification of sweet glycosides from the Stevia rebaudiana plant
CN101472487B (zh) * 2006-06-19 2013-05-01 可口可乐公司 甜菊双糖苷a组合物及其纯化方法
US8017168B2 (en) * 2006-11-02 2011-09-13 The Coca-Cola Company High-potency sweetener composition with rubisco protein, rubiscolin, rubiscolin derivatives, ace inhibitory peptides, and combinations thereof, and compositions sweetened therewith
CN101200480B (zh) * 2006-12-15 2011-03-30 成都华高药业有限公司 莱鲍迪甙a的提取方法
CN101220062A (zh) 2008-01-23 2008-07-16 石任兵 一种同时制备甜菊苷和莱鲍迪苷a的方法
WO2011094423A1 (en) * 2010-01-28 2011-08-04 Cargill, Incorporated Methods to treat mixtures of glycosides to obtain one or more of these glycosides in more pure form

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20060083838A1 (en) * 2004-10-18 2006-04-20 Sweet Aloha Farms, L.L.C. High yield method of producing pure rebaudioside A
US20070082103A1 (en) * 2005-10-11 2007-04-12 Stevian Biotechnology Corporation Sdn. Bhd Process for manufacturing a sweetner and use thereof
US20070292582A1 (en) * 2006-06-19 2007-12-20 The Coca-Cola Company Rebaudioside A Composition and Method for Purifying Rebaudioside A
WO2008091547A2 (en) * 2007-01-22 2008-07-31 Cargill, Incorporated Method of producing purified rebaudioside a compositions using solvent/antisolvent crystallization
WO2010118218A1 (en) * 2009-04-09 2010-10-14 Cargill, Incorporated Sweetener composition comprising high solubility form of rebaudioside a and method of making

Also Published As

Publication number Publication date
CA2788359A1 (en) 2011-08-04
CN106986905B (zh) 2019-07-26
WO2011094423A1 (en) 2011-08-04
JP2013518118A (ja) 2013-05-20
KR20120117895A (ko) 2012-10-24
AR080051A1 (es) 2012-03-07
US9024012B2 (en) 2015-05-05
CN106986905A (zh) 2017-07-28
MX337550B (es) 2016-03-10
PY1102598A (es) 2014-08-01
MX2012008546A (es) 2012-09-07
EP2528455A4 (en) 2013-11-27
US20120289687A1 (en) 2012-11-15
EP2528455A1 (en) 2012-12-05
CA2788359C (en) 2019-01-08
AU2011210818A1 (en) 2012-08-23
CN102811627A (zh) 2012-12-05
PE20121696A1 (es) 2012-12-16
RU2012136639A (ru) 2014-03-10
BR112012018791A2 (pt) 2015-09-01
US20160009749A1 (en) 2016-01-14

Similar Documents

Publication Publication Date Title
US9024012B2 (en) Methods to treat mixtures of glycosides to obtain one or more of these glycosides in more pure form
AU2008209573B2 (en) Method of producing purified rebaudioside A compositions using solvent/antisolvent crystallization
AU2010339459B2 (en) Rebaudioside A composition and method for purifying rebaudioside A
CN101662955B (zh) 使用溶剂/抗溶剂结晶法制备提纯的莱苞迪甙a组合物的方法
AU2007261243B2 (en) Rebaudioside a composition and method for purifying rebaudioside A
EP2160395B1 (en) Stevioside polymorphic and amorphous forms, methods for their formulation, and uses
WO2013088246A2 (en) Process for the purification of rebaudioside a and compositions thereof
CN102485736A (zh) 一种常温下从甜菊糖中提取高纯度莱鲍迪苷a的方法
US20240041080A1 (en) Method for purifying a crude composition comprising one or more steviol glycosides
CN112110962A (zh) 一种从含有甜菊糖苷的来源中分离和纯化斯替维苷的方法

Legal Events

Date Code Title Description
MK25 Application lapsed reg. 22.2i(2) - failure to pay acceptance fee