AU2001295046B2 - Process for producing and cooling titanium dioxide - Google Patents
Process for producing and cooling titanium dioxide Download PDFInfo
- Publication number
- AU2001295046B2 AU2001295046B2 AU2001295046A AU2001295046A AU2001295046B2 AU 2001295046 B2 AU2001295046 B2 AU 2001295046B2 AU 2001295046 A AU2001295046 A AU 2001295046A AU 2001295046 A AU2001295046 A AU 2001295046A AU 2001295046 B2 AU2001295046 B2 AU 2001295046B2
- Authority
- AU
- Australia
- Prior art keywords
- titanium dioxide
- vanes
- heat exchanger
- spiraling
- reaction products
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 title claims abstract description 105
- 239000004408 titanium dioxide Substances 0.000 title claims abstract description 52
- 238000000034 method Methods 0.000 title claims abstract description 24
- 238000001816 cooling Methods 0.000 title claims description 9
- 239000007795 chemical reaction product Substances 0.000 claims abstract description 38
- 238000009991 scouring Methods 0.000 claims abstract description 35
- 239000007787 solid Substances 0.000 claims abstract description 20
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 claims abstract description 11
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000001301 oxygen Substances 0.000 claims abstract description 10
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 10
- 239000000463 material Substances 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 5
- 235000002639 sodium chloride Nutrition 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 4
- 239000011780 sodium chloride Substances 0.000 claims description 4
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 3
- 229910045601 alloy Inorganic materials 0.000 claims description 2
- 239000000956 alloy Substances 0.000 claims description 2
- 238000005260 corrosion Methods 0.000 claims description 2
- 230000007797 corrosion Effects 0.000 claims description 2
- 239000011833 salt mixture Substances 0.000 claims description 2
- 239000000126 substance Substances 0.000 claims description 2
- 229910010293 ceramic material Inorganic materials 0.000 claims 1
- 238000012546 transfer Methods 0.000 description 29
- 238000012360 testing method Methods 0.000 description 26
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 8
- 239000007789 gas Substances 0.000 description 8
- 239000000049 pigment Substances 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 6
- 229910010413 TiO 2 Inorganic materials 0.000 description 5
- 239000002826 coolant Substances 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 4
- 239000004576 sand Substances 0.000 description 4
- 239000000919 ceramic Substances 0.000 description 3
- 239000000498 cooling water Substances 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 2
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 239000000377 silicon dioxide Substances 0.000 description 2
- KPZGRMZPZLOPBS-UHFFFAOYSA-N 1,3-dichloro-2,2-bis(chloromethyl)propane Chemical compound ClCC(CCl)(CCl)CCl KPZGRMZPZLOPBS-UHFFFAOYSA-N 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- 229910000599 Cr alloy Inorganic materials 0.000 description 1
- 229910000990 Ni alloy Inorganic materials 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000003466 anti-cipated effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000011651 chromium Substances 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 235000011164 potassium chloride Nutrition 0.000 description 1
- 239000001103 potassium chloride Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 1
- 229910010271 silicon carbide Inorganic materials 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/04—Oxides; Hydroxides
- C01G23/047—Titanium dioxide
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/04—Oxides; Hydroxides
- C01G23/047—Titanium dioxide
- C01G23/07—Producing by vapour phase processes, e.g. halide oxidation
- C01G23/075—Evacuation and cooling of the gaseous suspension containing the oxide; Desacidification and elimination of gases occluded in the separated oxide
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/04—Oxides; Hydroxides
- C01G23/047—Titanium dioxide
- C01G23/07—Producing by vapour phase processes, e.g. halide oxidation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Catalysts (AREA)
- Heat-Exchange Devices With Radiators And Conduit Assemblies (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US09/664,334 US6419893B1 (en) | 2000-09-18 | 2000-09-18 | Process for producing and cooling titanium dioxide |
| US09/664,334 | 2000-09-18 | ||
| PCT/US2001/042176 WO2002022504A1 (en) | 2000-09-18 | 2001-09-17 | Process for producing and cooling titanium dioxide |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| AU2001295046A1 AU2001295046A1 (en) | 2002-06-13 |
| AU2001295046B2 true AU2001295046B2 (en) | 2005-11-10 |
Family
ID=24665571
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AU2001295046A Ceased AU2001295046B2 (en) | 2000-09-18 | 2001-09-17 | Process for producing and cooling titanium dioxide |
| AU9504601A Pending AU9504601A (en) | 2000-09-18 | 2001-09-17 | Process for producing and cooling titanium dioxide |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AU9504601A Pending AU9504601A (en) | 2000-09-18 | 2001-09-17 | Process for producing and cooling titanium dioxide |
Country Status (19)
Families Citing this family (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20050201927A1 (en) * | 2004-03-12 | 2005-09-15 | Flynn Harry E. | Process for improving raw pigment grindability |
| US20050249659A1 (en) * | 2004-05-04 | 2005-11-10 | Flynn Harry E | Scour media for titanium dioxide production |
| US7708975B2 (en) * | 2004-07-20 | 2010-05-04 | E.I. Du Pont De Nemours And Company | Process for making metal oxide nanoparticles |
| CA2512313A1 (en) * | 2004-07-20 | 2006-01-20 | E.I. Dupont De Nemours And Company | Apparatus for making metal oxide nanopowder |
| MX2007006381A (es) * | 2004-11-30 | 2008-01-24 | Millennium Inorganic Chem | Proceso y dispositivo para enfriar pigmentos inorganicos. |
| US7854917B2 (en) * | 2005-09-16 | 2010-12-21 | Tronox Llc | Methods of controlling the particle size of titanium dioxide produced by the chloride process |
| US20070072783A1 (en) * | 2005-09-26 | 2007-03-29 | Tronox Llc | Scour medium for titanium dioxide production |
| US7247200B2 (en) * | 2005-11-01 | 2007-07-24 | E. I. Du Pont De Nemours And Company | Titanium dioxide finishing process |
| US20080069764A1 (en) * | 2006-09-18 | 2008-03-20 | Tronox Llc | Process for making pigmentary titanium dioxide |
| US7968077B2 (en) * | 2006-12-20 | 2011-06-28 | Kronos International, Inc. | Method for manufacturing titanium dioxide by oxidizing of titanium tetrachloride |
| DE102007048553A1 (de) * | 2006-12-20 | 2008-06-26 | Kronos International, Inc. | Verfahren zur Herstellung von Titandioxid durch Oxidation von Titantetrachlorid |
| CN102422115A (zh) * | 2009-05-08 | 2012-04-18 | 纳幕尔杜邦公司 | 在二氧化钛工艺中使用改善的烟道的方法 |
| US20130283703A1 (en) | 2012-04-27 | 2013-10-31 | Cristal Usa Inc. | TiO2 BASED SCRUBBING GRANULES, AND METHODS OF MAKING AND USING SUCH TiO2 BASED SCRUBBING GRANULES |
| KR101382544B1 (ko) * | 2012-07-13 | 2014-04-10 | 한국과학기술연구원 | 질소산화물 제거용 바나디아-티타니아 촉매 및 그 제조방법 |
| CA3079647A1 (en) * | 2017-10-27 | 2019-05-02 | China Petroleum & Chemical Corporation | Heat transfer enhancement pipe as well as cracking furnace and atmospheric and vacuum heating furnace including the same |
| CN107804870A (zh) * | 2017-11-14 | 2018-03-16 | 黄林海 | 一种二氧化钛的生产方法 |
| CN112552149B (zh) * | 2020-11-03 | 2023-03-17 | 金华永和氟化工有限公司 | 一种制备全氟烷基乙烯基醚的反应系统及其方法 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3615202A (en) * | 1969-11-28 | 1971-10-26 | David R Stern | Process for the manufacture of titanium dioxide |
| US5840112A (en) * | 1996-07-25 | 1998-11-24 | Kerr Mcgee Chemical Corporation | Method and apparatus for producing titanium dioxide |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2899278A (en) * | 1959-08-11 | lewis | ||
| US3273599A (en) | 1966-09-20 | Internally finned condenser tube | ||
| US2721626A (en) * | 1951-12-15 | 1955-10-25 | Du Pont | Cooling and separating by condensation of hot gaseous suspensions |
| US3443630A (en) | 1967-06-19 | 1969-05-13 | Du Pont | Magnesium surface for cooling tio2 |
| BE755089A (fr) * | 1969-08-20 | 1971-02-22 | Montedison Spa | Reacteur et procede pour la fabrication de dioxyde de titane dequalite pigmentaire |
| US4066424A (en) | 1976-10-13 | 1978-01-03 | E. I. Du Pont De Nemours And Company | Selectively recovering metal chlorides from gaseous effluent |
| US4462979A (en) | 1982-02-25 | 1984-07-31 | E. I. Du Pont De Nemours And Company | Process for preparing soft TiO2 agglomerates |
| US4937064A (en) | 1987-11-09 | 1990-06-26 | E. I. Du Pont De Nemours And Company | Process of using an improved flue in a titanium dioxide process |
| RU2008992C1 (ru) * | 1991-07-16 | 1994-03-15 | Цих Сергей Владимирович | Устройство для очистки внутренней поверхности трубопровода |
| US5266108A (en) | 1992-04-22 | 1993-11-30 | E. I. Du Pont De Nemours And Company | Using compacted titanium dioxide pigment particles in the cooling section of the chloride process for making TiO2 |
| US5372639A (en) | 1993-09-03 | 1994-12-13 | E. I. Du Pont De Nemours And Company | Use of a bimodal distribution of scrubs in a process for cooling a hot gaseous suspension |
| US5508015A (en) | 1994-07-15 | 1996-04-16 | E. I. Du Pont De Nemours And Company | Process for controlling agglomeration in the manufacture of TiO2 |
| US5538708A (en) | 1994-12-06 | 1996-07-23 | E. I. Du Pont De Nemours And Company | Expansion section as the inlet to the flue in a titanium dioxide process |
-
2000
- 2000-09-18 US US09/664,334 patent/US6419893B1/en not_active Expired - Lifetime
-
2001
- 2001-09-17 UA UA2003043506A patent/UA74008C2/uk unknown
- 2001-09-17 EP EP01975754A patent/EP1326804B1/en not_active Revoked
- 2001-09-17 PL PL36066001A patent/PL360660A1/xx not_active Application Discontinuation
- 2001-09-17 AU AU2001295046A patent/AU2001295046B2/en not_active Ceased
- 2001-09-17 MX MXPA03002302A patent/MXPA03002302A/es active IP Right Grant
- 2001-09-17 CN CNB018157734A patent/CN1197779C/zh not_active Expired - Fee Related
- 2001-09-17 RU RU2003110961/15A patent/RU2245303C2/ru not_active IP Right Cessation
- 2001-09-17 BR BR0113958-4A patent/BR0113958A/pt not_active IP Right Cessation
- 2001-09-17 AT AT01975754T patent/ATE496006T1/de not_active IP Right Cessation
- 2001-09-17 DE DE60143902T patent/DE60143902D1/de not_active Expired - Lifetime
- 2001-09-17 JP JP2002526705A patent/JP2004509045A/ja active Pending
- 2001-09-17 KR KR10-2003-7003567A patent/KR20030059134A/ko not_active Abandoned
- 2001-09-17 WO PCT/US2001/042176 patent/WO2002022504A1/en active IP Right Grant
- 2001-09-17 CZ CZ2003747A patent/CZ2003747A3/cs unknown
- 2001-09-17 AU AU9504601A patent/AU9504601A/xx active Pending
- 2001-09-19 TW TW090122995A patent/TW593154B/zh not_active IP Right Cessation
-
2002
- 2002-01-22 SA SA02220644A patent/SA02220644B1/ar unknown
-
2003
- 2003-02-26 ZA ZA200301574A patent/ZA200301574B/en unknown
- 2003-03-17 NO NO20031203A patent/NO20031203L/no unknown
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3615202A (en) * | 1969-11-28 | 1971-10-26 | David R Stern | Process for the manufacture of titanium dioxide |
| US5840112A (en) * | 1996-07-25 | 1998-11-24 | Kerr Mcgee Chemical Corporation | Method and apparatus for producing titanium dioxide |
| US6207131B1 (en) * | 1996-07-25 | 2001-03-27 | Kerr-Mcgee Chemical Llc | Method and apparatus for producing titanium dioxide |
Also Published As
| Publication number | Publication date |
|---|---|
| BR0113958A (pt) | 2003-07-29 |
| CN1458906A (zh) | 2003-11-26 |
| US6419893B1 (en) | 2002-07-16 |
| EP1326804A4 (en) | 2005-04-06 |
| AU9504601A (en) | 2002-03-26 |
| UA74008C2 (en) | 2005-10-17 |
| RU2245303C2 (ru) | 2005-01-27 |
| CZ2003747A3 (cs) | 2003-09-17 |
| WO2002022504A1 (en) | 2002-03-21 |
| ATE496006T1 (de) | 2011-02-15 |
| MXPA03002302A (es) | 2003-09-10 |
| KR20030059134A (ko) | 2003-07-07 |
| DE60143902D1 (de) | 2011-03-03 |
| EP1326804B1 (en) | 2011-01-19 |
| PL360660A1 (en) | 2004-09-20 |
| NO20031203D0 (no) | 2003-03-17 |
| TW593154B (en) | 2004-06-21 |
| ZA200301574B (en) | 2004-02-26 |
| NO20031203L (no) | 2003-05-16 |
| EP1326804A1 (en) | 2003-07-16 |
| SA02220644B1 (ar) | 2006-11-27 |
| JP2004509045A (ja) | 2004-03-25 |
| CN1197779C (zh) | 2005-04-20 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FGA | Letters patent sealed or granted (standard patent) | ||
| TC | Change of applicant's name (sec. 104) |
Owner name: TRONOX LLC Free format text: FORMER NAME: KERR-MCGEE CHEMICAL LLC |
|
| MK14 | Patent ceased section 143(a) (annual fees not paid) or expired |