ATE277494T1 - Instrument für mikrowellenunterstützte chemische synthese versehen mit stationärer abstimmung - Google Patents
Instrument für mikrowellenunterstützte chemische synthese versehen mit stationärer abstimmungInfo
- Publication number
- ATE277494T1 ATE277494T1 AT02705941T AT02705941T ATE277494T1 AT E277494 T1 ATE277494 T1 AT E277494T1 AT 02705941 T AT02705941 T AT 02705941T AT 02705941 T AT02705941 T AT 02705941T AT E277494 T1 ATE277494 T1 AT E277494T1
- Authority
- AT
- Austria
- Prior art keywords
- needle
- vessel
- pressure
- microwave
- assisted chemical
- Prior art date
Links
Classifications
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B6/00—Heating by electric, magnetic or electromagnetic fields
- H05B6/64—Heating using microwaves
- H05B6/80—Apparatus for specific applications
- H05B6/806—Apparatus for specific applications for laboratory use
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J19/12—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
- B01J19/122—Incoherent waves
- B01J19/126—Microwaves
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01P—WAVEGUIDES; RESONATORS, LINES, OR OTHER DEVICES OF THE WAVEGUIDE TYPE
- H01P7/00—Resonators of the waveguide type
- H01P7/06—Cavity resonators
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00054—Controlling or regulating the heat exchange system
- B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
- B01J2219/00058—Temperature measurement
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00054—Controlling or regulating the heat exchange system
- B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
- B01J2219/00058—Temperature measurement
- B01J2219/00063—Temperature measurement of the reactants
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00054—Controlling or regulating the heat exchange system
- B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
- B01J2219/00065—Pressure measurement
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00191—Control algorithm
- B01J2219/00193—Sensing a parameter
- B01J2219/00195—Sensing a parameter of the reaction system
- B01J2219/002—Sensing a parameter of the reaction system inside the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00191—Control algorithm
- B01J2219/00222—Control algorithm taking actions
- B01J2219/00227—Control algorithm taking actions modifying the operating conditions
- B01J2219/0024—Control algorithm taking actions modifying the operating conditions other than of the reactor or heat exchange system
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J2219/12—Processes employing electromagnetic waves
- B01J2219/1203—Incoherent waves
- B01J2219/1206—Microwaves
- B01J2219/1209—Features relating to the reactor or vessel
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J2219/12—Processes employing electromagnetic waves
- B01J2219/1203—Incoherent waves
- B01J2219/1206—Microwaves
- B01J2219/1209—Features relating to the reactor or vessel
- B01J2219/1221—Features relating to the reactor or vessel the reactor per se
- B01J2219/1224—Form of the reactor
- B01J2219/123—Vessels in the form of a cup
- B01J2219/1233—Closure means, such as lids, caps, seals
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J2219/12—Processes employing electromagnetic waves
- B01J2219/1203—Incoherent waves
- B01J2219/1206—Microwaves
- B01J2219/1248—Features relating to the microwave cavity
- B01J2219/1269—Microwave guides
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J2219/12—Processes employing electromagnetic waves
- B01J2219/1203—Incoherent waves
- B01J2219/1206—Microwaves
- B01J2219/1275—Controlling the microwave irradiation variables
Landscapes
- Chemical & Material Sciences (AREA)
- Electromagnetism (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Physics & Mathematics (AREA)
- Organic Chemistry (AREA)
- Toxicology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Clinical Laboratory Science (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Constitution Of High-Frequency Heating (AREA)
- Control Of High-Frequency Heating Circuits (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US09/773,846 US6753517B2 (en) | 2001-01-31 | 2001-01-31 | Microwave-assisted chemical synthesis instrument with fixed tuning |
PCT/US2002/002072 WO2002062104A2 (en) | 2001-01-31 | 2002-01-24 | Microwave-assisted chemical synthesis instrument with fixed tuning |
Publications (1)
Publication Number | Publication Date |
---|---|
ATE277494T1 true ATE277494T1 (de) | 2004-10-15 |
Family
ID=25099496
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AT02705941T ATE277494T1 (de) | 2001-01-31 | 2002-01-24 | Instrument für mikrowellenunterstützte chemische synthese versehen mit stationärer abstimmung |
Country Status (8)
Country | Link |
---|---|
US (4) | US6753517B2 (de) |
EP (1) | EP1356710B1 (de) |
JP (1) | JP4099064B2 (de) |
AT (1) | ATE277494T1 (de) |
AU (1) | AU2002240058A1 (de) |
CA (1) | CA2436090C (de) |
DE (1) | DE60201330T2 (de) |
WO (1) | WO2002062104A2 (de) |
Families Citing this family (35)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7282184B2 (en) * | 2002-04-19 | 2007-10-16 | Cem Corporation | Microwave assisted chemical synthesis instrument with controlled pressure release |
US6744024B1 (en) * | 2002-06-26 | 2004-06-01 | Cem Corporation | Reaction and temperature control for high power microwave-assisted chemistry techniques |
US6867400B2 (en) * | 2002-07-31 | 2005-03-15 | Cem Corporation | Method and apparatus for continuous flow microwave-assisted chemistry techniques |
US7144739B2 (en) * | 2002-11-26 | 2006-12-05 | Cem Corporation | Pressure measurement and relief for microwave-assisted chemical reactions |
AU2003291587A1 (en) * | 2002-12-18 | 2004-07-09 | Personal Chemistry I Uppsala Ab | Vessel for performing microwave-assisted chemistry on small volumes of reagents |
US7393920B2 (en) * | 2003-06-23 | 2008-07-01 | Cem Corporation | Microwave-assisted peptide synthesis |
US7902488B2 (en) * | 2003-06-23 | 2011-03-08 | Cem Corporation | Microwave-assisted peptide synthesis |
US6989519B2 (en) | 2003-09-02 | 2006-01-24 | Cem Corporation | Controlled flow instrument for microwave assisted chemistry with high viscosity liquids and heterogeneous mixtures |
US7041947B2 (en) * | 2003-09-02 | 2006-05-09 | Cem Corporation | Controlled flow instrument for microwave assisted chemistry with high viscosity liquids and heterogeneous mixtures |
US7307248B2 (en) * | 2003-12-09 | 2007-12-11 | Cem Corporation | Method and apparatus for microwave assisted high throughput high pressure chemical synthesis |
DE102004010894A1 (de) * | 2004-03-06 | 2005-09-22 | Voith Paper Patent Gmbh | Verfahren und Vorrichtung zum Behandeln einer Bahn aus Papier oder Karton |
US7348526B2 (en) | 2004-08-20 | 2008-03-25 | Cem Corporation | Microwave-assisted chromatography preparation |
FR2876714B1 (fr) * | 2004-10-20 | 2008-05-02 | Francois Charles Oberthur Fidu | Procede de securisation de documents de valeur |
US7141769B2 (en) * | 2005-04-01 | 2006-11-28 | Cem Corporation | Spectroscopy-based real-time control for microwave-assisted chemistry |
US7405381B2 (en) * | 2005-08-23 | 2008-07-29 | Cem, Corporation | Real-time imaging and spectroscopy during microwave assisted chemistry |
US8314208B2 (en) * | 2006-02-10 | 2012-11-20 | Cem Corporation | Microwave enhanced N-fmoc deprotection in peptide synthesis |
AT503448B1 (de) * | 2006-03-29 | 2007-10-15 | Leica Mikrosysteme Gmbh | Gerät zur präparation biologischer proben für die elektronenmikroskopie |
US7537917B2 (en) * | 2006-03-31 | 2009-05-26 | Collins Michael J | Microwave assisted PCR amplification of DNA |
US20070251941A1 (en) * | 2006-04-26 | 2007-11-01 | Givens Kenneth R | Modular microwave processing system |
AT504371B8 (de) * | 2006-10-03 | 2008-09-15 | Leica Mikrosysteme Gmbh | Vorrichtung zur mikrowellen-gestützten präparation von proben |
US20100206834A1 (en) * | 2007-09-12 | 2010-08-19 | Q Labtech Llc | Chemical reactor with pressure release |
US8142736B2 (en) * | 2007-09-12 | 2012-03-27 | Weimin Qian | Reaction bottle with pressure release |
WO2009036186A1 (en) * | 2007-09-12 | 2009-03-19 | Q Labtech Llc | Chemical reactor with pressure release |
FR2922652B1 (fr) * | 2007-10-17 | 2010-01-01 | Millipore Corp | Systeme d'analyse microbiologique |
FR2922649B1 (fr) * | 2007-10-17 | 2010-01-01 | Millipore Corp | Machine d'analyse microbiologique |
FR2922453B1 (fr) * | 2007-10-17 | 2011-01-14 | Millipore Corp | Procede de decontamination et systeme le mettant en oeuvre |
FR2922650A1 (fr) * | 2007-10-17 | 2009-04-24 | Millipore Corp | Machine d'analyse microbiologique |
FR2922651B1 (fr) * | 2007-10-17 | 2010-03-19 | Millipore Corp | Systeme d'analyse microbiologique |
CN201404734Y (zh) * | 2009-04-28 | 2010-02-17 | 厦门市毕恩生物技术有限公司 | 底部控制式标本过滤容器 |
US9161395B2 (en) | 2011-06-30 | 2015-10-13 | Cem Corporation | Instrument for performing microwave-assisted reactions |
US10315126B2 (en) | 2013-03-14 | 2019-06-11 | Donald W. Ramer | Apparatus for molecular targeting and separation of feedstock fluids |
US9844101B2 (en) * | 2013-12-20 | 2017-12-12 | Scp Science | System and method for uniform microwave heating |
USD798814S1 (en) | 2014-12-02 | 2017-10-03 | Tdk Corporation | Coil component |
FR3066275B1 (fr) * | 2017-05-10 | 2020-09-18 | Stago Diagnostica | Automate pour la conduite automatisee d'analyses, notamment medicales |
CN111750228B (zh) * | 2020-07-09 | 2022-08-16 | 淄博齐星化学科技有限公司 | 一种用于混合气体的甲醛提纯设备及提取方法 |
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-
2001
- 2001-01-31 US US09/773,846 patent/US6753517B2/en not_active Expired - Lifetime
-
2002
- 2002-01-24 DE DE60201330T patent/DE60201330T2/de not_active Expired - Lifetime
- 2002-01-24 CA CA002436090A patent/CA2436090C/en not_active Expired - Lifetime
- 2002-01-24 WO PCT/US2002/002072 patent/WO2002062104A2/en active IP Right Grant
- 2002-01-24 AU AU2002240058A patent/AU2002240058A1/en not_active Abandoned
- 2002-01-24 EP EP02705941A patent/EP1356710B1/de not_active Expired - Lifetime
- 2002-01-24 JP JP2002562121A patent/JP4099064B2/ja not_active Expired - Fee Related
- 2002-01-24 AT AT02705941T patent/ATE277494T1/de not_active IP Right Cessation
- 2002-05-03 US US10/063,628 patent/US6630652B2/en not_active Expired - Fee Related
- 2002-05-23 US US10/063,914 patent/US6649889B2/en not_active Expired - Lifetime
- 2002-12-13 US US10/248,052 patent/US6713739B2/en not_active Expired - Lifetime
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CA2436090C (en) | 2006-07-25 |
US20020101310A1 (en) | 2002-08-01 |
US20020121513A1 (en) | 2002-09-05 |
DE60201330D1 (de) | 2004-10-28 |
WO2002062104A2 (en) | 2002-08-08 |
DE60201330T2 (de) | 2005-02-17 |
US6649889B2 (en) | 2003-11-18 |
EP1356710B1 (de) | 2004-09-22 |
WO2002062104A3 (en) | 2003-02-06 |
US6713739B2 (en) | 2004-03-30 |
US20030089706A1 (en) | 2003-05-15 |
JP4099064B2 (ja) | 2008-06-11 |
US20020117498A1 (en) | 2002-08-29 |
CA2436090A1 (en) | 2002-08-08 |
US6753517B2 (en) | 2004-06-22 |
AU2002240058A1 (en) | 2002-08-12 |
EP1356710A2 (de) | 2003-10-29 |
JP2004523863A (ja) | 2004-08-05 |
US6630652B2 (en) | 2003-10-07 |
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