ATE112978T1 - Verfahren und vorrichtung für kontinuierliche chemische reaktionen. - Google Patents
Verfahren und vorrichtung für kontinuierliche chemische reaktionen.Info
- Publication number
- ATE112978T1 ATE112978T1 AT89911229T AT89911229T ATE112978T1 AT E112978 T1 ATE112978 T1 AT E112978T1 AT 89911229 T AT89911229 T AT 89911229T AT 89911229 T AT89911229 T AT 89911229T AT E112978 T1 ATE112978 T1 AT E112978T1
- Authority
- AT
- Austria
- Prior art keywords
- feed
- chemical reactions
- reactants
- microwave heating
- section
- Prior art date
Links
Classifications
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B6/00—Heating by electric, magnetic or electromagnetic fields
- H05B6/64—Heating using microwaves
- H05B6/80—Apparatus for specific applications
- H05B6/806—Apparatus for specific applications for laboratory use
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J19/12—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
- B01J19/122—Incoherent waves
- B01J19/126—Microwaves
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
- C07C45/67—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton
- C07C45/673—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by change of size of the carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B6/00—Heating by electric, magnetic or electromagnetic fields
- H05B6/64—Heating using microwaves
- H05B6/6447—Method of operation or details of the microwave heating apparatus related to the use of detectors or sensors
- H05B6/645—Method of operation or details of the microwave heating apparatus related to the use of detectors or sensors using temperature sensors
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00054—Controlling or regulating the heat exchange system
- B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
- B01J2219/00058—Temperature measurement
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00054—Controlling or regulating the heat exchange system
- B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
- B01J2219/00065—Pressure measurement
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00132—Controlling the temperature using electric heating or cooling elements
- B01J2219/00137—Peltier cooling elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J2219/12—Processes employing electromagnetic waves
- B01J2219/1203—Incoherent waves
- B01J2219/1206—Microwaves
- B01J2219/1209—Features relating to the reactor or vessel
- B01J2219/1221—Features relating to the reactor or vessel the reactor per se
- B01J2219/1224—Form of the reactor
- B01J2219/1227—Reactors comprising tubes with open ends
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Electromagnetism (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Clinical Laboratory Science (AREA)
- Toxicology (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AUPJ087288 | 1988-10-10 | ||
AUPJ505789 | 1989-07-04 | ||
US07/892,996 US5387397A (en) | 1988-10-10 | 1992-06-03 | Method and apparatus for continuous chemical reactions |
Publications (1)
Publication Number | Publication Date |
---|---|
ATE112978T1 true ATE112978T1 (de) | 1994-11-15 |
Family
ID=27157459
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AT89911229T ATE112978T1 (de) | 1988-10-10 | 1989-10-09 | Verfahren und vorrichtung für kontinuierliche chemische reaktionen. |
Country Status (6)
Country | Link |
---|---|
US (1) | US5387397A (de) |
EP (1) | EP0437480B1 (de) |
AT (1) | ATE112978T1 (de) |
CA (1) | CA2000351C (de) |
DE (1) | DE68918950T2 (de) |
WO (1) | WO1990003840A1 (de) |
Families Citing this family (73)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2665264A1 (fr) * | 1990-07-24 | 1992-01-31 | Prolabo Sa | Procede pour realiser une reaction chimique par voie humide sur une succession d'echantillons, appareil pour la mise en óoeuvre du procede et utilisation dudit appareil. |
FR2697448B1 (fr) * | 1992-10-30 | 1995-06-16 | Moulinex Sa | Dispositif de conduite d'opérations chimiques. |
US5420039A (en) * | 1992-12-31 | 1995-05-30 | Cem Corporation | Control of continuous microwave digestion process |
WO1994026077A1 (en) * | 1993-05-05 | 1994-11-10 | Ciba-Geigy Ag | Process and plant for the manufacture of solid castings from an essentially liquid reactive medium, and oven for heating an essentially liquid medium |
WO1994026408A1 (en) * | 1993-05-11 | 1994-11-24 | Srl Inc. | Microwave irradiation method and microwave irradiation device |
ATE168039T1 (de) * | 1993-11-11 | 1998-07-15 | Werner Lautenschlaeger | Vorrichtung zum auslösen und/oder fördern chemischer oder physikalischer prozesse in einem material, insbesondere probenmaterial |
US5470541A (en) * | 1993-12-28 | 1995-11-28 | E. I. Du Pont De Nemours And Company | Apparatus and process for the preparation of hydrogen cyanide |
US5689008A (en) * | 1996-02-02 | 1997-11-18 | United Technologies Corporation | Catalytic reaction rate enhancement at low temperatures |
DE19631201C2 (de) * | 1996-08-02 | 2001-07-05 | Rainer Buchholz | Verfahren und Reaktor zur Umwandlung von Biomasse in flüssige, feste oder gasförmige Brennstoffe und Chemierohstoffe |
US6793890B2 (en) | 1997-08-20 | 2004-09-21 | The University Of Miami | Rapid tissue processor |
EP1005633B1 (de) | 1997-08-20 | 2008-09-03 | The University Of Miami | Hochqualitatives durchlaufendes verfahren zur fixierung, dehydratisierung, entfettung und imprägnation von geweben |
US6031100A (en) * | 1997-09-18 | 2000-02-29 | Bayer Corporation | Microwave syntheses of quinacridones, 6,13-Dihydroquinacridones, and 6,13-quinacridonequinones |
US6084226A (en) * | 1998-04-21 | 2000-07-04 | Cem Corporation | Use of continuously variable power in microwave assisted chemistry |
US6175037B1 (en) | 1998-10-09 | 2001-01-16 | Ucb, S.A. | Process for the preparation of (meth)acrylate esters and polyester (meth)acrylates using microwave energy as a heating source |
FR2791670A1 (fr) * | 1999-03-31 | 2000-10-06 | Rhodia Chimie Sa | Procede d'activation de substrats aromatiques par micro-ondes |
KR100411194B1 (ko) * | 2000-11-03 | 2003-12-18 | 한국화학연구원 | 연속식 마이크로파 합성법을 이용한 무기소재의 제조방법및 그 장치 |
AU2001260518A1 (en) | 2000-05-08 | 2001-11-20 | Personal Chemistry I Uppsala Ab. | Method for performing multiple chemical reactions and a kit and system therefor |
US20030091487A1 (en) * | 2001-10-19 | 2003-05-15 | Magnus Fagrell | Continuous flow heating system |
WO2003041856A1 (en) * | 2001-10-19 | 2003-05-22 | Personal Chemistry I Uppsala Ab | Continuous flow system with microwave heating |
FR2839069B1 (fr) * | 2002-04-25 | 2006-04-07 | Satie Sa | Nouveaux procedes de transesterification, esterification, interesterification, par chauffage dielectrique |
US6744024B1 (en) * | 2002-06-26 | 2004-06-01 | Cem Corporation | Reaction and temperature control for high power microwave-assisted chemistry techniques |
US6867400B2 (en) * | 2002-07-31 | 2005-03-15 | Cem Corporation | Method and apparatus for continuous flow microwave-assisted chemistry techniques |
US7157401B2 (en) * | 2002-10-17 | 2007-01-02 | Carnegie Mellon University | Catalyst for the treatment of organic compounds |
US20040074760A1 (en) * | 2002-10-17 | 2004-04-22 | Carnegie Mellon University | Production of biofuels |
US7387712B2 (en) * | 2002-10-17 | 2008-06-17 | Carnegie Mellon University | Catalytic process for the treatment of organic compounds |
JP2006510683A (ja) * | 2002-12-18 | 2006-03-30 | バイオテージ・アクチボラグ | 化学反応を制御するための方法及び装置 |
AU2002353365A1 (en) * | 2002-12-19 | 2004-07-14 | Council Of Scientific And Industrial Research | A microwave induced process for the preparation of substituted 4-vinylphenols |
FR2849343B1 (fr) | 2002-12-23 | 2009-01-23 | Aldivia | Synthese chimique comportant un traitement thermique par chauffage dielectrique intermittent, combine a un systeme de recirculation |
US7393920B2 (en) * | 2003-06-23 | 2008-07-01 | Cem Corporation | Microwave-assisted peptide synthesis |
FR2858616B1 (fr) * | 2003-08-07 | 2006-02-17 | Aldivia Sa | Procede d'estolidation par chauffage dielectrique |
US7041947B2 (en) * | 2003-09-02 | 2006-05-09 | Cem Corporation | Controlled flow instrument for microwave assisted chemistry with high viscosity liquids and heterogeneous mixtures |
US6989519B2 (en) * | 2003-09-02 | 2006-01-24 | Cem Corporation | Controlled flow instrument for microwave assisted chemistry with high viscosity liquids and heterogeneous mixtures |
US7470401B2 (en) * | 2003-10-24 | 2008-12-30 | The University Of Miami | Simplified tissue processing |
EE200400060A (et) * | 2004-02-25 | 2005-10-17 | Nordic Alternative Energy OÜ | Meetod ja seade karboksüülhapete estrite pidevaprotsessiliseks transesterifikatsioonikssuperkriitilises monovalentses alkoholis |
US20050274065A1 (en) * | 2004-06-15 | 2005-12-15 | Carnegie Mellon University | Methods for producing biodiesel |
JPWO2006126439A1 (ja) * | 2005-05-24 | 2008-12-25 | 日立化成工業株式会社 | 共役ポリマーの製造方法 |
KR100693126B1 (ko) * | 2005-07-14 | 2007-03-13 | 한국화학연구원 | 다공성 물질 및 혼합 금속산화물의 연속적 제조방법 및연속적 제조 장치 |
GB0608512D0 (en) | 2006-04-28 | 2006-06-07 | Vincent Processes Ltd | Process for the production of esters of sugars and sugar derivatives |
US7998418B1 (en) | 2006-06-01 | 2011-08-16 | Nanotek, Llc | Evaporator and concentrator in reactor and loading system |
US7641860B2 (en) | 2006-06-01 | 2010-01-05 | Nanotek, Llc | Modular and reconfigurable multi-stage microreactor cartridge apparatus |
US7854902B2 (en) * | 2006-08-23 | 2010-12-21 | Nanotek, Llc | Modular and reconfigurable multi-stage high temperature microreactor cartridge apparatus and system for using same |
DE102006047619B4 (de) * | 2006-10-09 | 2008-11-13 | Clariant International Limited | Verfahren zur Herstellung basischer Fettsäureamide |
DE102006047617B4 (de) | 2006-10-09 | 2008-11-27 | Clariant International Limited | Verfahren zur Herstellung basischer (Meth)acrylamide |
US7797988B2 (en) | 2007-03-23 | 2010-09-21 | Advion Biosystems, Inc. | Liquid chromatography-mass spectrometry |
DE102008017219A1 (de) * | 2008-04-04 | 2009-10-08 | Clariant International Ltd. | Verfahren zur Herstellung von Amiden in Gegenwart von überhitztem Wasser |
DE102008017213B4 (de) * | 2008-04-04 | 2012-08-09 | Clariant International Limited | Kontinuierliches Verfahren zur Herstellung von Amiden aliphatischer Hydroxycarbonsäuren |
DE102008017214B4 (de) * | 2008-04-04 | 2012-02-16 | Clariant International Limited | Kontinuierliches Verfahren zur Herstellung von Fettsäurealkanolamiden |
DE102008017215B4 (de) * | 2008-04-04 | 2012-08-09 | Clariant International Ltd. | Kontinuierliches Verfahren zur Herstellung von Amiden ethylenisch ungesättigter Carbonsäuren |
DE102008017216B4 (de) | 2008-04-04 | 2013-08-14 | Clariant International Ltd. | Kontinuierliches Verfahren zur Herstellung von Fettsäureamiden |
DE102008017217A1 (de) * | 2008-04-04 | 2009-10-08 | Clariant International Ltd. | Kontinuierliches Verfahren zur Herstellung von Amiden aromatischer Carbonsäuren |
DE102008017218B4 (de) * | 2008-04-04 | 2011-09-22 | Clariant International Ltd. | Kontinuierliches Verfahren zur Herstellung von Amiden niederer aliphatischer Carbonsäuren |
US20090298172A1 (en) | 2008-05-28 | 2009-12-03 | Steven Paul Wheeler | Histological specimen treatment apparatus and method |
PL2343994T3 (pl) | 2008-09-23 | 2015-06-30 | Aseptia Inc | Układ elektromagnetyczny |
WO2010084333A1 (en) | 2009-01-26 | 2010-07-29 | Cambrex Karlskoga Ab | Microwave apparatus |
JP5107278B2 (ja) * | 2009-02-16 | 2012-12-26 | 株式会社日立製作所 | マイクロ波加熱装置および加熱方法 |
DE102009031053A1 (de) * | 2009-06-30 | 2011-01-13 | Clariant International Ltd. | Kontinuierliches Verfahren zur Herstellung von Estern aliphatischer Carbonsäuren |
DE102009031056A1 (de) * | 2009-06-30 | 2011-01-27 | Clariant International Ltd. | Kontinuierliches Verfahren zur Acrylierung von Aminogruppen tragenden organischen Säuren |
DE102009031054A1 (de) * | 2009-06-30 | 2011-01-13 | Clariant International Ltd. | Kontinuierliches Verfahren zur Herstellung von Estern aromatischer Carbonsäuren |
DE102009031058A1 (de) | 2009-06-30 | 2011-01-27 | Clariant International Ltd. | Kontinuierliches Verfahren zur Herstellung von Amiden aromatischer Carbonsäuren |
DE102009031059A1 (de) * | 2009-06-30 | 2011-01-05 | Clariant International Ltd. | Vorrichtung zur kontinuierlichen Durchführung chemischer Reaktionen bei hohen Temperaturen |
DE102009031057A1 (de) * | 2009-06-30 | 2011-01-05 | Clariant International Ltd. | Kontinuierliches Verfahren zur Herstellung von Amiden aliphatischer Carbonsäuren |
DE102009033216A1 (de) | 2009-07-15 | 2011-01-27 | Brümmer, Heinz | Vorrichtung und Verfahren zur Herstellung von Leichtölen aus Biomasse und kohlenwasserstoffhaltigen Stoffen mittels Verpressen der Reaktionsmasse zusammen mit einem zeolithischen Katalysator als Reaktionsbeschleuniger zu Pellets und anschließender Molekülverkürzung der Reaktionsmasse durch von Mikrowellenstrahlung initiiertem Plasma in einem Flachbettreaktor |
DE102009042522A1 (de) | 2009-09-22 | 2011-04-07 | Clariant International Ltd. | Kontinuierliches Umesterungsverfahren |
DE102009042523B4 (de) | 2009-09-22 | 2012-02-16 | Clariant International Ltd. | Vorrichtung und Verfahren zur kontinuierlichen Durchführung heterogen katalysierter chemischer Reaktionen bei hohen Temperaturen |
DE102010056564A1 (de) | 2010-12-30 | 2012-07-05 | Clariant International Limited | Hydroxylgruppen und Estergruppen tragende Polymere und Verfahren zu ihrer Herstellung |
DE102010056566A1 (de) | 2010-12-30 | 2012-07-05 | Clariant International Ltd. | Kontinuierliches Verfahren zur Veresterung Säuregruppen tragender Polymere |
DE102010056565A1 (de) | 2010-12-30 | 2012-07-05 | Clariant International Ltd. | Verfahren zur Modifizierung Hydroxylgruppen tragender Polymere |
CN102260170B (zh) * | 2011-06-02 | 2014-10-15 | 浙江大学 | 微波管道化生产乙酸正t酯的方法 |
US9180429B2 (en) | 2012-02-28 | 2015-11-10 | Inventram Fikri Mulkiyet Haklari Yonetim Ticaret Ve Yatirim Anonim Sirketi | Zeolite coating preparation assembly and operation method |
US10450259B2 (en) | 2013-06-26 | 2019-10-22 | University Of Virginia Patent Foundation | Compositions and methods for hydrocarbon functionalization |
EP3006103A1 (de) * | 2014-10-06 | 2016-04-13 | Paul Scherrer Institut | Verfahren zur Herstellung metallorganischer Rahmen und kovalenter organischer Rahmen |
US10365189B2 (en) | 2015-05-07 | 2019-07-30 | Steven Wheeler | Histological specimen treatment |
CN116520712B (zh) * | 2023-07-03 | 2023-08-22 | 贵阳职业技术学院 | 一种反应容器入料量自适应调控方法、系统、终端及介质 |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3535482A (en) * | 1968-06-26 | 1970-10-20 | Hammtronics Systems Inc | Microwave apparatus for rapid heating of fluids |
GB1371400A (en) * | 1972-06-14 | 1974-10-23 | Camph Eng Co Ab | Method of heating blood |
NL7509305A (nl) * | 1974-08-07 | 1976-02-10 | British Petroleum Co | Werkwijze voor het tot stand brengen van chemische reacties. |
AU521896B2 (en) * | 1976-11-17 | 1982-05-06 | Jean, O.A.L. | Apparatus for subjecting a material to electromagnetic waves |
AU7556981A (en) * | 1976-12-23 | 1981-12-24 | Kenneth Frederick Currie | Irradiation unit |
US4353890A (en) * | 1979-10-24 | 1982-10-12 | Colgate-Palmolive Company | Stabilization of carrageenan-containing toothpaste |
GB2098040A (en) * | 1981-03-31 | 1982-11-10 | Sanyo Electric Co | System for and method of sterilization of food material |
-
1989
- 1989-10-09 AT AT89911229T patent/ATE112978T1/de not_active IP Right Cessation
- 1989-10-09 WO PCT/AU1989/000437 patent/WO1990003840A1/en active IP Right Grant
- 1989-10-09 DE DE68918950T patent/DE68918950T2/de not_active Expired - Fee Related
- 1989-10-09 EP EP89911229A patent/EP0437480B1/de not_active Expired - Lifetime
- 1989-10-10 CA CA002000351A patent/CA2000351C/en not_active Expired - Fee Related
-
1992
- 1992-06-03 US US07/892,996 patent/US5387397A/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
DE68918950T2 (de) | 1995-03-16 |
CA2000351C (en) | 1999-11-30 |
EP0437480A4 (en) | 1991-10-30 |
US5387397A (en) | 1995-02-07 |
EP0437480A1 (de) | 1991-07-24 |
WO1990003840A1 (en) | 1990-04-19 |
EP0437480B1 (de) | 1994-10-19 |
DE68918950D1 (de) | 1994-11-24 |
CA2000351A1 (en) | 1990-04-10 |
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