AR124679A1 - Forma cristalina novedosa de piroxasulfona, métodos para su preparación y uso de la misma - Google Patents

Forma cristalina novedosa de piroxasulfona, métodos para su preparación y uso de la misma

Info

Publication number
AR124679A1
AR124679A1 ARP220100104A ARP220100104A AR124679A1 AR 124679 A1 AR124679 A1 AR 124679A1 AR P220100104 A ARP220100104 A AR P220100104A AR P220100104 A ARP220100104 A AR P220100104A AR 124679 A1 AR124679 A1 AR 124679A1
Authority
AR
Argentina
Prior art keywords
pyroxasulfone
crystal modification
preparation
novel crystalline
modification
Prior art date
Application number
ARP220100104A
Other languages
English (en)
Inventor
James Timothy Bristow
Original Assignee
Rotam Agrochem Int Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rotam Agrochem Int Co Ltd filed Critical Rotam Agrochem Int Co Ltd
Publication of AR124679A1 publication Critical patent/AR124679A1/es

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D411/00Heterocyclic compounds containing two or more hetero rings, at least one ring having oxygen and sulfur atoms as the only ring hetero atoms
    • C07D411/02Heterocyclic compounds containing two or more hetero rings, at least one ring having oxygen and sulfur atoms as the only ring hetero atoms containing two hetero rings
    • C07D411/12Heterocyclic compounds containing two or more hetero rings, at least one ring having oxygen and sulfur atoms as the only ring hetero atoms containing two hetero rings linked by a chain containing hetero atoms as chain links
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D413/00Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms
    • C07D413/02Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings
    • C07D413/12Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings linked by a chain containing hetero atoms as chain links
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01GHORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
    • A01G13/00Protecting plants
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/02Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
    • A01N25/04Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/12Powders or granules
    • A01N25/14Powders or granules wettable
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/72Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
    • A01N43/80Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms five-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,2
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01PBIOCIDAL, PEST REPELLANT, PEST ATTRACTANT OR PLANT GROWTH REGULATORY ACTIVITY OF CHEMICAL COMPOUNDS OR PREPARATIONS
    • A01P13/00Herbicides; Algicides
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07BGENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00Indexing scheme relating to specific properties of organic compounds
    • C07B2200/13Crystalline forms, e.g. polymorphs

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Environmental Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Wood Science & Technology (AREA)
  • Agronomy & Crop Science (AREA)
  • Dentistry (AREA)
  • Toxicology (AREA)
  • Dispersion Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Steroid Compounds (AREA)
  • Plural Heterocyclic Compounds (AREA)

Abstract

Se proporciona una modificación cristalina novedosa de Piroxasulfona, caracterizada por un difractograma de rayos X en polvo (XRD), un espectro de infrarrojos (IR), un punto de fusión y/o un perfil de calorimetría diferencial de barrido (DSC). También se proporciona un método para la preparación de la modificación cristalina de Piroxasulfona, que comprende: i) proporcionar una solución de Piroxasulfona en un sistema de disolvente que comprende uno o más disolventes; ii) precipitar la modificación cristalina I de Piroxasulfona en la solución; y iii) aislar la modificación cristalina I de Piroxasulfona precipitada. También se proporcionan composiciones que comprenden la modificación cristalina I de Piroxasulfona y el uso de la modificación cristalina I en el control del crecimiento de plantas no deseadas. Reivindicación 1: Una modificación cristalina I de Piroxasulfona, presentando la modificación cristalina al menos tres de las siguientes reflexiones, en cualquier combinación, como 2q ± 0.2 grados en un difractograma de rayos X en polvo (XRD en inglés) registrado usando radiación Cu-Ka a 25ºC: @@@@@@@@@
ARP220100104A 2021-02-11 2022-01-19 Forma cristalina novedosa de piroxasulfona, métodos para su preparación y uso de la misma AR124679A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB2101909.6A GB2603771A (en) 2021-02-11 2021-02-11 Novel crystalline form of pyroxa-sulfone, methods for its preparation and use of the same

Publications (1)

Publication Number Publication Date
AR124679A1 true AR124679A1 (es) 2023-04-26

Family

ID=75338926

Family Applications (1)

Application Number Title Priority Date Filing Date
ARP220100104A AR124679A1 (es) 2021-02-11 2022-01-19 Forma cristalina novedosa de piroxasulfona, métodos para su preparación y uso de la misma

Country Status (10)

Country Link
US (1) US20220256852A1 (es)
EP (1) EP4043456A1 (es)
CN (1) CN114920735A (es)
AR (1) AR124679A1 (es)
AU (1) AU2021427503B2 (es)
FR (1) FR3119622A1 (es)
GB (1) GB2603771A (es)
MA (1) MA55436A1 (es)
TW (1) TW202231637A (es)
WO (1) WO2022170871A1 (es)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2023047416A1 (en) * 2021-09-24 2023-03-30 Upl Limited A process for preparation of isoxazole compound
WO2023194957A1 (en) * 2022-04-08 2023-10-12 Upl Limited A process for preparation of 3-[5-(difluoromethoxy)-1- methyl-3-(trifluoromethyl)pyrazol-4- ylmethylsulfonyl]-4,5-dihydro-5,5-dimethyl-1,2-oxazole and its intermediates
CN114989157A (zh) * 2022-06-28 2022-09-02 安徽久易农业股份有限公司 一种砜吡草唑的晶型a及其制备方法和应用
WO2024105520A1 (en) * 2022-11-15 2024-05-23 Upl Limited Herbicide composition

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2004013106A1 (ja) * 2002-08-01 2004-02-12 Ihara Chemical Industry Co., Ltd. ピラゾール誘導体及びその製造方法
UA78071C2 (en) * 2002-08-07 2007-02-15 Kumiai Chemical Industry Co Herbicidal composition
WO2011063842A1 (de) * 2009-11-26 2011-06-03 Basf Se Verfahren zur herstellung 5,5-disubstituierter 4,5-dihydroisoxazol-3-thiocarboxamidin-salze
PL3319437T3 (pl) * 2015-07-10 2020-03-31 BASF Agro B.V. Kompozycja chwastobójcza zawierająca cynmetylinę i piroksasulfon
CN106966983B (zh) 2017-05-02 2019-07-02 青岛清原化合物有限公司 无定形态苯唑氟草酮及其制备方法和用途
MX2021004358A (es) * 2018-10-31 2021-05-31 Kumiai Chemical Industry Co Composicion de microcapsula, metodo de produccion, formulacion agroquimica que contiene dicha composicion, y metodo de control de malezas.
US20210392881A1 (en) * 2018-10-31 2021-12-23 Kumiai Chemical Industry Co., Ltd. Microcapsule composition, method for manufacturing same, agrochemical formulation comprising same and weed control method
WO2020240392A1 (en) 2019-05-24 2020-12-03 Pi Industries Limited Process for preparation of pyroxasulfone
WO2021002484A2 (ja) 2019-10-31 2021-01-07 クミアイ化学工業株式会社 除草剤及びその中間体の製造方法
AR121018A1 (es) * 2020-01-15 2022-04-06 Adama Agan Ltd Forma en estado sólido de piroxasulfona
CN111393427B (zh) 2020-04-30 2021-11-30 安徽久易农业股份有限公司 一种砜吡草唑的合成方法
CN111574511A (zh) * 2020-06-28 2020-08-25 安徽久易农业股份有限公司 一种砜吡草唑的合成方法及其应用

Also Published As

Publication number Publication date
US20220256852A1 (en) 2022-08-18
TW202231637A (zh) 2022-08-16
GB2603771A (en) 2022-08-17
WO2022170871A1 (en) 2022-08-18
MA55436A1 (fr) 2022-09-30
AU2021427503A1 (en) 2022-10-27
FR3119622A1 (fr) 2022-08-12
CN114920735A (zh) 2022-08-19
EP4043456A1 (en) 2022-08-17
AU2021427503B2 (en) 2024-02-15
GB202101909D0 (en) 2021-03-31

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