ZA202307893B - Preparation method for ioversol hydrolysate - Google Patents
Preparation method for ioversol hydrolysateInfo
- Publication number
- ZA202307893B ZA202307893B ZA2023/07893A ZA202307893A ZA202307893B ZA 202307893 B ZA202307893 B ZA 202307893B ZA 2023/07893 A ZA2023/07893 A ZA 2023/07893A ZA 202307893 A ZA202307893 A ZA 202307893A ZA 202307893 B ZA202307893 B ZA 202307893B
- Authority
- ZA
- South Africa
- Prior art keywords
- ioversol
- hydrolysate
- preparation
- industrial
- iodide
- Prior art date
Links
- AMDBBAQNWSUWGN-UHFFFAOYSA-N Ioversol Chemical compound OCCN(C(=O)CO)C1=C(I)C(C(=O)NCC(O)CO)=C(I)C(C(=O)NCC(O)CO)=C1I AMDBBAQNWSUWGN-UHFFFAOYSA-N 0.000 title abstract 4
- 229960004537 ioversol Drugs 0.000 title abstract 4
- 239000000413 hydrolysate Substances 0.000 title abstract 2
- 238000002360 preparation method Methods 0.000 title abstract 2
- XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 abstract 2
- 239000002994 raw material Substances 0.000 abstract 2
- HZDNNJABYXNPPV-UHFFFAOYSA-N (2-chloro-2-oxoethyl) acetate Chemical compound CC(=O)OCC(Cl)=O HZDNNJABYXNPPV-UHFFFAOYSA-N 0.000 abstract 1
- 108010009736 Protein Hydrolysates Proteins 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 238000002425 crystallisation Methods 0.000 abstract 1
- 230000008025 crystallization Effects 0.000 abstract 1
- 230000007613 environmental effect Effects 0.000 abstract 1
- 230000003301 hydrolyzing effect Effects 0.000 abstract 1
- 238000009776 industrial production Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- 230000001105 regulatory effect Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/14—Preparation of carboxylic acid amides by formation of carboxamide groups together with reactions not involving the carboxamide groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/12—Preparation of carboxylic acid amides by reactions not involving the formation of carboxamide groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210049754.0A CN114409566B (zh) | 2022-01-17 | 2022-01-17 | 一种碘佛醇水解物的制备方法 |
| PCT/CN2022/137106 WO2023104063A1 (zh) | 2022-01-17 | 2022-12-07 | 一种碘佛醇水解物的制备方法 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ZA202307893B true ZA202307893B (en) | 2024-04-24 |
Family
ID=81272913
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ZA2023/07893A ZA202307893B (en) | 2022-01-17 | 2023-08-14 | Preparation method for ioversol hydrolysate |
Country Status (3)
| Country | Link |
|---|---|
| CN (1) | CN114409566B (zh) |
| WO (1) | WO2023104063A1 (zh) |
| ZA (1) | ZA202307893B (zh) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114409566B (zh) * | 2022-01-17 | 2022-11-22 | 安庆朗坤药业有限公司 | 一种碘佛醇水解物的制备方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1993016981A1 (en) * | 1992-02-28 | 1993-09-02 | Mallinckrodt Medical, Inc. | Synthesis of ioversol using a minimal excess of acetoxyacetylchloride |
| CN109134289B (zh) * | 2017-06-16 | 2021-06-11 | 成都西岭源药业有限公司 | 一种造影剂中间体的合成方法及其应用 |
| CN110028418A (zh) * | 2019-03-26 | 2019-07-19 | 大道隆达（北京）医药科技发展有限公司 | 一种碘佛醇的制备方法 |
| GB202009917D0 (en) * | 2020-06-29 | 2020-08-12 | Ge Healthcare As | Process for the preparation of iopamidol |
| CN114409566B (zh) * | 2022-01-17 | 2022-11-22 | 安庆朗坤药业有限公司 | 一种碘佛醇水解物的制备方法 |
-
2022
- 2022-01-17 CN CN202210049754.0A patent/CN114409566B/zh active Active
- 2022-12-07 WO PCT/CN2022/137106 patent/WO2023104063A1/zh unknown
-
2023
- 2023-08-14 ZA ZA2023/07893A patent/ZA202307893B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CN114409566B (zh) | 2022-11-22 |
| WO2023104063A1 (zh) | 2023-06-15 |
| CN114409566A (zh) | 2022-04-29 |
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