WO2023284749A1 - Side-feeding monocrystal furnace - Google Patents
Side-feeding monocrystal furnace Download PDFInfo
- Publication number
- WO2023284749A1 WO2023284749A1 PCT/CN2022/105269 CN2022105269W WO2023284749A1 WO 2023284749 A1 WO2023284749 A1 WO 2023284749A1 CN 2022105269 W CN2022105269 W CN 2022105269W WO 2023284749 A1 WO2023284749 A1 WO 2023284749A1
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- WO
- WIPO (PCT)
- Prior art keywords
- hole
- sealing member
- single crystal
- feeding
- crystal furnace
- Prior art date
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- 238000007789 sealing Methods 0.000 claims abstract description 94
- 239000013078 crystal Substances 0.000 claims abstract description 65
- 238000009413 insulation Methods 0.000 claims abstract description 61
- 230000000630 rising effect Effects 0.000 claims abstract description 16
- 230000007246 mechanism Effects 0.000 claims description 65
- 230000001681 protective effect Effects 0.000 claims description 17
- 230000001174 ascending effect Effects 0.000 claims description 4
- 238000004321 preservation Methods 0.000 claims description 4
- 229910021421 monocrystalline silicon Inorganic materials 0.000 abstract description 9
- 239000010410 layer Substances 0.000 description 58
- 238000000034 method Methods 0.000 description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 12
- 239000002994 raw material Substances 0.000 description 8
- 230000000694 effects Effects 0.000 description 6
- 230000008569 process Effects 0.000 description 6
- 239000011261 inert gas Substances 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 230000009471 action Effects 0.000 description 4
- 230000005484 gravity Effects 0.000 description 4
- 229910002804 graphite Inorganic materials 0.000 description 3
- 239000010439 graphite Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 230000000903 blocking effect Effects 0.000 description 2
- CREMABGTGYGIQB-UHFFFAOYSA-N carbon carbon Chemical compound C.C CREMABGTGYGIQB-UHFFFAOYSA-N 0.000 description 2
- 239000011203 carbon fibre reinforced carbon Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- 239000011810 insulating material Substances 0.000 description 2
- 239000011229 interlayer Substances 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000010298 pulverizing process Methods 0.000 description 2
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 229910021419 crystalline silicon Inorganic materials 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
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- 239000003039 volatile agent Substances 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B15/00—Single-crystal growth by pulling from a melt, e.g. Czochralski method
- C30B15/02—Single-crystal growth by pulling from a melt, e.g. Czochralski method adding crystallising materials or reactants forming it in situ to the melt
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/02—Elements
- C30B29/06—Silicon
Definitions
- the present application relates to the technical field of single crystal manufacturing equipment, in particular to a side feeding single crystal furnace.
- the industry has begun to develop side-feeding single crystal furnaces, that is, feeding from the side of the single crystal furnace, to improve the loss of heat energy caused by feeding, and to reduce the impact of the original high-altitude drop feeding on heat. effect on field life.
- the feeding device is usually installed on the side of the single crystal furnace, that is, it is necessary to open a through hole in the side of the furnace cylinder of the single crystal furnace and the thermal field insulation layer, so that the feeding device can enter the furnace cylinder through the through hole. feed.
- the embodiments of the present application are proposed to provide a side-feed single crystal furnace that overcomes the above problems or at least partially solves the above problems.
- the embodiment of the present application discloses a single crystal furnace with side feeding. device, the insulation layer is located between the crucible and the furnace body, wherein,
- a first through hole is opened on the side of the furnace body, and a second through hole is opened at a position opposite to the first through hole in the thermal insulation layer;
- the lifting device is connected with the sealing member, and is used to drive the sealing member to switch between a raised state and a lowered state.
- the sealing member rises, and the feeding device can pass through the sealing member.
- the first through hole and the second through hole are opposite to the opening of the crucible.
- the sealing member descends, and the sealing member can seal the second through hole.
- the single crystal furnace further includes a protection cylinder, and the protection cylinder is embedded in the second through hole;
- the protective cylinder is provided with a third through hole, and the third through hole is used for passing through the feeding device.
- the single crystal furnace includes a flexible hanging piece, one end of the hanging piece is connected to the lifting device, and the other end of the hanging piece is used to hang the sealing element.
- a counterweight is further provided in the single crystal furnace, and the counterweight is installed at the end where the sealing member is connected to the pendant.
- a first inclined plane structure is provided at the position where the thermal insulation layer is opposite to the sealing member, and a second inclined plane structure is provided at the position where the sealing member is opposite to the thermal insulation layer;
- the first slope structure includes: a first sub-slope structure and a second sub-slope structure, and the second through hole is disposed between the first sub-slope structure and the second sub-slope structure;
- both the first sub-slope structure and the second sub-slope structure are in contact with the second slope structure.
- the first included angle between the first slope structure and the axis of the thermal insulation layer is 5-15°
- the second angle between the second slope structure and the axis of the thermal insulation layer It is 75-85°.
- the feeding device further includes a feeding valve connected to the first through hole and the feeding device respectively;
- the feeding valve is opened, and the feeding device can pass through the first through hole and the second through hole to be opposite to the opening of the crucible.
- the feeding device includes a feeding mechanism and a telescopic tube, the charging mechanism is connected to the telescopic tube, and the telescopic tube is connected to the feeding valve;
- the telescopic tube includes a compressed state and an expanded state.
- the feeding mechanism can be driven to pass through the first through hole, the second through hole and the crucible.
- the opening is opposite.
- the lifting device includes: a driving mechanism and a lifting mechanism, the driving mechanism is arranged in the furnace body, the driving mechanism is connected to the lifting mechanism, and the lifting mechanism is connected to the sealing member;
- the driving mechanism is used to drive the lifting mechanism to rise or fall, and the rising or falling of the lifting mechanism drives the sealing member to switch between the rising state and the falling state.
- the single crystal furnace further includes a heat exchange mechanism, the heat exchange mechanism is arranged above the crucible, the lifting device is connected to the heat exchange mechanism, and the heat exchange mechanism is connected to the sealing member connect;
- the lifting device is used to drive the heat exchange mechanism to ascend or descend, and the ascending or descending of the heat exchanging mechanism drives the sealing member to switch between the ascending state and the descending state.
- the lifting device can drive the sealing member to switch to the rising state, so that the charging device can pass through the first through hole on the side of the furnace body and the second through hole on the insulation layer and the The openings of the crucibles are opposite to each other, so that the side feeding of the single crystal furnace can be realized, which can improve the influence of the high-altitude drop feeding on the life of the thermal field.
- the lifting device can also drive the sealing member to switch to the descending state, so that the sealing member can block and protect the second through hole on the heat preservation layer, improve the life of the thermal field, and reduce the temperature loss in the non-feeding condition. Heat energy loss, stabilize the temperature field and air flow balance in the furnace body of the single crystal furnace, reduce the probability of disconnection and polycrystalline growth, and improve the crystal pulling efficiency and quality of single crystal silicon.
- Fig. 1 is the structural representation of a kind of single crystal furnace of the present application
- Fig. 2 is the structural representation of another kind of single crystal furnace of the present application.
- Fig. 3 is a schematic structural view of another single crystal furnace of the present application.
- Fig. 4 is a schematic structural diagram of another single crystal furnace of the present application.
- 1-furnace body 11-first through hole, 2-feeding device, 21-feeding valve, 22-feeding mechanism, 23-telescopic tube, 3-insulation layer, 31 first slope structure, 311-first sub-slope structure , 312-second sub-slope structure, 32-second through hole, 41-seal, 411-second slope structure, 42-counterweight, 5-crucible, 6-lifting device, 7-protective cylinder, 71- The third through hole, 81-the pendant, 82-the rigid connecting plate, 9-the heat exchange mechanism.
- One of the core ideas of the embodiments of the present application is to provide a side-feed single crystal furnace.
- FIG. 1 it shows a schematic structural view of a single crystal furnace of the present application.
- the present application provides a single crystal furnace with side feeding, and the single crystal furnace may specifically include: a furnace body 1.
- the feeding device 2 and the insulation layer 3, the seal 41, the crucible 5 and the lifting device 6 arranged in the furnace body 1, the insulation layer 3 can be located between the crucible 5 and the furnace body 1, wherein the side of the furnace body 1
- a first through hole 11 can be provided, and a second through hole 32 can be provided at the position where the insulation layer 3 is opposite to the first through hole 11; Switch between the descending state.
- the sealing member 41 rises, and the feeding device 2 can pass through the first through hole 11 and the second through hole 32 to be opposite to the opening of the crucible 5.
- the sealing member 41 descends.
- the seal 41 may seal the second through hole 32 .
- the lifting device 6 can drive the sealing member 41 to switch to the rising state, so that the charging device 2 can pass through the first through hole 11 on the side of the furnace body 1 and the second through hole 32 on the insulation layer 3 and The openings of the crucible 5 face each other to realize lateral feeding of the single crystal furnace, which can improve the influence of falling feeding from high altitude on the service life of the thermal field.
- the lifting device 6 can also be switched to the descending state, and the sealing member 41 can be lowered, so that the sealing member 41 can block and protect the second through hole 32 on the insulation layer 3, improve the life of the thermal field, and reduce the heat energy in the non-feeding situation. Loss, stabilize the temperature field and air flow balance in the furnace body 1 of the single crystal furnace, reduce the probability of disconnection and polycrystalline growth, and improve the crystal pulling efficiency and quality of single crystal silicon.
- the first through hole 11 is arranged on the side of the furnace body 1, and the charging device 2 is also arranged on the side of the furnace body 1, so that the charging device 2 can feed into the crucible 5 from the side of the furnace body 1, which can reduce the The loss of heat energy caused during the process of stopping feeding; it can also avoid the impact of high-altitude falling feeding on the life of the thermal field; and the feeding device 2 is set on the side of the furnace body 1, which can break the restriction on the weight of feeding, save feeding time and reduce feeding Number of workers.
- the power consumption of the single crystal furnace in the embodiment of the present application can be reduced by more than 60%.
- the lifting device 6 drives the sealing member 41 to switch to the rising state, the sealing member 41 rises, the second through hole 32 is opened, and the feeding device 2 can pass through the first through hole 11 and the second through hole 32, and to Add raw materials in the crucible 5 .
- the lifting device 6 can drive the sealing member 41 to switch to the descending state, and the sealing member 41 can be closely attached to the insulation layer 3 to block the second through hole 32.
- the single crystal furnace in the embodiment of the present application is a device that melts polycrystalline material with a heater and grows a single crystal by Czochralski method in an environment of inert gas (mainly nitrogen and helium).
- the furnace body 1 in the embodiment of the present application is the equipment body of the single crystal furnace, which is used for installing and connecting the insulation layer 3 , the sealing member 41 , the crucible 5 , the lifting device 6 and the feeding device 2 .
- the feeding device 2 in the embodiment of the present application is a device for storing raw materials and putting the raw materials into the crucible 5 .
- the crucible 5 in the embodiment of the present application is an important part of a chemical instrument. It is a container that can melt and refine metal liquid and solid-liquid heating and reaction, and is the basis for ensuring the smooth progress of chemical reactions. Specifically, in the embodiment of the present application, the crucible 5 is a container for melting raw materials to grow single crystal silicon.
- the insulation layer 3 in the embodiment of the present application may be an insulation interlayer used between the furnace body 1 and the heater in the single crystal furnace.
- the heater can be used to heat the raw material in the crucible 5 .
- the insulation layer 3 can be located between the crucible 5 and the furnace body 1 to prevent heat loss and stabilize the growth environment of single crystal silicon.
- the insulation layer 3 can be a material with many advantages such as high heat preservation rate, windproof, rainproof, anti-aging, flame retardant, strong water resistance, dustproof, moistureproof, acid and alkali resistance, easy retractable, long service life, etc. insulation felt.
- the sealing member 41 in the embodiment of the present application can be used to seal the thermal insulation layer 3 to further improve the thermal insulation effect of the thermal insulation layer 3 .
- both the thermal insulation layer 3 and the sealing member 41 can be heat insulating material pieces.
- both the heat insulating layer 3 and the sealing member 41 are made of heat insulating material, which can reduce heat loss and increase the crystal pulling speed of single crystal silicon.
- the materials of the insulation layer 3 and the sealing member 41 may be graphite soft felt, solidified carbon felt, etc., which are not specifically limited in this embodiment of the present application.
- the lifting device 6 in the embodiment of the present application can drive the sealing member 41 to rise or fall.
- the lifting device 6 may include a driving motor, and the driving motor may provide a motive force.
- the drive motor can be connected with the seal 41 to directly drive the seal 41 to rise or fall.
- a heat shielding device is also provided in the furnace body 1, and the heat shielding device may be a structural component in the single crystal furnace for passing water through the interlayer satisfying the process.
- the heat shielding device may include a water pipe, and the water pipe may include a water inlet pipe and a water outlet pipe, and the hardness of the water inlet pipe and the water outlet pipe is relatively high.
- the lifting device 6 can be connected with the water pipe, and drives the heat shielding device to rise or fall, and the heat shielding device can be a heat exchanger or a heat shield.
- the sealing member 41 can also be connected to a water pipe, so that the driving motor can also drive the sealing member 41 to rise or fall through the water pipe, which is not specifically limited in this embodiment of the present application.
- first through hole 11 and the second through hole 32 may be circular, quadrilateral, pentagonal or hexagonal, etc., which are not specifically limited in this embodiment of the present application.
- the single crystal furnace can also include a protective cylinder 7, which can be embedded in the second through hole 32; the protective cylinder 7 can be provided with a third through hole 71, and the third through hole 71 can be Used for threading the feeding device 2.
- the protective cylinder 7 is embedded in the second through hole 32, and is provided with a third through hole 71, so that the feeding device 2 can pass through the first through hole 11 and the third through hole 71 to the crucible in sequence. 5 to feed.
- the airflow can scour the third through hole 71, so that the protective cylinder 7 can protect the insulation layer 3, alleviate the pulverization phenomenon caused by the airflow scour to the insulation layer 3, and improve the service life of the insulation layer 3.
- the furnace body 1 can be evacuated with an inert gas, and the inert gas with pressure can enter the furnace body 1 from the first through hole 11, and the third through hole of the protective cylinder 7
- the holes 71 are scoured by high-temperature air flow.
- the inert gas can also drive volatiles out of the furnace body 1 , and the inert gas can also flush the third through hole 71 of the protective cylinder 7 with a high-temperature air flow.
- the protection tube 7 is embedded in the second through hole 32 of the insulation layer 3, which can protect the insulation layer 3 and prevent it from being scoured by the high-temperature air flow, thereby preventing the insulation layer 3 from being washed by the second through hole 32. Pulverization occurs at the through hole 32, which improves the service life of the insulation layer 3.
- the protective tube 7 can better protect the heat insulating layer 3.
- the heat insulating layer 3 in the embodiment of the present application has no second through hole 32 compared with the prior art.
- the insulating layer 3 of the through hole 32 can have a substantially equal service life.
- the material of the protective cylinder 7 includes at least one of graphite and carbon-carbon composite materials.
- the material of the protective cylinder 7 is graphite or carbon-carbon composite material, which can improve the protective effect of the protective cylinder 7 on the insulation layer 3 and further increase the service life of the insulation layer 3 .
- the outer side of the protective tube 7 can be connected to the second through hole 32 of the thermal insulation layer 3 , and the outer structure of the protective tube 7 is adapted to the structure of the second through hole 32 .
- the structure of the second through hole 32 is circular, and the outer structure of the protective tube 7 is also circular; the structure of the second through hole 32 is pentagonal, and the outer structure of the protective tube 7 is also pentagonal.
- the structure of the third through hole 71 may be circular, quadrangular, pentagonal, or hexagonal, etc., which is not specifically limited in this embodiment of the present application.
- the single crystal furnace may include a flexible hanging piece 81 , one end of the hanging piece 81 may be connected to the lifting device 6 , and the other end of the hanging piece 81 may be used to hang the seal 41 .
- the flexible feature refers to the feature that an object can deform arbitrarily under the action of force, and can maintain the deformation when the force disappears. It can also be interpreted as flexibility, or a characteristic of an object relative to rigidity. Flexibility refers to a physical property that an object deforms after being subjected to a force, and the object itself cannot return to its original shape after the force is lost. After a rigid object is stressed, its shape can be regarded as unchanged from a macroscopic point of view.
- the pendant 81 with flexible features is used to suspend the seal 41.
- the seal 41 In the lowered state, the seal 41 can be attached to the insulation layer 3 by its own gravity, thereby realizing the second through hole 32 of the insulation layer 3. The sealing can improve the sealing effect.
- the pendant 81 has a flexible feature, and is mainly guided freely by the structure of the suspended object and its own gravity. Specifically, the pendant 81 can be bent at will, and the movement track of the lifting sealing member 41 can also be changed arbitrarily. When the pendant 81 is lowered to the limit position, the pendant 81 may not apply any force to the sealing member 41 .
- the pendant 81 may include structures such as soft ropes and chains, which are not specifically limited in this embodiment of the present application.
- the pendant 81 can also be used with a rigid connection plate 82 , as shown in FIG. 1 , one end of the rigid connection plate 82 can be connected to a water pipe, and the pendant 81 can be connected to the other end of the rigid connection plate 82 .
- the lifting device 6 drives the sealing member 41 to switch to the rising state, the sealing member 41 rises, the second through hole 32 is opened, and the feeding device 2 can pass through the first through hole 11 and the second through hole 32, and to Add raw materials in the crucible 5 .
- the lifting device 6 can be switched to the descending state.
- the sealing member 41 is closely tangent to the insulation layer 3 under the action of gravity, and slides downward.
- the lifting device 6 can continue to descend, the pendant 81 can be in a relaxed state, and the sealing member 41 can be in close contact with the insulation layer 3 to achieve the purpose of blocking the second through hole 32 .
- a counterweight 42 may also be provided in the single crystal furnace, and the counterweight 42 may be installed at the end where the sealing member 41 is connected to the hanging member 81 .
- installing a counterweight 42 at the end where the seal 41 is connected to the pendant 81 can increase the weight of the seal 41 and further improve the sealing effect of the seal 41 on the second through hole 32 of the insulation layer 3 .
- the counterweight 42 is a weight that can increase the self-weight of the sealing member 41 and maintain balance.
- the counterweight 42 may include ordinary sand-type counterweight iron or extra-heavy iron, which can be set according to actual needs, which is not specifically limited in this embodiment of the present application.
- the position where the insulation layer 3 is opposite to the sealing member 41 can be provided with a first inclined plane structure 31, and the position where the sealing member 41 is opposite to the insulating layer 3 can be provided with a second inclined plane structure 411;
- the first slope structure 31 and the second slope structure 411 can be bonded together.
- the position where the insulation layer 3 is opposite to the sealing member 41 is the first inclined plane structure 31, and the position where the sealing member 41 is opposite to the insulating layer 3 is the second inclined plane structure 411.
- the sealing member 41 depends on its own gravity and When the insulation layer 3 is bonded, the tightness of bonding is better, and the sealing effect of the sealing member 41 on the second through hole 32 of the insulation layer 3 can be further improved.
- the shapes of the first slope structure 31 and the second slope structure 411 are matched.
- the first slope structure 31 includes a plurality of protrusions, and the second slope structure 411 is provided with a plurality of grooves at positions opposite to the protrusions;
- the first slope structure 31 includes a plurality of grooves, and the second slope structure 411 and the A plurality of protrusions are provided at positions opposite to the protrusions;
- the first slope structure 31 is a planar structure, and the second slope structure 411 may also be a planar structure.
- the specific arrangement manner of the first slope structure 31 and the second slope structure 411 can be set according to actual needs, which is not specifically limited in this embodiment of the present application.
- the first slope structure 31 can be an integral structure, and the second through hole 32 can be a through hole opened on the first slope structure 31; or, the first slope structure 31 can be composed of multiple split structures.
- the second through hole 32 may be disposed between multiple split structures, which is not specifically limited in this embodiment of the present application.
- the first slope structure 31 may include: a first sub-slope structure 311 and a second sub-slope structure 312, and the second through hole 32 may be provided between the first sub-slope structure 311 and the second sub-slope structure 312;
- the lifting device 6 drives the sealing member 41 to switch to the descending state, both the first sub-slope structure 311 and the second sub-slope structure 312 can be attached to the second slope structure.
- both the first sub-slope structure 311 and the second sub-slope structure 312 are attached to the second slope structure, because the second through hole 32 is disposed between the first sub-slope structure 311 and the second sub-slope structure 312, so that the sealing member 41 can seal the second through hole 32 to reduce heat loss.
- the first included angle between the first slope structure 31 and the axis of the thermal insulation layer 3 may be 5° to 15°
- the second angle between the second slope structure 411 and the axis of the thermal insulation layer 3 may be 75°. ⁇ 85°.
- the first included angle is 5-15°, and the second included angle may be 75-85°, so that the bonding effect between the sealing member 41 and the insulation layer 3 is better.
- the first included angle can be 4°, 5°, 10°, 15°, 20°, etc.
- the second included angle can be 70°, 75°, 80°, 85°, 90°, etc., specifically according to The actual requirements are set, and this embodiment of the present application does not specifically limit it.
- the first included angle is 0° and the second included angle is 90°
- the first inclined plane structure 31 and the second inclined plane structure 32 are arranged in parallel, so that the sealing member 41 can face the second side of the side blocking insulation layer 3 directly.
- Through hole 32 a pendant 81 can be used to connect the lifting device and the seal 41 respectively, so that the pendant 81 can drive the seal 41 to rise or fall;
- a hard pendant can also be used to connect the lifting device and the seal 41 respectively, so that the hard pendant can drive The seal 41 is raised or lowered.
- the first included angle is 5° to 15°
- the second included angle is 75° to 85°
- the pendant 81 is used to hang the seal 41 .
- Holes 32 and the use of rigid pendants to connect the seal 41 can reduce consumption by about 20%.
- the feeding device 2 can also include a feeding valve 21, which can be connected to the first through hole 11 and the feeding device 2 respectively; when the feeding valve 21 is opened, the feeding device 2 can pass through the first through hole 11 and the second feeding device.
- the through hole 32 is opposite to the opening of the crucible 5 .
- the feeding valve 21 is connected to the first through hole 11 and the feeding device 2 respectively.
- the feeding valve 21 can be opened, and the feeding device 2 can pass through the first through hole 11 and the second through hole.
- the hole 32 is opposite to the opening of the crucible 5, and feeds into the crucible 5; when no feeding is required, the feeding valve 21 can be closed, effectively isolating the feeding device 2 and the furnace body 1.
- the feeding valve 21 may be an electric control valve or a manual valve, which is not specifically limited in this embodiment of the present application. As shown in Figure 1, a manual valve is shown.
- the feeding device 2 can include a feeding mechanism 22 and a telescopic tube 23, the charging mechanism 22 can be connected with the telescopic tube 23, and the telescopic tube 23 can be connected with the feeding valve 21; the telescopic tube 23 can include a compressed state and an expanded state, and the telescopic tube 23 is switched to the compressed state, it can drive the feeding mechanism 22 to pass through the first through hole 11 and the second through hole 32 to face the opening of the crucible 5 .
- the telescopic tube 23 when the telescopic tube 23 is switched to the compressed state, the telescopic tube 23 can drive the feeding mechanism 22 to pass through the first through hole 11 and the second through hole 32 to be opposite to the opening of the crucible 5, so that the feeding mechanism 22 The raw materials can be introduced into the crucible 5, making feeding more convenient and fast.
- the telescopic tube 23 may be a corrugated tube, or the telescopic tube 23 may also be a sleeve formed by socketing a plurality of tubes, which may be set according to actual needs, which is not specifically limited in this embodiment of the present application.
- the telescopic tube 23 is switched from the expanded state to the compressed state, and the feeding mechanism 22 can pass through the feeding valve 21, the first through hole 11 and the third through hole 71 from the original position in sequence, and deliver the raw material to the crucible 5.
- the telescopic tube 23 is gradually expanded, and when the feeding device 2 withdraws from the second through hole 32 , the sealing member 41 can descend immediately to seal the second through hole 32 .
- the telescopic tube 23 is switched from the telescopic state to the unfolded state, the feeding mechanism 22 can return to the original position, and the feeding valve 21 can be closed.
- the lifting device 6 may include: a driving mechanism and a lifting mechanism, the driving mechanism may be arranged in the furnace body 1, the driving mechanism may be connected with the lifting mechanism, and the lifting mechanism may be connected with the sealing member 41;
- the driving mechanism can be used to drive the lifting mechanism to rise or fall, and the rising or falling of the lifting mechanism can drive the sealing member 41 to switch between the rising state and the falling state.
- the sealing member 41 can be switched between the raised state and the lowered state, and the convenience of use of the sealing member 41 can be improved.
- the lifting device 6 may be disposed close to the sealing member 41 , as shown in FIG. 1 , the lifting device 6 may also be disposed above the sealing member 41 , which is not specifically limited in this embodiment of the present application.
- the single crystal furnace may include a heat exchange mechanism 9, which may be arranged above the crucible 5, and the lifting device 6 is connected to the heat exchange mechanism 9,
- the heat exchange mechanism 9 is connected to the seal 41; the lifting device 6 is used to drive the heat exchange mechanism 9 to rise or fall, and the rise or fall of the heat exchange mechanism 9 drives the seal 41 to switch between the rising state and the falling state.
- the lifting device 6 can drive the heat exchange mechanism 9 to rise or fall, and the rise or fall of the heat exchange mechanism 9 can drive the seal 41 to switch between the rising state and the falling state, so that the heat exchange mechanism 9 and the sealing
- the pieces 41 can share one lifting device 6, which can save the layout space and cost of the single crystal furnace.
- the heat exchange device 9 may be a heat shielding device.
- the lifting device can drive the sealing member to switch to the rising state, so that the charging device can pass through the first through hole on the side of the furnace body and the second through hole on the insulation layer and the The openings of the crucibles are opposite to each other, so that the side feeding of the single crystal furnace can be realized, which can improve the influence of the high-altitude drop feeding on the life of the thermal field.
- the lifting device can also drive the sealing member to switch to the descending state, so that the sealing member can block and protect the second through hole on the heat preservation layer, improve the life of the thermal field, and reduce the temperature loss in the non-feeding condition. Heat energy loss, stabilize the temperature field and air flow balance in the furnace body of the single crystal furnace, reduce the probability of disconnection and polycrystalline growth, and improve the crystal pulling efficiency and quality of single crystal silicon.
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- Engineering & Computer Science (AREA)
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Abstract
Description
Claims (11)
- 一种侧向加料的单晶炉,其中,所述单晶炉包括:炉体、加料装置以及设于所述炉体内的保温层、密封件、坩埚和升降装置,所述保温层位于所述坩埚与所述炉体之间,其中,A single crystal furnace with side feeding, wherein the single crystal furnace includes: a furnace body, a feeding device, and an insulation layer, a seal, a crucible and a lifting device arranged in the furnace body, and the insulation layer is located on the Between the crucible and the furnace body, wherein,所述炉体的侧部开设有第一通孔,所述保温层与所述第一通孔相对的位置开设有第二通孔;A first through hole is opened on the side of the furnace body, and a second through hole is opened at a position opposite to the first through hole in the thermal insulation layer;所述升降装置与所述密封件连接,用于带动所述密封件在上升状态和下降状态之间切换,在所述上升状态下,所述密封件上升,所述加料装置可穿过所述第一通孔和第二通孔与所述坩埚开口处相对,在所述下降状态下,所述密封件下降,所述密封件可密封所述第二通孔。The lifting device is connected with the sealing member, and is used to drive the sealing member to switch between a raised state and a lowered state. In the raised state, the sealing member rises, and the feeding device can pass through the sealing member. The first through hole and the second through hole are opposite to the opening of the crucible. In the descending state, the sealing member descends, and the sealing member can seal the second through hole.
- 根据权利要求1所述的单晶炉,其中,所述单晶炉还包括保护筒,所述保护筒嵌设于所述第二通孔内;The single crystal furnace according to claim 1, wherein the single crystal furnace further comprises a protection tube, and the protection tube is embedded in the second through hole;所述保护筒设有第三通孔,所述第三通孔用于穿设所述加料装置。The protective cylinder is provided with a third through hole, and the third through hole is used for passing through the feeding device.
- 根据权利要求1所述的单晶炉,其中,所述单晶炉包括具有柔性特征的挂件,所述挂件的一端与所述升降装置连接,所述挂件的另一端用于悬挂所述密封件。The single crystal furnace according to claim 1, wherein the single crystal furnace includes a hanging piece with flexible features, one end of the hanging piece is connected with the lifting device, and the other end of the hanging piece is used to hang the sealing member .
- 根据权利要求3所述的单晶炉,其中,所述单晶炉内还设有配重块,所述配重块安装于所述密封件与所述挂件连接的一端。The single crystal furnace according to claim 3, wherein a counterweight is further provided in the single crystal furnace, and the counterweight is installed at the end where the sealing member is connected to the pendant.
- 根据权利要求1所述的单晶炉,其中,所述保温层与所述密封件相对的位置设有第一斜面结构,所述密封件与所述保温层相对的位置设有第二斜面结构;The single crystal furnace according to claim 1, wherein a first slope structure is provided at the position where the insulation layer is opposite to the sealing member, and a second slope structure is provided at a position where the sealing member is opposite to the heat preservation layer ;在所述升降装置带动所述密封件切换至所述下降状态的情况下,所述第一斜面结构和所述第二斜面结构贴合。When the lifting device drives the sealing member to switch to the descending state, the first inclined-plane structure and the second inclined-plane structure are attached.
- 根据权利要求5所述的单晶炉,其中,所述第一斜面结构包括:第一子斜面结构和第二子斜面结构,所述第二通孔设于所述第一子斜面结构和所述第二子斜面结构之间;The single crystal furnace according to claim 5, wherein the first slope structure comprises: a first sub-slope structure and a second sub-slope structure, and the second through hole is provided on the first sub-slope structure and the second through-hole between the second sub-slope structures;在所述升降装置带动所述密封件切换至所述下降状态的情况下,所述第一子斜面结构和所述第二子斜面结构均与所述第二斜面结构贴合。When the lifting device drives the sealing member to switch to the descending state, both the first sub-slope structure and the second sub-slope structure are in contact with the second slope structure.
- 根据权利要求5所述的单晶炉,其中,所述第一斜面结构与所述保 温层的轴线之间的第一夹角为5~15°,所述第二斜面结构与所述保温层的轴线之间的第二夹角为75~85°。The single crystal furnace according to claim 5, wherein, the first included angle between the first slope structure and the axis of the insulation layer is 5-15°, and the second slope structure and the insulation layer The second included angle between the axes is 75-85°.
- 根据权利要求1所述的单晶炉,其中,所述加料装置还包括加料阀,所述加料阀分别与所述第一通孔和所述加料装置连接;The single crystal furnace according to claim 1, wherein the charging device further comprises a charging valve, and the charging valve is respectively connected to the first through hole and the charging device;所述加料阀打开,所述加料装置可穿过所述第一通孔和第二通孔与所述坩埚开口处相对。The feeding valve is opened, and the feeding device can pass through the first through hole and the second through hole to be opposite to the opening of the crucible.
- 根据权利要求8所述的单晶炉,其中,所述加料装置包括加料机构和伸缩管,所述加料机构与所述伸缩管连接,所述伸缩管与所述加料阀连接;The single crystal furnace according to claim 8, wherein the feeding device comprises a feeding mechanism and a telescopic tube, the charging mechanism is connected to the telescopic tube, and the telescopic tube is connected to the feeding valve;所述伸缩管包括压缩状态和展开状态,所述伸缩管切换至所述压缩状态的情况下,可带动所述加料机构穿过所述第一通孔和所述第二通孔与所述坩埚开口处相对。The telescopic tube includes a compressed state and an expanded state. When the telescopic tube is switched to the compressed state, the feeding mechanism can be driven to pass through the first through hole, the second through hole and the crucible. The opening is opposite.
- 根据权利要求1所述的单晶炉,其中,所述升降装置包括:驱动机构和升降机构,所述驱动机构设于所述炉体内,所述驱动机构和所述升降机构连接,所述升降机构与所述密封件连接;The single crystal furnace according to claim 1, wherein the lifting device comprises: a driving mechanism and a lifting mechanism, the driving mechanism is arranged in the furnace body, the driving mechanism is connected to the lifting mechanism, and the lifting mechanism a mechanism is connected to the seal;所述驱动机构用于驱动所述升降机构上升或下降,所述升降机构的上升或下降带动所述密封件在所述上升状态和所述下降状态之间切换。The driving mechanism is used to drive the lifting mechanism to rise or fall, and the rising or falling of the lifting mechanism drives the sealing member to switch between the rising state and the falling state.
- 根据权利要求1所述的单晶炉,其中,所述单晶炉还包括换热机构,所述换热机构设于所述坩埚的上方,所述升降装置与所述换热机构连接,所述换热机构与所述密封件连接;The single crystal furnace according to claim 1, wherein the single crystal furnace further comprises a heat exchange mechanism, the heat exchange mechanism is arranged above the crucible, the lifting device is connected with the heat exchange mechanism, the The heat exchange mechanism is connected with the sealing member;所述升降装置用于驱动所述换热机构上升或下降,所述换热机构的上升或下降带动所述密封件在所述上升状态和所述下降状态之间切换。The lifting device is used to drive the heat exchange mechanism to ascend or descend, and the ascending or descending of the heat exchanging mechanism drives the sealing member to switch between the ascending state and the descending state.
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EP22841383.7A EP4372128A1 (en) | 2021-07-15 | 2022-07-12 | Side-feeding monocrystal furnace |
US18/578,456 US20240287703A1 (en) | 2021-07-15 | 2022-07-12 | Side-feeding monocrystal furnace |
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CN202110800642.XA CN115613122A (en) | 2021-07-15 | 2021-07-15 | Single crystal furnace capable of feeding materials laterally |
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Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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US20120199221A1 (en) * | 2010-08-09 | 2012-08-09 | Sinfonia Technology Co., Ltd. | Raw material loading apparatus |
CN212128337U (en) * | 2020-03-03 | 2020-12-11 | 隆基绿能科技股份有限公司 | Single crystal furnace charging system |
CN113337884A (en) * | 2020-03-03 | 2021-09-03 | 隆基绿能科技股份有限公司 | Single crystal furnace charging system |
CN215800033U (en) * | 2021-07-15 | 2022-02-11 | 隆基绿能科技股份有限公司 | Single crystal furnace capable of feeding materials laterally |
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2021
- 2021-07-15 CN CN202110800642.XA patent/CN115613122A/en active Pending
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2022
- 2022-07-12 US US18/578,456 patent/US20240287703A1/en active Pending
- 2022-07-12 WO PCT/CN2022/105269 patent/WO2023284749A1/en active Application Filing
- 2022-07-12 EP EP22841383.7A patent/EP4372128A1/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20120199221A1 (en) * | 2010-08-09 | 2012-08-09 | Sinfonia Technology Co., Ltd. | Raw material loading apparatus |
CN212128337U (en) * | 2020-03-03 | 2020-12-11 | 隆基绿能科技股份有限公司 | Single crystal furnace charging system |
CN113337884A (en) * | 2020-03-03 | 2021-09-03 | 隆基绿能科技股份有限公司 | Single crystal furnace charging system |
CN215800033U (en) * | 2021-07-15 | 2022-02-11 | 隆基绿能科技股份有限公司 | Single crystal furnace capable of feeding materials laterally |
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