WO2023095849A1 - Procédé de lutte antiparasitaire et aérosol pour la lutte antiparasitaire - Google Patents

Procédé de lutte antiparasitaire et aérosol pour la lutte antiparasitaire Download PDF

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Publication number
WO2023095849A1
WO2023095849A1 PCT/JP2022/043423 JP2022043423W WO2023095849A1 WO 2023095849 A1 WO2023095849 A1 WO 2023095849A1 JP 2022043423 W JP2022043423 W JP 2022043423W WO 2023095849 A1 WO2023095849 A1 WO 2023095849A1
Authority
WO
WIPO (PCT)
Prior art keywords
aerosol
injection
pest control
aerosol composition
screen door
Prior art date
Application number
PCT/JP2022/043423
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English (en)
Japanese (ja)
Inventor
諒平 鈴木
Original Assignee
アース製薬株式会社
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by アース製薬株式会社 filed Critical アース製薬株式会社
Priority to CN202280078298.0A priority Critical patent/CN118302047A/zh
Priority to JP2023520216A priority patent/JP7352050B1/ja
Publication of WO2023095849A1 publication Critical patent/WO2023095849A1/fr
Priority to JP2023146362A priority patent/JP2023158191A/ja

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Classifications

    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
    • A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
    • A01N25/06—Aerosols
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N53/00—Biocides, pest repellants or attractants, or plant growth regulators containing cyclopropane carboxylic acids or derivatives thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01P—BIOCIDAL, PEST REPELLANT, PEST ATTRACTANT OR PLANT GROWTH REGULATORY ACTIVITY OF CHEMICAL COMPOUNDS OR PREPARATIONS
    • A01P7/00—Arthropodicides
    • A01P7/04—Insecticides
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

Definitions

  • the present invention relates to a pest control method and a pest control aerosol, and more particularly to a pest control method and a pest control aerosol for screen doors.
  • Patent Document 1 describes an aerosol composition for repelling pests, which consists of a pest repellent agent for screen doors containing pest repellent components and a propellant.
  • the pest-repellent aerosol composition described in Patent Document 1 is to be continuously sprayed onto the screen door, and is usually sprayed from a relatively short distance from the screen door.
  • the amount of the applied chemical will be uneven, and in order to prevent uneven treatment, it is necessary to move the aerosol up, down, left and right during treatment.
  • liquid dripping and traces may occur, resulting in a decrease in the adhesion efficiency and a feeling of use.
  • an object of the present invention is to provide a pest control method and an aerosol for pest control for a screen door, which can obtain a uniform and sufficient control effect and can reduce the user's burden and excessive spraying.
  • the inventors of the present invention have found that the adhesion rate and uniform adhesion of the pest control component to the screen door can be increased by setting the injection pressure to a predetermined level and by injecting the material from a predetermined distance.
  • the present inventors have found that a constant injection type aerosol that injects a fixed amount of aerosol composition in one injection operation can reduce the burden on the user during treatment and excessive use associated with long-term injection operation.
  • the present invention relates to the following (1) to (4) pest control method and pest control aerosol.
  • a method for controlling insect pests using a metered injection type aerosol that injects a fixed amount of an aerosol composition in one injection operation The aerosol composition comprises a stock solution containing pest control ingredients and a propellant, The injection pressure of the aerosol composition at 25° C. at an injection distance of 5 cm is 5 to 50 gf, Inject from a distance of 20 to 80 cm from the object to be injected, The object to be injected is a screen door, pest control method.
  • a pest control aerosol comprising a pressure container and an aerosol composition filled in the pressure container,
  • the aerosol is a fixed injection type aerosol that injects a fixed amount of the aerosol composition in one injection operation
  • the aerosol composition comprises a stock solution containing pest control ingredients and a propellant
  • the injection pressure of the aerosol composition at 25° C. at an injection distance of 5 cm is 5 to 50 gf
  • the injection target is a screen door, Aerosol for pest control.
  • the pest control aerosol according to (3) which has a plurality of orifices.
  • the pest control method and the pest control aerosol of the present invention it is possible to set a predetermined injection pressure and inject from a predetermined distance. , the adhesion rate and uniform adhesion of the pest control component to the screen door can be enhanced, and a uniform and sufficient pest control effect can be obtained. Furthermore, by making it a fixed injection type aerosol that injects a certain amount of aerosol composition in one injection operation, it is not necessary to move the aerosol during treatment, so the burden on the user during treatment can be reduced, and excessive use can be avoided. can be avoided.
  • the pest-controlling aerosol of the present invention comprises a pressure-resistant container and an aerosol composition filled in the pressure-resistant container.
  • Aerosol compositions consist of a liquid concentrate containing the pest control ingredient and a propellant. Each component will be described below.
  • the pest control component is a component capable of killing, repelling, or knocking down target pests.
  • the type of pest control component is not particularly limited, and known compounds can be used.
  • Pest control ingredients include, for example, permethrin, cyfluthrin, bifenthrin, phenothrin, cyphenothrin, cypermethrin, tralomethrin, pyrethrin, allethrin, phthalthrin, resmethrin, flamethrin, empentrin, prallethrin, imiprothrin, monfluorothrin, transfluthrin, metofluthrin, Pyrethroid compounds such as profluthrin, dimeflutrin and mepafluthrin; organophosphorus compounds such as fenitrothion, dichlorvos, chlorpyrifosmethyl, diazinon and fenthion; carbamate compounds such as carbaryl and propoxur;
  • non-volatile pyrethroid compounds are preferred from the viewpoint of control efficacy and persistence on screen doors, and permethrin, cyfluthrin, bifenthrin, phenothrin, cyphenothrin, cypermethrin, and tralomethrin are particularly preferred.
  • Target pests include, for example, flying pests and crawling pests. Not only that, but also pests belonging to the class Arachnida and Arachnid. Specifically, Diptera flying pests such as mosquitoes, flies, midges, moth flies, mushroom flies, horse flies, black flies, and crane flies; Hemiptera flying pests such as stink bugs, leafhoppers, leafhoppers, and cicadas; ; Isoptera crawling pests such as cockroaches or isoptera flying pests such as termites (ptera); Hymenoptera flying pests such as bees and ants (ptera); insect pests of the order Coleoptera; insect pests of the order Castroptera such as bookworms; flying pests of the order Mayfly such as mayfly;
  • the content of the pest control component is preferably 0.01-70% by mass/volume in the undiluted solution.
  • the lower limit of the content of the pest control component is more preferably 0.1% by mass/volume or more, more preferably 0.3% by mass/volume or more, particularly preferably 0.5% by mass/volume or more, and the upper limit is 65%. It is more preferably 50 mass/volume % or less, particularly preferably 25 mass/volume % or less.
  • the stock solution may contain a solvent for the purpose of adjusting the viscosity of the stock solution, adjusting the particle size of the sprayed particles, and increasing the permeability of the pest-controlling component to pests.
  • solvents include hydrocarbon solvents, alcohol solvents, aromatic solvents, ester solvents, and water.
  • hydrocarbon-based solvents include aliphatic hydrocarbons such as paraffinic hydrocarbons and naphthenic hydrocarbons, and alicyclic hydrocarbons, and kerosene such as JIS No. 1 kerosene is preferred. Specific examples include normal paraffin and isoparaffin.
  • Normal paraffins typically have 8 to 16 carbon atoms, such as Neothiosol manufactured by Sanko Kagaku Kogyo Co., Ltd., for example.
  • Isoparaffins typically have 8 to 16 carbon atoms, such as IP Clean LX manufactured by Idemitsu Kosan Co., Ltd., and the like.
  • alcohol solvents include lower alcohols such as ethanol and propanol (normal, iso), and polyhydric alcohols such as glycerin and ethylene glycol.
  • aromatic solvents include toluene and xylene.
  • ester solvents include isopropyl myristate, hexyl laurate, isopropyl palmitate and the like. These may be used individually by 1 type, and may be used in combination of 2 or more type. Among these, lower alcohols are preferred from the viewpoint of adjusting the particle size of the sprayed particles reaching the screen door.
  • the content of the solvent is preferably 30 to 99.99% by mass/volume in the stock solution.
  • the content of the solvent is 30% by mass/volume or more in the stock solution, the uniform diffusibility of the sprayed particles can be improved, and when it is 99.99% by mass/volume or less, a sufficient pest control effect can be obtained. It is preferable because it can be secured.
  • the lower limit of the solvent content is more preferably 35% by mass/volume or more, more preferably 50% by mass/volume or more, and the upper limit is more preferably 99.9% by mass/volume or less, 99.5% by mass. /% by volume or less is more preferable.
  • the stock solution can contain other ingredients as long as the effects of the present invention are not impaired.
  • Other components include, for example, fragrances, deodorants, disinfectants, bactericides, preservatives, pH adjusters, ultraviolet absorbers, inorganic substances, surfactants, dissolution aids, and the like.
  • the content of the stock solution in the aerosol composition can be appropriately changed according to the purpose of use of the metered dose aerosol and the combination with the propellant, and is not particularly limited. can be When the stock solution is 1% by volume or more in the aerosol composition, a sufficient pest control effect can be obtained, and when it is 50% by volume or less, the uniform diffusion of the sprayed particles is improved, and liquid drips and marks on the screen door. The rest can be suppressed.
  • the content of the stock solution in the aerosol composition is more preferably 3% by volume or more, more preferably 5% by volume or more, and more preferably 40% by volume or less, and 30% by volume. More preferred are:
  • the propellant is a medium for injecting the stock solution, and is pressure-filled into the pressure-resistant container together with the stock solution.
  • the propellant include liquefied petroleum gas (LPG) such as propane, propylene, n-butane and isobutane, liquefied gas such as dimethyl ether (DME), compressed gas such as carbon dioxide, nitrogen gas, and compressed air, and HFC-152a. , HFC-134a, HFO-1234yf, HFO-1234ze, and other halogenated carbon gases.
  • LPG liquefied petroleum gas
  • DME dimethyl ether
  • the content of the propellant in the aerosol composition can be appropriately changed according to the purpose of use of the metered dose aerosol and the combination with the stock solution, and is not particularly limited.
  • the propellant is 99% by volume or less, a sufficient pest control effect can be obtained.
  • the lower limit of the propellant content in the aerosol composition is more preferably 60% by volume or more, more preferably 70% by volume or more, and the upper limit is more preferably 97% by volume or less, and 95% by volume or less. More preferred.
  • the volume ratio of the stock solution to the propellant in the aerosol composition is preferably 1:99 to 50:50, more preferably 3:97 to 40:60, even more preferably 5:95 to 30:70. . With such a volume ratio, a sufficient pest control effect can be obtained.
  • the pest-controlling aerosol of the present invention comprises a pressure-resistant container and the aerosol composition filled in the pressure-resistant container.
  • the pressure container has its opening closed by an aerosol valve.
  • the pest-controlling aerosol of the present invention is also a metered-dose aerosol that injects a fixed amount of the aerosol composition in one injection operation.
  • a fixed quantity injection type aerosol is a spray member attached to an aerosol valve (hereinafter also referred to as a spray button) that is operated by the user to pass through the aerosol valve and spray a fixed amount of the aerosol composition in a pressure container.
  • the stock solution is granulated by a propellant and sprayed as spray particles.
  • the aerosol valve includes an opening/closing member for switching between communication and disconnection between the inside and the outside of the pressure vessel when the injection member is operated by the user, a housing to which the opening/closing member is attached, and the housing at a predetermined position in the pressure vessel.
  • a mounting member is provided for holding.
  • the opening/closing member includes a stem that slides up and down in conjunction with the injection member. By sliding the stem, communication (injection state) and blocking (non-injection state) of the aerosol composition are switched.
  • the aerosol valve is formed with a housing hole for taking in the aerosol composition from the pressure container and a stem hole for sending the taken in aerosol composition to the injection member.
  • the path from the housing bore to the stem bore constitutes an internal passageway through which the aerosol composition passes.
  • the aerosol valve is a fixed quantity type aerosol valve that performs a fixed quantity injection by operating the injection member once.
  • the injection amount of the aerosol valve is a predetermined constant amount, preferably in the range of 0.1 to 4.0 mL, more preferably in the range of 0.2 to 2.0 mL, in one injection operation. By setting the injection amount within such a range, the amount of the pest control component adhering to the screen door can be increased. If the injection amount of the aerosol valve is within the above range, a predetermined injection amount can be appropriately set.
  • injection member is a member attached to the pressure container via the aerosol valve.
  • the injection button is formed with a passage in the operation part through which the aerosol composition taken in from the pressure container passes through the stem hole of the aerosol valve, and a nozzle hole through which the aerosol composition is injected.
  • the injection button may be a button type that is pressed from above, or may be a trigger type from the viewpoint of operability.
  • the inner diameter of the injection hole of the injection button is preferably ⁇ 0.45 to 3.0 mm, more preferably ⁇ 0.5 to 2.0 mm, and ⁇ 0. 6 to 1.6 mm is more preferred.
  • the pest-controlling aerosol of the present invention may have a plurality of nozzle holes. Having a plurality of nozzle holes is preferable because it is possible to inject the medicine over a wide range and it is easy to prevent the medicine from passing through the mesh of the screen door. When a plurality of nozzle holes are provided, it is preferable that the inner diameters of the respective nozzle holes (orifice diameters) are the same.
  • the number of nozzle holes is preferably 1-6, more preferably 2-5.
  • the aerosol pressure container is filled with the aerosol composition as described above, and the injection member is operated to inject a certain amount of the aerosol composition in one operation.
  • the pest-controlling aerosol of the present invention has an injection pressure of 5 to 50 gf, preferably 10 to 30 gf, and particularly preferably 12 to 25 gf at 25° C. at an injection distance of 5 cm. If the injection pressure at 5 cm from the nozzle is 5 gf or more, the aerosol composition can adhere sufficiently to the screen door, and if it is 50 gf or less, the aerosol composition can adhere without passing through the mesh of the screen door. By setting the injection pressure in the vicinity of the injection port within the above range, the amount of the insect-controlling component adhered to the screen door can be increased.
  • the jet pressure of the aerosol composition at 25°C at a jet distance of 30 cm is preferably 1 to 30 gf, more preferably 2 to 20 gf, and particularly preferably 3 to 15 gf. If the injection pressure at 30 cm from the nozzle is 1 gf or more, the aerosol composition can reach up to about 60 cm. By setting the injection pressure in the vicinity of the screen door within the above range, the aerosol composition can be efficiently adhered to the screen door at a distance of about 60 cm.
  • the injection pressure was measured at a distance of 5 cm or 30 cm from the pest control aerosol nozzle at a room temperature of 25 ° C.
  • a digital force gauge for example, manufactured by Imada Co., Ltd., model number: DS2-2N
  • the method of adjusting the injection pressure includes, for example, changing the gas pressure according to the type of propellant, changing the diameter and shape of the nozzle hole of the button, adjusting the diameter of the valve stem, and adjusting the ratio of the undiluted solution to the propellant. change.
  • the gas pressure can be appropriately changed according to the purpose of use of the metered injection type aerosol and the combination with the propellant, and is not particularly limited. If the internal pressure is 0.35 MPa or more, ejection failure is unlikely to occur, and if the internal pressure is 0.55 MPa or less, it is possible to suppress the medicine from passing through the mesh of the screen door.
  • the pest control aerosol in the present invention should have an average particle size (D50) of 10 to 50 ⁇ m at a spray distance of 60 cm under conditions of 25° C. from the viewpoint of improving diffusivity and uniformly treating the screen door. It is preferably 10 to 40 ⁇ m, even more preferably 10 to 30 ⁇ m.
  • the average particle size of the aerosol composition can be measured using a laser particle size distribution analyzer (for example, "LDSA-1400A” manufactured by Microtrac Bell Co., Ltd.).
  • the average particle size of the aerosol composition can be adjusted by changing the gas pressure depending on the type of propellant, changing the diameter and shape of the button orifice, changing the ratio of the stock solution to the propellant, and the like.
  • the pest control method of the present invention uses the aerosol for controlling pests of the present invention, which is a metered injection type aerosol, and injects a fixed amount of the aerosol composition onto a screen door, which is an object to be sprayed, to efficiently repel pests approaching the screen door. It can be controlled.
  • the spray is applied from a distance of 20 to 80 cm, preferably 30 to 70 cm, particularly preferably 40 to 60 cm, from the screen door to be sprayed.
  • the sprayed aerosol composition is sufficiently dispersed in the form of particles when it reaches the screen door, so that the aerosol composition can be uniformly adhered to the mesh.
  • a mesh of 18 to 30 mesh is preferable from the viewpoint of improving the uniform adhesion of the sprayed particles.
  • the injection amount of the insect pest control component to the screen door is preferably 1 mg or more, more preferably 20 mg or more, particularly preferably 60 mg or more, and preferably 100 mg or less, from the viewpoint of obtaining a sufficient pest control effect and suppressing contamination of the screen door. , 80 mg or less.
  • the amount of the pest control component attached to the screen door is preferably 1 mg/m 2 or more, more preferably 20 mg/m 2 or more, particularly preferably 60 mg/m 2 or more, and preferably 100 mg/m 2 or less, and 80 mg/m 2 or more. m 2 or less is more preferable.
  • the aerosol composition can be uniformly and sufficiently adhered to the mesh by injecting a fixed amount of the aerosol composition onto the screen door from a specific injection distance at a specific injection pressure. Pest control effect can be obtained, and the user's burden during processing and overuse can be reduced.
  • Each stock solution was filled in an aerosol pressure container (capacity: 100 mL), and the aerosol pressure container was closed with an aerosol valve (one injection amount: 1 mL). Subsequently, liquefied petroleum gas (0.45 MPa (25° C.)) was filled under pressure as a propellant. The total filling amount of the stock solution and the propellant was 90 mL, and the filling ratio (v/v%) was as shown in Table 2 below.
  • An injection button (hole diameter ⁇ 1 mm, number of injection holes shown in Table 2 below) was attached to the aerosol valve, and quantitative injection type aerosol products of specimens 1 to 8 having performance shown in Table 2 below were obtained. The method of measuring each performance is as described later.
  • the injection pressure of the aerosol composition at 25 ° C. and the injection distance of 5 cm was measured from a circular flat plate with a diameter of ⁇ 60 mm attached to a digital force gauge (manufactured by Imada Co., Ltd., model number: DS2-2N) from a distance of 5 cm from the nozzle of the aerosol product.
  • the maximum value was measured when the aerosol composition was sprayed toward the center, and the average value of three measurements was obtained.
  • the injection pressure of the aerosol composition at 25° C. and the injection distance of 30 cm was measured in the same manner as described above, except that the distance from the nozzle of the aerosol product was 30 cm.
  • the average particle size of the aerosol composition at 25° C. was measured at a position of 60 cm using a laser particle size distribution analyzer (“LDSA-1400A” manufactured by Microtrack Bell Co., Ltd.).
  • the measurement method was auto-start averaging (3 times of averaging, interval of 0.60 ms), and the measurement was performed by calculating the average value of 5 times.
  • Examples 9-13, Comparative Examples 1-2 Efficacy test for stink bugs> (1) A metered injection type aerosol product of sample 1 was sprayed once toward the center of a 30 cm x 30 cm screen door (manufactured by Dio Kasei Co., Ltd., 20 mesh) from distances of 10 cm, 60 cm, and 100 cm.
  • Example 14 to 20 Efficacy test for stink bugs> An efficacy test against stink bugs was conducted in the same manner as in Example 11 or 12, except that the metered-dose aerosol product of Sample 1 was replaced with the metered-dose aerosol product of each sample shown in Table 4 below. The test was repeated three times, and the average drop time was obtained. The results are shown in Table 4 below.

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  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Environmental Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Zoology (AREA)
  • Engineering & Computer Science (AREA)
  • Agronomy & Crop Science (AREA)
  • Dentistry (AREA)
  • Dispersion Chemistry (AREA)
  • Toxicology (AREA)
  • Insects & Arthropods (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Catching Or Destruction (AREA)

Abstract

La présente invention concerne un procédé de lutte antiparasitaire destiné à lutter contre les parasites à l'aide d'un aérosol de type à pulvérisation dosée pour pulvériser une quantité fixe d'une composition d'aérosol par pulvérisation, la composition d'aérosol comprenant une solution mère contenant un ingrédient de lutte antiparasitaire et un agent propulseur, la pression de pulvérisation de la composition d'aérosol à 25 °C étant de 5 à 50 gf à une distance de pulvérisation de 5 cm, la pulvérisation étant réalisée à une distance de 20 à 80 cm à partir d'une cible de pulvérisation, et la cible de pulvérisation étant une fenêtre à moustiquaire.
PCT/JP2022/043423 2021-11-26 2022-11-24 Procédé de lutte antiparasitaire et aérosol pour la lutte antiparasitaire WO2023095849A1 (fr)

Priority Applications (3)

Application Number Priority Date Filing Date Title
CN202280078298.0A CN118302047A (zh) 2021-11-26 2022-11-24 害虫防治方法和害虫防治用气溶胶
JP2023520216A JP7352050B1 (ja) 2021-11-26 2022-11-24 網戸用害虫防除方法および網戸用害虫防除用エアゾール
JP2023146362A JP2023158191A (ja) 2021-11-26 2023-09-08 害虫防除方法および害虫防除用エアゾール

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2021-192385 2021-11-26
JP2021192385 2021-11-26

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WO2023095849A1 true WO2023095849A1 (fr) 2023-06-01

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WO (1) WO2023095849A1 (fr)

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH11315002A (ja) * 1998-01-21 1999-11-16 Earth Chem Corp Ltd 網戸用スプレ―
WO2011065413A1 (fr) * 2009-11-25 2011-06-03 株式会社ダイゾー Buse de pulvérisation et produit d'aérosol
JP2013126959A (ja) * 2011-12-17 2013-06-27 Dainippon Jochugiku Co Ltd ガラス面ならびに網戸用の飛翔害虫防除用エアゾール
JP2014005271A (ja) * 2012-05-31 2014-01-16 Dainippon Jochugiku Co Ltd 害虫防除用マイクロエマルジョン組成物及びこれを用いた害虫防除用製品
JP2020152728A (ja) * 2018-12-14 2020-09-24 大日本除蟲菊株式会社 害虫、ダニ防除方法、及び害虫、ダニ防除用エアゾール
JP2021075526A (ja) * 2019-11-08 2021-05-20 大日本除蟲菊株式会社 害虫、ダニ防除方法、及び害虫、ダニ防除用エアゾール

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH11315002A (ja) * 1998-01-21 1999-11-16 Earth Chem Corp Ltd 網戸用スプレ―
WO2011065413A1 (fr) * 2009-11-25 2011-06-03 株式会社ダイゾー Buse de pulvérisation et produit d'aérosol
JP2013126959A (ja) * 2011-12-17 2013-06-27 Dainippon Jochugiku Co Ltd ガラス面ならびに網戸用の飛翔害虫防除用エアゾール
JP2014005271A (ja) * 2012-05-31 2014-01-16 Dainippon Jochugiku Co Ltd 害虫防除用マイクロエマルジョン組成物及びこれを用いた害虫防除用製品
JP2020152728A (ja) * 2018-12-14 2020-09-24 大日本除蟲菊株式会社 害虫、ダニ防除方法、及び害虫、ダニ防除用エアゾール
JP2021075526A (ja) * 2019-11-08 2021-05-20 大日本除蟲菊株式会社 害虫、ダニ防除方法、及び害虫、ダニ防除用エアゾール

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JP2023158191A (ja) 2023-10-26
JPWO2023095849A1 (fr) 2023-06-01
CN118302047A (zh) 2024-07-05
JP7352050B1 (ja) 2023-09-27

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