WO2022127431A1 - Differential-pressure antigravity filling and solidifying device under action of external field and process method - Google Patents
Differential-pressure antigravity filling and solidifying device under action of external field and process method Download PDFInfo
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- WO2022127431A1 WO2022127431A1 PCT/CN2021/128992 CN2021128992W WO2022127431A1 WO 2022127431 A1 WO2022127431 A1 WO 2022127431A1 CN 2021128992 W CN2021128992 W CN 2021128992W WO 2022127431 A1 WO2022127431 A1 WO 2022127431A1
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- 230000008569 process Effects 0.000 title claims abstract description 32
- 238000005266 casting Methods 0.000 claims abstract description 68
- 239000000155 melt Substances 0.000 claims abstract description 44
- 230000006698 induction Effects 0.000 claims abstract description 43
- 238000003756 stirring Methods 0.000 claims abstract description 36
- 238000003723 Smelting Methods 0.000 claims abstract description 27
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- 230000005672 electromagnetic field Effects 0.000 claims abstract description 11
- 239000007788 liquid Substances 0.000 claims abstract description 10
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 52
- 238000007711 solidification Methods 0.000 claims description 41
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- 238000002844 melting Methods 0.000 claims description 35
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- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 7
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- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 4
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D18/00—Pressure casting; Vacuum casting
- B22D18/04—Low pressure casting, i.e. making use of pressures up to a few bars to fill the mould
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D18/00—Pressure casting; Vacuum casting
- B22D18/06—Vacuum casting, i.e. making use of vacuum to fill the mould
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D27/00—Treating the metal in the mould while it is molten or ductile ; Pressure or vacuum casting
- B22D27/02—Use of electric or magnetic effects
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D27/00—Treating the metal in the mould while it is molten or ductile ; Pressure or vacuum casting
- B22D27/15—Treating the metal in the mould while it is molten or ductile ; Pressure or vacuum casting by using vacuum
Definitions
- the invention relates to the technical field of low-pressure casting, in particular, to a differential pressure anti-gravity mold filling and solidification device and a process method under the action of an external field.
- Low pressure casting technology is a casting technology between pressure casting and gravity casting, mainly used in low pressure casting of non-ferrous metals.
- the technology has the advantages of high raw material utilization, less casting defects, less oxide inclusions, high dimensional accuracy, and easy adjustment of the casting speed.
- the casting obtained by the low pressure casting method has poor uniformity of solidification structure and coarse grains, which seriously reduces the performance of the casting.
- Grain refinement treatment is an important method to improve the performance of castings.
- Al-Ti alloy or Al-Ti-B alloy grain refiners are generally used in the industry, which can reduce the hot cracking and segregation tendency of the castings while refining the grains and reduce the porosity. Rate.
- the existing process is characterized by adding Al-Sr intermediate alloy, mixed rare earth (Re) and Al-Zr intermediate alloy to the aluminum alloy melt in the tundish for modification and refinement treatment to improve product quality.
- Re mixed rare earth
- Al-Zr intermediate alloy mixed rare earth
- the refiner is extremely sensitive to factors such as melt temperature, treatment time, and addition method, the refining effect is quite different, and the addition of alloying elements increases the production cost, changes the alloy composition, and affects the recycling of the alloy.
- stirring the melt is a method to improve the performance of castings; the traditional mechanical stirring process is simple, but because the stirrer is in direct contact with the melt, it is easy to contaminate the melt under the action of friction stirring for a long time; the existing The electromagnetic stirring method uses a steady and constant magnetic field to increase the subcooling degree of the metal melt, thereby increasing the nucleation rate and refining the solidification structure, but the strong magnetic field equipment is expensive and complicated, the pouring process requires high temperature control, and the steady and constant magnetic field cannot remove the molten metal. Gases and inclusions in the body.
- the existing low-pressure casting technology has the technical problems that impurities and gas cannot be completely removed and cannot be completely stirred, and a differential pressure anti-gravity filling and solidification device and process method under the action of an external field are provided.
- the invention mainly utilizes the vacuum and electromagnetic coupling external field processing device and the differential pressure anti-gravity filling and solidification method, by applying electromagnetic field and vacuum field to the melt, so as to effectively remove the gas in the melt, promote the floating of inclusions, and obtain The effect of uniform and fine casting structure.
- a differential pressure anti-gravity filling and solidification device under the action of an external field is characterized in that it comprises: a solidification cavity, a high pressure part, a low pressure part and a vacuum part, the solidification cavity comprises: an upper cavity and a lower cavity, the The upper cavity is provided with a casting mold, the upper cavity and the lower cavity are connected by an intermediate plate, and an infusion tube is arranged between the upper cavity and the lower cavity, and the infusion tube passes through the intermediate plate
- the lower end of the lower cavity is provided with a hydraulic lifting platform, the upper end of the hydraulic lifting platform is provided with a melting crucible, the bottom of the lower cavity is provided with an induction melting device, and the upper end of the induction melting device is provided with an electromagnetic a stirring device, the lower cavity is provided with an induction electric inlet at the corresponding position of the electromagnetic stirring device and the induction melting device;
- the high pressure part includes a constant pressure high pressure tank and a valved air duct, the constant pressure high pressure tank The lower ends of the upper
- the air pipe is connected to the upper cavity;
- the vacuum part includes a vacuum pump, a vacuum tank and a valved air pipe, the vacuum pump is connected to the vacuum tank, and the vacuum tank is connected to the valve through the valved air pipe The lower end of the upper cavity and the upper end of the lower cavity.
- the material of the water cooling jacket of the electromagnetic stirring device is austenitic stainless steel; the upper end of the lower cavity is provided with a quartz glass observation hole.
- the present invention also provides a solidification process of a differential pressure anti-gravity filling solidification device under the action of an external field, characterized in that the solidification process steps include:
- Step S1 put the aluminum alloy raw material or the intermediate alloy of pure aluminum and related elements into the smelting crucible after drying and removing surface impurities, start the induction melting device to melt the raw material into liquid, and then use the hydraulic lifting platform to melt the raw material into a liquid.
- the smelting crucible is lifted up, metamorphic agent is used for metamorphism, and high-purity argon gas with a purity greater than 99.99% is used for degassing, and then slag removal is carried out;
- Step S2 After slag removal, use the hydraulic lifting platform to lower the melting crucible to the induction melting device, close the middle plate, install the infusion pipe, the mold and the upper cavity, and then pump vacuum;
- Step S3 start the induction smelting device to raise the molten metal to a predetermined temperature and keep it isothermally for a period of time;
- Step S4 using the hydraulic lifting platform to lift the smelting crucible to the external field action area, start the electromagnetic field to process the melt, deeply remove the gas in the melt, and maintain the uniformity of alloy composition and melt temperature;
- Step S5 After the external field acts for a certain period of time, stop the electromagnetic stirring, let it stand for a period of time, and then use the constant pressure high-pressure tank to pass high-purity argon gas with a purity greater than 99.99% into the upper cavity and the lower cavity at the same time ;
- Step S6 use the constant-pressure low-pressure tank to decompress the upper cavity, and use the argon pressure difference between the lower cavity and the upper cavity to pour aluminum alloy melt into the mold for casting , the casting time is 10-25s, and the pressure holding time is 5-15min; after the melt solidifies to form a casting, the pressure is relieved, and the upper cavity is opened to take out the casting.
- Al-Ti-B, Al-Sr or Al-RE master alloy may be used as the alloy melt modifier in step S1.
- Aluminum alloys such as ZL114A, ZL205A, ZL104A, ZL101, A356 and A357 can be used as aluminum alloys.
- step S2 the degree of vacuum is 10-40Pa.
- step S3 the isothermal standing time of the aluminum alloy melt under the vacuum condition is 18-25 min.
- step S4 when the melt reaches 80-100°C above TL, the electromagnetic stirring device is started to electromagnetically stir the melt, the central magnetic induction intensity is 0-30 mT, and the electromagnetic field action time is 1-5 min.
- the present invention has the following advantages:
- a differential pressure anti-gravity filling and solidification device and a process method under the action of an external field provided by the present invention utilize the induced current generated by the electromagnetic field to cut the molten metal during the differential pressure anti-gravity filling and solidification process, which is generated in the metal melt. Electromagnetic force promotes the forced convection of the melt, makes the solute distribution more uniform at the temperature of the melt, and strengthens nucleation and dissociation. The application of magnetic field and vacuum field during the casting process will not introduce other impurities, which is an ideal improvement. Methods of casting quality.
- the differential pressure antigravity mold filling and solidification device and process method provided by the present invention introduce electromagnetic fields and vacuum fields during the differential pressure antigravity mold filling and solidification process, which does not affect the existing casting conditions and processes, and the equipment is simple , easy to operate, with the advantages of strong process adaptability, convenience and flexibility, low porosity of castings, and high mechanical properties, suitable for the forming and industrial production of large and medium-sized aluminum alloy castings.
- the differential pressure anti-gravity filling and solidification device and process method provided by the present invention organically combine non-vacuum alloy smelting, metamorphism and preliminary degassing refining with vacuum field and electromagnetic field coupling deep refining to realize large-volume aluminum alloys.
- the deep refining of alloy melt is very beneficial for improving the compactness of large and complex aluminum alloy casting products.
- the present invention can be widely promoted in the fields of low pressure casting technology and the like.
- FIG. 1 is a schematic structural diagram of a differential pressure antigravity filling and solidification device and a process method under the action of an external field of the present invention.
- Fig. 2 is a schematic diagram of the position of the crucible during smelting, metamorphism and degassing under non-vacuum conditions of a differential pressure antigravity filling and solidification device and a process method under the action of an external field of the present invention.
- FIG 3 is a schematic diagram of the position of the crucible during the deep purification of the melt under the vacuum condition of a differential pressure antigravity filling and solidification device and a process method under the action of an external field of the present invention.
- orientation words such as “front, rear, top, bottom, left, right", “horizontal, vertical, vertical, horizontal” and “top, bottom” etc.
- positional relationship is usually based on the orientation or positional relationship shown in the drawings, which is only for the convenience of describing the present invention and simplifying the description, and these orientation words do not indicate or imply the indicated device or element unless otherwise stated. It must have a specific orientation or be constructed and operated in a specific orientation, so it should not be construed as a limitation on the scope of protection of the present invention: the orientation words “inside and outside” refer to the inside and outside relative to the contour of each component itself.
- spatially relative terms such as “on”, “over”, “on the surface”, “above”, etc., may be used herein to describe what is shown in the figures.
- spatially relative terms are intended to encompass different orientations of the device in use or operation in addition to the orientation depicted in the figures. For example, if the device in the figures is turned over, elements described as “above” or “over” other devices or features would then be oriented “below” or “over” the other devices or features under its device or structure".
- the exemplary term “above” can encompass both an orientation of "above” and “below.”
- the device may also be otherwise oriented (rotated 90 degrees or at other orientations) and the spatially relative descriptions used herein interpreted accordingly.
- the present invention provides a differential pressure anti-gravity filling and solidification device under the action of an external field, including: a solidification cavity, a high pressure part, a low pressure part and a vacuum part, and the solidification cavity includes: an upper cavity
- the upper cavity 1 and the lower cavity 12 are provided with a casting mold 2, and the upper cavity 1 and the lower cavity 12 are connected by the intermediate plate 4; the upper cavity 1 and the lower cavity
- An infusion pipe 5 is arranged between 12, and the infusion pipe 5 passes through the center of the intermediate plate 4; the lower end of the lower cavity 12 is provided with a hydraulic lifting platform 10, and the hydraulic lifting platform 10 passes through the position control device 11.
- the upper end of the hydraulic lifting platform 10 is provided with a melting crucible 7; the bottom of the lower cavity 12 is provided with an induction melting device 9, and the induction melting device can be an induction heating device, such as an induction heating coil;
- the upper end of the smelting device 9 is provided with an electromagnetic stirring device 8 , and the material of the water cooling jacket of the electromagnetic stirring device 8 is austenitic stainless steel; the lower cavity 12 is located between the electromagnetic stirring device 8 and the induction melting device 9 .
- the high-pressure part includes a constant-pressure high-pressure tank 14 and a valved air conduit, and the constant-pressure high-pressure tank 14 is connected to the upper cavity 1 and the valved air conduit through the valved air conduit.
- the vacuum part includes a vacuum pump 15, a vacuum tank 16, and the valved gas conduit. The vacuum pump 15 is connected to the vacuum tank 16, and the vacuum tank 16 is connected to the upper cavity 1 through the valved gas conduit.
- the lower end of the lower chamber 12 and the upper end of the lower chamber 12; the upper end of the lower chamber 12 is provided with a quartz glass observation hole 6; the constant pressure high pressure tank 14 is filled with high pressure argon; the constant pressure low pressure tank 18 is Low pressure argon.
- the present invention also provides a solidification process of a differential pressure anti-gravity filling solidification device under the action of an external field, characterized in that the solidification process steps include:
- Step S1 put the aluminum alloy raw material or the intermediate alloy of pure aluminum and related elements into the melting crucible 7 after drying and removing surface impurities, start the induction melting device 9 to melt the raw material into liquid, and then use the hydraulic lifting platform 10 lift the smelting crucible 7, use a metamorphic agent for metamorphism, use high-purity argon with a purity greater than 99.99% to rotate and spray for degassing, and then carry out slag removal;
- Step S2 After removing the slag, use the hydraulic lifting platform 10 to lower the melting crucible 7 to the induction melting device 9, close the middle plate 4, install the infusion pipe 5, the casting mold 2 and the After the upper cavity is evacuated;
- Step S3 start the induction smelting device 9 to raise the molten metal to a predetermined temperature and keep it isothermally for a period of time;
- Step S4 using the hydraulic lifting platform 10 to lift the smelting crucible 7 to the external field action area, start the electromagnetic field to process the melt, deeply remove the gas in the melt, and maintain the uniformity of alloy composition and melt temperature;
- Step S5 After the external field acts for a certain period of time, stop the electromagnetic stirring, let it stand for a period of time, and then use the constant pressure high-pressure tank 14 to simultaneously pass the upper cavity 1 and the lower cavity 12 into the high purity greater than 99.99%. pure argon;
- Step S6 use the constant pressure low pressure tank 18 to decompress the upper cavity 1, and use the argon pressure difference between the lower cavity 12 and the upper cavity 1 to inject aluminum alloy melt into the Casting mold 2 is cast, the casting time is 10-25s, and the pressure holding time is 5-15min; after the melt solidifies to form a casting, the pressure is relieved, and the upper cavity is opened to take out the casting.
- Al-Ti-B, Al-Sr or Al-RE master alloy may be used as the alloy melt modifier in step S1.
- the aluminum alloy can be aluminum alloys such as ZL114A, ZL205A, ZL104A, ZL101, A356 and A357; the vacuum degree in step S2 is 10-40Pa; the isothermal standing time of the aluminum alloy melt under vacuum conditions in step S3 is 18-25min; step S4 When the melt reaches 80-100°C above TL, start the electromagnetic stirring device 8 to electromagnetically stir the melt, the central magnetic induction intensity is 0-30mT, and the electromagnetic field action time is 1-5min.
- the alternating rotating magnetic field is used to promote forced convection of the ZL114A aluminum alloy melt, which uniformizes the melt temperature field, strengthens the nucleation and dissociation of the crystal nucleus, realizes the grain refinement of the casting structure, and reduces the inclusions.
- the deep purification of ZL114A aluminum alloy melt was realized by using vacuum field and electromagnetic long coupling effect, and the casting performance was improved.
- the alternating rotating magnetic field is used to promote forced convection of the ZL104A and A357 aluminum alloy melts, which uniformizes the melt temperature field, strengthens the nucleation and dissociation of the crystal nucleus, realizes the grain refinement of the casting structure, and reduces the inclusions.
- the deep purification of ZL104A aluminum alloy melt was realized by using the vacuum field and electromagnetic long coupling effect, and the performance of the casting was improved.
- the alternating rotating magnetic field is used to promote forced convection of the ZL101 and A356 aluminum alloy melts, which uniformizes the melt temperature field, strengthens the nucleation and dissociation of the crystal nucleus, realizes the grain refinement of the casting structure, and reduces the inclusions.
- the deep purification of ZL101 and A356 aluminum alloy melts was realized by using the vacuum field and electromagnetic long-coupling, and the performance of the castings was improved.
Abstract
Provided are a differential-pressure antigravity filling and solidifying device under the action of an external field and a process method. The device comprises a solidifying cavity, a high-pressure portion, a low-pressure portion and a vacuum portion, wherein the solidifying cavity comprises an upper cavity and a lower cavity; a casting mould is arranged in the upper cavity; the upper cavity and the lower cavity are connected by means of an intermediate plate; a liquid delivery pipe is arranged between the upper cavity and the lower cavity and passes through the center of the intermediate plate; a hydraulic lifting platform is arranged at a lower end of the lower cavity, and a smelting crucible is arranged at an upper end of the hydraulic lifting platform; an induction smelting device is arranged at the bottom of the lower cavity; an electromagnetic stirring device is arranged at an upper end of the induction smelting device; and the lower cavity is provided with an induced electricity inlet in a position corresponding to the electromagnetic stirring device and the induction smelting device. The present invention mainly utilizes a vacuum and electromagnetic-coupling external field processing device and a differential-pressure anti-gravity filling and solidifying method therefor, and applies an electromagnetic field and a vacuum field to a melt, thus achieving the effects of effectively removing gases in the melt, promoting the floating of inclusions, and obtaining a uniform fine casting structure.
Description
本发明涉及低压铸造技术领域,具体而言,尤其涉及一种外场作用下差压反重力充型凝固装置及工艺方法。The invention relates to the technical field of low-pressure casting, in particular, to a differential pressure anti-gravity mold filling and solidification device and a process method under the action of an external field.
低压铸造技术是一种介于压力铸造和重力铸造之间的一种铸造技术,主要应用于有色金属低压铸造。该技术具有原料利用率高,铸件缺陷少,氧化夹杂物少,尺寸精度高,浇铸速度便于调节等优点。但是,通过低压铸造法获得的铸件,其凝固组织均匀性较差,晶粒较粗大,从而严重降低了铸件性能。Low pressure casting technology is a casting technology between pressure casting and gravity casting, mainly used in low pressure casting of non-ferrous metals. The technology has the advantages of high raw material utilization, less casting defects, less oxide inclusions, high dimensional accuracy, and easy adjustment of the casting speed. However, the casting obtained by the low pressure casting method has poor uniformity of solidification structure and coarse grains, which seriously reduces the performance of the casting.
晶粒细化处理是提高铸件性能的重要方法。对于应用最为广泛的铝合金铸件,行业内一般使用Al-Ti合金或Al-Ti-B合金晶粒细化剂,在细化晶粒的同时也可以减轻铸件的热裂和偏析倾向,降低气孔率。现有的工艺特点为在中间包内向铝合金熔体添加Al-Sr中间合金、混合稀土(Re)和Al-Zr中间合金作变质、细化处理,提高产品质量。但是由于细化剂对熔体温度、处理时间、加入方式等因素极其敏感,使细化效果出现较大差异,且合金元素的加入使生产成本提高,改变了合金成分,影响合金的回收利用,另一方面,对熔体进行搅拌是提高铸件性能的一种方法;传统的机械搅拌工艺简单,但是由于搅拌器与熔体直接接触,在长时间搅拌摩擦作用下容易污染熔体;现有的电磁搅拌方法利用稳恒磁场增大金属熔体过冷度,从而增加形核速率,细化凝固组织,但是强磁场设备贵重且复杂,浇注过程对温度控制要求高,且稳恒磁场不能去除熔体中的气体和夹杂。Grain refinement treatment is an important method to improve the performance of castings. For the most widely used aluminum alloy castings, Al-Ti alloy or Al-Ti-B alloy grain refiners are generally used in the industry, which can reduce the hot cracking and segregation tendency of the castings while refining the grains and reduce the porosity. Rate. The existing process is characterized by adding Al-Sr intermediate alloy, mixed rare earth (Re) and Al-Zr intermediate alloy to the aluminum alloy melt in the tundish for modification and refinement treatment to improve product quality. However, because the refiner is extremely sensitive to factors such as melt temperature, treatment time, and addition method, the refining effect is quite different, and the addition of alloying elements increases the production cost, changes the alloy composition, and affects the recycling of the alloy. On the other hand, stirring the melt is a method to improve the performance of castings; the traditional mechanical stirring process is simple, but because the stirrer is in direct contact with the melt, it is easy to contaminate the melt under the action of friction stirring for a long time; the existing The electromagnetic stirring method uses a steady and constant magnetic field to increase the subcooling degree of the metal melt, thereby increasing the nucleation rate and refining the solidification structure, but the strong magnetic field equipment is expensive and complicated, the pouring process requires high temperature control, and the steady and constant magnetic field cannot remove the molten metal. Gases and inclusions in the body.
因此需要设计一种外场作用下差压反重力充型凝固装置及工艺方法。Therefore, it is necessary to design a differential pressure anti-gravity filling and solidification device and a process method under the action of an external field.
发明内容SUMMARY OF THE INVENTION
根据上述提出现有的低压铸造技术存在无法完全去除杂质和气体且无法完全搅拌的技术问题,而提供一种外场作用下差压反重力充型凝固装置及工艺方法。本发明主要利用真空和电磁耦合外场处理装置及其差压反重力充型及凝固方法,通过对熔体施加电磁场及真空场,从而起到有效去除熔体中的气体,促进夹杂物上浮,获得均匀细小的铸件组织的效果。According to the above, the existing low-pressure casting technology has the technical problems that impurities and gas cannot be completely removed and cannot be completely stirred, and a differential pressure anti-gravity filling and solidification device and process method under the action of an external field are provided. The invention mainly utilizes the vacuum and electromagnetic coupling external field processing device and the differential pressure anti-gravity filling and solidification method, by applying electromagnetic field and vacuum field to the melt, so as to effectively remove the gas in the melt, promote the floating of inclusions, and obtain The effect of uniform and fine casting structure.
本发明采用的技术手段如下:The technical means adopted in the present invention are as follows:
一种外场作用下差压反重力充型凝固装置,其特征在于,包括:凝固腔体、高压部、低压部和真空部,所述凝固腔体包括:上腔体和下腔体,所述上腔体内设有铸型,所述上腔体和下腔体通过中间板连接,所述上腔体和所述下腔体之间设有输液管,所述输液管穿过所述中间板的中心,所述下腔体的下端设有液压升降平台,所述液压升降平台的上端设有熔炼坩埚,所述下腔体底部设有感应熔炼装置,所述感应熔炼装置的上端设有电磁搅拌装置,所述下腔体在所述电磁搅拌装置和所述感应熔炼装置的对应位置设有感应电进口;所述高压部包括恒压高压罐和带阀导气管,所述恒压高压罐通过所述带阀导气管连接在所述上腔体和所述下腔体的下端;所述低压部包括恒压低压罐和带阀导气管,所述恒压低压罐通过所述带阀导气管连接在所述上腔体上;所述真空部包括真空泵、真空罐和带阀导气管,所述真空泵与所述真空罐连接,所述真空罐通过所述带阀导气管连接在所述上腔体的下端和所述下腔体的上端。A differential pressure anti-gravity filling and solidification device under the action of an external field is characterized in that it comprises: a solidification cavity, a high pressure part, a low pressure part and a vacuum part, the solidification cavity comprises: an upper cavity and a lower cavity, the The upper cavity is provided with a casting mold, the upper cavity and the lower cavity are connected by an intermediate plate, and an infusion tube is arranged between the upper cavity and the lower cavity, and the infusion tube passes through the intermediate plate The lower end of the lower cavity is provided with a hydraulic lifting platform, the upper end of the hydraulic lifting platform is provided with a melting crucible, the bottom of the lower cavity is provided with an induction melting device, and the upper end of the induction melting device is provided with an electromagnetic a stirring device, the lower cavity is provided with an induction electric inlet at the corresponding position of the electromagnetic stirring device and the induction melting device; the high pressure part includes a constant pressure high pressure tank and a valved air duct, the constant pressure high pressure tank The lower ends of the upper cavity and the lower cavity are connected through the valved air conduit; the low pressure part includes a constant pressure low pressure tank and a valved air conduit, and the constant pressure low pressure tank passes through the valved conduit. The air pipe is connected to the upper cavity; the vacuum part includes a vacuum pump, a vacuum tank and a valved air pipe, the vacuum pump is connected to the vacuum tank, and the vacuum tank is connected to the valve through the valved air pipe The lower end of the upper cavity and the upper end of the lower cavity.
进一步地,所述电磁搅拌装置的水冷套的材料为奥氏体不锈钢;所述下腔体的上端设有石英玻璃观察孔。Further, the material of the water cooling jacket of the electromagnetic stirring device is austenitic stainless steel; the upper end of the lower cavity is provided with a quartz glass observation hole.
进一步地,所述恒压高压罐内为高压氩气;所述恒压低压罐内为低压氩气。Further, inside the constant pressure high pressure tank is high pressure argon gas; inside the constant pressure low pressure tank is low pressure argon gas.
本发明还提供一种外场作用下差压反重力充型凝固装置的凝固工艺,其特征在于该凝固工艺步骤包括:The present invention also provides a solidification process of a differential pressure anti-gravity filling solidification device under the action of an external field, characterized in that the solidification process steps include:
步骤S1:将铝合金原料或纯铝及相关元素的中间合金烘干和除去表面杂质后投入所述熔炼坩埚,启动所述感应熔炼装置将原料熔化成液体,然后利用所述液压升降平台将所述熔炼坩埚升起,利用变质剂进行变质,利用纯度大于99.99%的高纯氩气旋转喷吹进行除气,然后进行除渣;Step S1: put the aluminum alloy raw material or the intermediate alloy of pure aluminum and related elements into the smelting crucible after drying and removing surface impurities, start the induction melting device to melt the raw material into liquid, and then use the hydraulic lifting platform to melt the raw material into a liquid. The smelting crucible is lifted up, metamorphic agent is used for metamorphism, and high-purity argon gas with a purity greater than 99.99% is used for degassing, and then slag removal is carried out;
步骤S2:除渣后利用所述液压升降平台将所述熔炼坩埚降至所述感应熔炼装置处,封闭所述中间板,安装所述输液管、所述铸型和所述上部腔体后抽真空;Step S2: After slag removal, use the hydraulic lifting platform to lower the melting crucible to the induction melting device, close the middle plate, install the infusion pipe, the mold and the upper cavity, and then pump vacuum;
步骤S3:启动所述感应熔炼装置将金属液升至预定温度后保持等温静置一段时间;Step S3: start the induction smelting device to raise the molten metal to a predetermined temperature and keep it isothermally for a period of time;
步骤S4:利用所述液压升降平台将所述熔炼坩埚升至外场作用区域,启动电磁场对熔体进行处理,深度去除熔体中的气体,保持合金成分和熔体温度的均匀性;Step S4: using the hydraulic lifting platform to lift the smelting crucible to the external field action area, start the electromagnetic field to process the melt, deeply remove the gas in the melt, and maintain the uniformity of alloy composition and melt temperature;
步骤S5:外场作用一定时间后,停止电磁搅拌,静置一段时间,然后利用所述恒压高压罐将所述上腔体和所述下腔体同时通入纯度大于99.99%的高纯氩气;Step S5: After the external field acts for a certain period of time, stop the electromagnetic stirring, let it stand for a period of time, and then use the constant pressure high-pressure tank to pass high-purity argon gas with a purity greater than 99.99% into the upper cavity and the lower cavity at the same time ;
步骤S6:利用所述恒压低压罐使所述上腔体减压,利用所述下腔体和所述上腔体之间的氩气压力差将铝合金熔液压入所述铸型进行浇铸,浇铸时间为10-25s,保压时间为5~15min;待熔液凝固形成铸件后卸压,打开上腔取出铸件。Step S6: use the constant-pressure low-pressure tank to decompress the upper cavity, and use the argon pressure difference between the lower cavity and the upper cavity to pour aluminum alloy melt into the mold for casting , the casting time is 10-25s, and the pressure holding time is 5-15min; after the melt solidifies to form a casting, the pressure is relieved, and the upper cavity is opened to take out the casting.
进一步地,步骤S1中合金熔体变质剂可采用Al-Ti-B、Al-Sr或Al-RE中间合金。铝合金可以采用ZL114A、ZL205A、ZL104A、ZL101、A356和A357等铝合金。Further, Al-Ti-B, Al-Sr or Al-RE master alloy may be used as the alloy melt modifier in step S1. Aluminum alloys such as ZL114A, ZL205A, ZL104A, ZL101, A356 and A357 can be used as aluminum alloys.
进一步地,步骤S2中真空度为10-40Pa。Further, in step S2, the degree of vacuum is 10-40Pa.
进一步地,步骤S3中真空条件下铝合金熔体等温静置时间为18-25min。Further, in step S3, the isothermal standing time of the aluminum alloy melt under the vacuum condition is 18-25 min.
进一步地,步骤S4中熔体达到TL以上80~100℃时启动电磁搅拌装置对熔体进行电磁搅拌,中心磁感应强度为0~30mT,电磁场作用时间1~5min。Further, in step S4, when the melt reaches 80-100°C above TL, the electromagnetic stirring device is started to electromagnetically stir the melt, the central magnetic induction intensity is 0-30 mT, and the electromagnetic field action time is 1-5 min.
较现有技术相比,本发明具有以下优点:Compared with the prior art, the present invention has the following advantages:
1、本发明提供的一种外场作用下差压反重力充型凝固装置及工艺方法,在差压反重力充型凝固过程中利用电磁场切割金属液产生的感生电流,在金属熔体内产生电磁力,促使熔体产生强制性对流,使熔体温度场合溶质分布更均匀,并加强了形核和游离,在铸造过程中施加磁场和真空场不会引入其他杂质,是一种理想的提高铸件质量的方法。1. A differential pressure anti-gravity filling and solidification device and a process method under the action of an external field provided by the present invention utilize the induced current generated by the electromagnetic field to cut the molten metal during the differential pressure anti-gravity filling and solidification process, which is generated in the metal melt. Electromagnetic force promotes the forced convection of the melt, makes the solute distribution more uniform at the temperature of the melt, and strengthens nucleation and dissociation. The application of magnetic field and vacuum field during the casting process will not introduce other impurities, which is an ideal improvement. Methods of casting quality.
2、本发明提供的一种外场作用下差压反重力充型凝固装置及工艺方法在差压反重力充型凝固过程中引入电磁场和真空场,不影响现有的铸造条件和工艺,设备简单,操作方便,具备工艺适应性强、方便灵活、铸件气孔率低、力学性能高的优势,适用于大中型铸造铝合金铸件的成形制造和工业化生产。2. The differential pressure antigravity mold filling and solidification device and process method provided by the present invention introduce electromagnetic fields and vacuum fields during the differential pressure antigravity mold filling and solidification process, which does not affect the existing casting conditions and processes, and the equipment is simple , easy to operate, with the advantages of strong process adaptability, convenience and flexibility, low porosity of castings, and high mechanical properties, suitable for the forming and industrial production of large and medium-sized aluminum alloy castings.
3、本发明提供的一种外场作用下差压反重力充型凝固装置及工艺方法将非真空合金熔炼、变质和初步除气精炼和真空场、电磁场耦合深度精炼有机结合,实现了大体积铝合金熔体的深度精炼,对于提升大型复杂铝合金铸造产品的致密性非常有益。3. The differential pressure anti-gravity filling and solidification device and process method provided by the present invention organically combine non-vacuum alloy smelting, metamorphism and preliminary degassing refining with vacuum field and electromagnetic field coupling deep refining to realize large-volume aluminum alloys. The deep refining of alloy melt is very beneficial for improving the compactness of large and complex aluminum alloy casting products.
基于上述理由本发明可在低压铸造技术等领域广泛推广。Based on the above reasons, the present invention can be widely promoted in the fields of low pressure casting technology and the like.
为了更清楚地说明本发明实施例或现有技术中的技术方案,下面将对实施例或现有技术描述中所需要使用的附图做以简单地介绍,显而易见地,下面描述中的附图是本发明的一些实施例,对于本领域普通技术人员来讲,在不付出创造性劳动性的前提下,还可以根据这些附图获得其他的附图。In order to illustrate the embodiments of the present invention or the technical solutions in the prior art more clearly, the following briefly introduces the accompanying drawings that need to be used in the description of the embodiments or the prior art. Obviously, the accompanying drawings in the following description These are some embodiments of the present invention, and for those of ordinary skill in the art, other drawings can also be obtained from these drawings without any creative effort.
图1为本发明一种外场作用下差压反重力充型凝固装置及工艺方法的结构示意图。FIG. 1 is a schematic structural diagram of a differential pressure antigravity filling and solidification device and a process method under the action of an external field of the present invention.
图2为本发明一种外场作用下差压反重力充型凝固装置及工艺方法的非真空条件熔炼、变质和除气时坩埚位置示意图。Fig. 2 is a schematic diagram of the position of the crucible during smelting, metamorphism and degassing under non-vacuum conditions of a differential pressure antigravity filling and solidification device and a process method under the action of an external field of the present invention.
图3为本发明一种外场作用下差压反重力充型凝固装置及工艺方法的真空条件熔体深度净化时坩埚位置示意图。3 is a schematic diagram of the position of the crucible during the deep purification of the melt under the vacuum condition of a differential pressure antigravity filling and solidification device and a process method under the action of an external field of the present invention.
图中:1、上腔体;2、铸型;3、铝合金铸件;4、中间板;5、输液管;6、石英玻璃观察孔;7、熔炼坩埚;8、电磁搅拌装置;9、感应熔炼装置;10、液压升降平台;11、位置控制装置;12、下腔体;13、感应电进口;14、恒压高压罐;15、真空泵;16、真空罐;17、气体控制阀;18、恒压低压罐。In the figure: 1. Upper cavity; 2. Casting mold; 3. Aluminum alloy casting; 4. Intermediate plate; 5. Infusion tube; 6. Quartz glass observation hole; 7. Melting crucible; 8. Electromagnetic stirring device; 9. Induction smelting device; 10. Hydraulic lifting platform; 11. Position control device; 12. Lower cavity; 13. Induction electric inlet; 14. Constant pressure high pressure tank; 15. Vacuum pump; 16. Vacuum tank; 17. Gas control valve; 18. Constant pressure low pressure tank.
需要说明的是,在不冲突的情况下,本发明中的实施例及实施例中的特征可以相互组合。下面将参考附图并结合实施例来详细说明本发明。It should be noted that the embodiments of the present invention and the features of the embodiments may be combined with each other under the condition of no conflict. The present invention will be described in detail below with reference to the accompanying drawings and in conjunction with the embodiments.
为使本发明实施例的目的、技术方案和优点更加清楚,下面将结合本发明实施例中的附图,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本发明一部分实施例,而不是全部的实施例。以下对至少一个示例性实施例的描述实际上仅仅是说明性的,决不作为对本发明及其应用或使用的任何限制。基于本发明中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。In order to make the purposes, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present invention. Obviously, the described embodiments It is only a part of the embodiments of the present invention, but not all of the embodiments. The following description of at least one exemplary embodiment is merely illustrative in nature and is in no way intended to limit the invention, its application, or uses. Based on the embodiments of the present invention, all other embodiments obtained by those of ordinary skill in the art without creative efforts shall fall within the protection scope of the present invention.
需要注意的是,这里所使用的术语仅是为了描述具体实施方式,而非意图限制根据本发明的示例性实施方式。如在这里所使用的,除非上下文另外明确指出,否则单数形式也意图包括复数形式,此外,还应当理解的是,当在本说明书中使用术语“包含”和/或“包括”时,其指明存在特征、步骤、操作、器件、组件和/或它们的组合。It should be noted that the terminology used herein is for the purpose of describing specific embodiments only, and is not intended to limit the exemplary embodiments according to the present invention. As used herein, unless the context clearly dictates otherwise, the singular is intended to include the plural as well, furthermore, it is to be understood that when the terms "comprising" and/or "including" are used in this specification, it indicates that There are features, steps, operations, devices, components and/or combinations thereof.
除非另外具体说明,否则在这些实施例中阐述的部件和步骤的相对布置、数字表达式和数值不限制本发明的范围。同时,应当清楚,为了便于描述,附图中所示出的各个部分的尺寸并不是按照实际的比例关系绘制的。对于相关领域普通技术人员己知的技术、方法和设备可能不作详细讨论,但在适当情况下,所述技术、方法和设备应当被视为授权说明书的一部分。在这里示出和讨论的所有示例中,任向具体值应被解释为仅仅是示例性的,而不是作为限制。因此,示例性实施例的其它示例可以具有不同的值。应注意到:相似的标号和字母在下面的附图中表示类似项,因此,一旦某一项在一个附图中被定义,则在随后的附图中不需要对其进行进一步讨论。The relative arrangement of the components and steps, the numerical expressions and numerical values set forth in these embodiments do not limit the scope of the invention unless specifically stated otherwise. Meanwhile, it should be understood that, for convenience of description, the dimensions of various parts shown in the accompanying drawings are not drawn in an actual proportional relationship. Techniques, methods, and devices known to those of ordinary skill in the relevant art may not be discussed in detail, but where appropriate, such techniques, methods, and devices should be considered part of the authorized specification. In all examples shown and discussed herein, any specific values should be construed as illustrative only and not limiting. Accordingly, other examples of exemplary embodiments may have different values. It should be noted that like numerals and letters refer to like items in the following figures, so once an item is defined in one figure, it does not require further discussion in subsequent figures.
在本发明的描述中,需要理解的是,方位词如“前、后、上、下、左、右”、“横向、竖向、垂直、水平”和“顶、底”等所指示的方位或位置关系通常是基于附图所示的方位或位置关系,仅是为了便于描述本发明和简化描述,在未作相反说明的情况下,这些方位词并不指示和暗示所指的装置或元件必须具有特定的方位或者以特定的方位构造和操作,因此不能理解为对本发明保护范围的限制:方位词“内、外”是指相对于各部件本身的轮廓的 内外。In the description of the present invention, it should be understood that the orientations indicated by orientation words such as "front, rear, top, bottom, left, right", "horizontal, vertical, vertical, horizontal" and "top, bottom" etc. Or the positional relationship is usually based on the orientation or positional relationship shown in the drawings, which is only for the convenience of describing the present invention and simplifying the description, and these orientation words do not indicate or imply the indicated device or element unless otherwise stated. It must have a specific orientation or be constructed and operated in a specific orientation, so it should not be construed as a limitation on the scope of protection of the present invention: the orientation words "inside and outside" refer to the inside and outside relative to the contour of each component itself.
为了便于描述,在这里可以使用空间相对术语,如“在……之上”、“在……上方”、“在……上表面”、“上面的”等,用来描述如在图中所示的一个器件或特征与其他器件或特征的空间位置关系。应当理解的是,空间相对术语旨在包含除了器件在图中所描述的方位之外的在使用或操作中的不同方位。例如,如果附图中的器件被倒置,则描述为“在其他器件或构造上方”或“在其他器件或构造之上”的器件之后将被定位为“在其他器件或构造下方”或“在其位器件或构造之下”。因而,示例性术语“在……上方”可以包括“在……上方”和“在……下方”两种方位。该器件也可以其他不同方式定位(旋转90度或处于其他方位),并且对这里所使用的空间相对描述作出相应解释。For ease of description, spatially relative terms, such as "on", "over", "on the surface", "above", etc., may be used herein to describe what is shown in the figures. The spatial positional relationship of one device or feature shown to other devices or features. It should be understood that spatially relative terms are intended to encompass different orientations of the device in use or operation in addition to the orientation depicted in the figures. For example, if the device in the figures is turned over, elements described as "above" or "over" other devices or features would then be oriented "below" or "over" the other devices or features under its device or structure". Thus, the exemplary term "above" can encompass both an orientation of "above" and "below." The device may also be otherwise oriented (rotated 90 degrees or at other orientations) and the spatially relative descriptions used herein interpreted accordingly.
此外,需要说明的是,使用“第一”、“第二”等词语来限定零部件,仅仅是为了便于对相应零部件进行区别,如没有另行声明,上述词语并没有特殊含义,因此不能理解为对本发明保护范围的限制。In addition, it should be noted that the use of words such as "first" and "second" to define components is only for the convenience of distinguishing corresponding components. Unless otherwise stated, the above words have no special meaning and therefore cannot be understood to limit the scope of protection of the present invention.
如图1-3所示,本发明提供了一种外场作用下差压反重力充型凝固装置,包括:凝固腔体、高压部、低压部和真空部,所述凝固腔体包括:上腔体1和下腔体12,所述上腔体1内设有铸型2,所述上腔体1和下腔体12通过中间板4连接;所述上腔体1和所述下腔体12之间设有输液管5,所述输液管5穿过所述中间板4的中心;所述下腔体12的下端设有液压升降平台10,所述液压升降平台10通过位置控制装置11进行控制,所述液压升降平台10的上端设有熔炼坩埚7;所述下腔体12底部设有感应熔炼装置9,所述感应熔炼装置可以是感应加热装置,如感应加热线圈;所述感应熔炼装置9的上端设有电磁搅拌装置8,所述电磁搅拌装置8的水冷套的材料为奥氏体不锈钢;所述下腔体12在所述电磁搅拌装置8和所述感应熔炼装置9的对应位置设有感应电进口13;所述高压部包括恒压高压罐14和带阀导气管,所述恒压高压罐14通过所述带阀导气管连接在所述上腔体1和所述下腔体12的下端;所述低压部包括恒压低压罐18和所述带阀导气管,所述恒压低压罐18通过所述带阀导气管连接在所述上腔体1上;所述真空部包括真空泵15、真空罐16和所述带阀导气管,所述真空泵15与所述真空罐16连接,所述真空罐16通过所述带阀导气管连接在所述上腔体1的下端和所述下腔体12的上端;所 述下腔体12的上端设有石英玻璃观察孔6;所述恒压高压罐14内为高压氩气;所述恒压低压罐18内为低压氩气。As shown in Figures 1-3, the present invention provides a differential pressure anti-gravity filling and solidification device under the action of an external field, including: a solidification cavity, a high pressure part, a low pressure part and a vacuum part, and the solidification cavity includes: an upper cavity The upper cavity 1 and the lower cavity 12 are provided with a casting mold 2, and the upper cavity 1 and the lower cavity 12 are connected by the intermediate plate 4; the upper cavity 1 and the lower cavity An infusion pipe 5 is arranged between 12, and the infusion pipe 5 passes through the center of the intermediate plate 4; the lower end of the lower cavity 12 is provided with a hydraulic lifting platform 10, and the hydraulic lifting platform 10 passes through the position control device 11. For control, the upper end of the hydraulic lifting platform 10 is provided with a melting crucible 7; the bottom of the lower cavity 12 is provided with an induction melting device 9, and the induction melting device can be an induction heating device, such as an induction heating coil; The upper end of the smelting device 9 is provided with an electromagnetic stirring device 8 , and the material of the water cooling jacket of the electromagnetic stirring device 8 is austenitic stainless steel; the lower cavity 12 is located between the electromagnetic stirring device 8 and the induction melting device 9 . There is an induction electric inlet 13 at the corresponding position; the high-pressure part includes a constant-pressure high-pressure tank 14 and a valved air conduit, and the constant-pressure high-pressure tank 14 is connected to the upper cavity 1 and the valved air conduit through the valved air conduit. The lower end of the lower cavity 12; the low pressure part includes a constant pressure low pressure tank 18 and the valved air conduit, and the constant pressure low pressure tank 18 is connected to the upper cavity 1 through the valved air conduit; The vacuum part includes a vacuum pump 15, a vacuum tank 16, and the valved gas conduit. The vacuum pump 15 is connected to the vacuum tank 16, and the vacuum tank 16 is connected to the upper cavity 1 through the valved gas conduit. The lower end of the lower chamber 12 and the upper end of the lower chamber 12; the upper end of the lower chamber 12 is provided with a quartz glass observation hole 6; the constant pressure high pressure tank 14 is filled with high pressure argon; the constant pressure low pressure tank 18 is Low pressure argon.
本发明还提供一种外场作用下差压反重力充型凝固装置的凝固工艺,其特征在于该凝固工艺步骤包括:The present invention also provides a solidification process of a differential pressure anti-gravity filling solidification device under the action of an external field, characterized in that the solidification process steps include:
步骤S1:将铝合金原料或纯铝及相关元素的中间合金烘干和除去表面杂质后投入所述熔炼坩埚7,启动所述感应熔炼装置9将原料熔化成液体,然后利用所述液压升降平台10将所述熔炼坩埚7升起,利用变质剂进行变质,利用纯度大于99.99%的高纯氩气旋转喷吹进行除气,然后进行除渣;Step S1: put the aluminum alloy raw material or the intermediate alloy of pure aluminum and related elements into the melting crucible 7 after drying and removing surface impurities, start the induction melting device 9 to melt the raw material into liquid, and then use the hydraulic lifting platform 10 lift the smelting crucible 7, use a metamorphic agent for metamorphism, use high-purity argon with a purity greater than 99.99% to rotate and spray for degassing, and then carry out slag removal;
步骤S2:除渣后利用所述液压升降平台10将所述熔炼坩埚7降至所述感应熔炼装置9处,封闭所述中间板4,安装所述输液管5、所述铸型2和所述上部腔体后抽真空;Step S2: After removing the slag, use the hydraulic lifting platform 10 to lower the melting crucible 7 to the induction melting device 9, close the middle plate 4, install the infusion pipe 5, the casting mold 2 and the After the upper cavity is evacuated;
步骤S3:启动所述感应熔炼装置9将金属液升至预定温度后保持等温静置一段时间;Step S3: start the induction smelting device 9 to raise the molten metal to a predetermined temperature and keep it isothermally for a period of time;
步骤S4:利用所述液压升降平台10将所述熔炼坩埚7升至外场作用区域,启动电磁场对熔体进行处理,深度去除熔体中的气体,保持合金成分和熔体温度的均匀性;Step S4: using the hydraulic lifting platform 10 to lift the smelting crucible 7 to the external field action area, start the electromagnetic field to process the melt, deeply remove the gas in the melt, and maintain the uniformity of alloy composition and melt temperature;
步骤S5:外场作用一定时间后,停止电磁搅拌,静置一段时间,然后利用所述恒压高压罐14将所述上腔体1和所述下腔体12同时通入纯度大于99.99%的高纯氩气;Step S5: After the external field acts for a certain period of time, stop the electromagnetic stirring, let it stand for a period of time, and then use the constant pressure high-pressure tank 14 to simultaneously pass the upper cavity 1 and the lower cavity 12 into the high purity greater than 99.99%. pure argon;
步骤S6:利用所述恒压低压罐18使所述上腔体1减压,利用所述下腔体12和所述上腔体1之间的氩气压力差将铝合金熔液压入所述铸型2进行浇铸,浇铸时间为10-25s,保压时间为5~15min;待熔液凝固形成铸件后卸压,打开上腔取出铸件。Step S6: use the constant pressure low pressure tank 18 to decompress the upper cavity 1, and use the argon pressure difference between the lower cavity 12 and the upper cavity 1 to inject aluminum alloy melt into the Casting mold 2 is cast, the casting time is 10-25s, and the pressure holding time is 5-15min; after the melt solidifies to form a casting, the pressure is relieved, and the upper cavity is opened to take out the casting.
步骤S1中合金熔体变质剂可采用Al-Ti-B、Al-Sr或Al-RE中间合金。铝合金可以采用ZL114A、ZL205A、ZL104A、ZL101、A356和A357等铝合金;步骤S2中真空度为10-40Pa;步骤S3中真空条件下铝合金熔体等温静置时间为18-25min;步骤S4中熔体达到TL以上80~100℃时启动电磁搅拌装置8对熔体进行电磁搅拌,中心磁感应强度为0~30mT,电磁场作用时间1~5min。Al-Ti-B, Al-Sr or Al-RE master alloy may be used as the alloy melt modifier in step S1. The aluminum alloy can be aluminum alloys such as ZL114A, ZL205A, ZL104A, ZL101, A356 and A357; the vacuum degree in step S2 is 10-40Pa; the isothermal standing time of the aluminum alloy melt under vacuum conditions in step S3 is 18-25min; step S4 When the melt reaches 80-100°C above TL, start the electromagnetic stirring device 8 to electromagnetically stir the melt, the central magnetic induction intensity is 0-30mT, and the electromagnetic field action time is 1-5min.
实施例1Example 1
1、将ZL114A铝合金原料或纯铝及Al-Si、Al-Mg等中间合金烘干和除去表面杂质后投入所述熔炼坩埚7,启动所述感应加热装置9将原料熔化成700~710℃液体,然后利用所述液压升降平台10将坩埚升起至如图2所示位置,利用变质剂进行变质,利用纯度大于99.99%的高纯氩气旋转喷吹进行除气,然后进行除渣;1. Put the ZL114A aluminum alloy raw material or pure aluminum and intermediate alloys such as Al-Si and Al-Mg into the smelting crucible 7 after drying and removing surface impurities, and start the induction heating device 9 to melt the raw materials to 700~710℃ liquid, and then use the hydraulic lifting platform 10 to lift the crucible to the position shown in Figure 2, use a modifier for metamorphism, and use high-purity argon with a purity greater than 99.99% to rotate and spray for degassing, and then slag removal;
2、除渣后利用所述液压升降平台10将所述熔炼坩埚7降至所述感应加热装置处,如图3所示,封闭所述中间板4,安装所述输液管5、所述铸型2和所述上腔体1后利用所述真空罐16将所述上腔体1和所述下腔体12同时抽真空10-20Pa;2. After slag removal, use the hydraulic lifting platform 10 to lower the melting crucible 7 to the induction heating device, as shown in FIG. After type 2 and the upper cavity 1, the upper cavity 1 and the lower cavity 12 are simultaneously evacuated by 10-20 Pa using the vacuum tank 16;
3、启动感应加热装置将金属液升至预定温度后保持等温静置15min;3. Start the induction heating device to raise the molten metal to a predetermined temperature and keep it at an isothermal stand for 15 minutes;
4、利用所述液压升降平台10将所述熔炼坩埚7升至外场作用区域所述电磁搅拌装置8处,启动所述电磁搅拌装置8对熔体进行处理1min,深度去除熔体中的气体,保持合金成分和熔体温度的均匀性;4. Use the hydraulic lifting platform 10 to lift the smelting crucible 7 to the electromagnetic stirring device 8 in the external field action area, start the electromagnetic stirring device 8 to process the melt for 1 min, and deeply remove the gas in the melt, Maintain uniformity of alloy composition and melt temperature;
5、外场作用一定时间后,停止电磁搅拌,静置10s,然后利用所述恒压高压罐14将所述上腔体1和所述下腔体12同时通入纯度大于99.99%的高纯氩气;5. After the external field acts for a certain period of time, stop the electromagnetic stirring, let it stand for 10s, and then use the constant pressure high-pressure tank 14 to pass the upper chamber 1 and the lower chamber 12 into high-purity argon with a purity greater than 99.99% at the same time. gas;
6、利用所述恒压低压罐18使所述上腔体1减压,利用所述下腔体12和所述上腔体1之间的氩气压力差将铝合金熔液压入所述铸型2进行浇铸,浇铸时间为10-25s,保压时间为5~15min;待熔液凝固形成铸件后卸压,打开上腔取出铸件。6. Use the constant pressure and low pressure tank 18 to decompress the upper cavity 1, and use the argon pressure difference between the lower cavity 12 and the upper cavity 1 to press the aluminum alloy melt into the casting Type 2 is cast, the casting time is 10-25s, and the pressure holding time is 5-15min; after the melt solidifies to form a casting, the pressure is relieved, and the upper cavity is opened to take out the casting.
本实施例利用交变旋转磁场促使ZL114A铝合金熔体产生强制性对流,均匀了熔体温度场,加强了晶核形核和游离,实现了铸件组织的晶粒细化,减少了夹杂物,利用真空场和电磁长耦合作用实现了ZL114A铝合金熔体的深度净化,改善了铸件性能。In this embodiment, the alternating rotating magnetic field is used to promote forced convection of the ZL114A aluminum alloy melt, which uniformizes the melt temperature field, strengthens the nucleation and dissociation of the crystal nucleus, realizes the grain refinement of the casting structure, and reduces the inclusions. The deep purification of ZL114A aluminum alloy melt was realized by using vacuum field and electromagnetic long coupling effect, and the casting performance was improved.
实施例2Example 2
1、将ZL205A铝合金原料或纯铝及Al-Cu等中间合金烘干和除去表面杂质后投入所述熔炼坩埚7,启动所述感应熔炼装置9将原料熔化成700~715 ℃液体,然后利用所述液压升降平台10将所述熔炼坩埚7升起至如图2所示位置,利用变质剂进行变质,利用纯度大于99.99%的高纯氩气旋转喷吹进行除气,然后进行除渣;1. Put ZL205A aluminum alloy raw materials or intermediate alloys such as pure aluminum and Al-Cu into the melting crucible 7 after drying and removing surface impurities, start the induction melting device 9 to melt the raw materials into 700-715 ℃ liquid, and then use The hydraulic lifting platform 10 lifts the smelting crucible 7 to the position shown in FIG. 2 , uses a metamorphic agent for metamorphism, uses a high-purity argon gas with a purity greater than 99.99% to rotate and blow for degassing, and then performs slag removal;
2、除渣后利用所述液压升降平台10将所述熔炼坩埚7降至所述感应熔炼装置9处,封闭所述中间板4,安装所述输液管5、所述铸型2和所述上腔体1后利用所述真空罐16将所述上腔体1和所述下腔体12同时抽真空10-30Pa;2. After slag removal, use the hydraulic lifting platform 10 to lower the melting crucible 7 to the induction melting device 9, close the middle plate 4, install the infusion pipe 5, the casting mold 2 and the After the upper cavity 1, the upper cavity 1 and the lower cavity 12 are simultaneously evacuated by 10-30 Pa using the vacuum tank 16;
3、启动所述感应熔炼装置9将金属液升至预定温度后保持等温静置18min;3. Start the induction smelting device 9 to raise the molten metal to a predetermined temperature and keep it at rest for 18 minutes at an isothermal temperature;
4、利用所述液压升降平台10将所述熔炼坩埚7升至外场作用区域所述电磁搅拌装置8处,启动所述电磁搅拌装置8对熔体进行处理2min,深度去除熔体中的气体,保持合金成分和熔体温度的均匀性;4. Use the hydraulic lifting platform 10 to lift the smelting crucible 7 to the electromagnetic stirring device 8 in the external field action area, start the electromagnetic stirring device 8 to process the melt for 2 minutes, and deeply remove the gas in the melt, Maintain uniformity of alloy composition and melt temperature;
5、外场作用一定时间后,停止电磁搅拌,静置20s,然后利用所述恒压高压罐14将所述上腔体1和所述下腔体12同时通入纯度大于99.99%的高纯氩气;5. After the external field acts for a certain period of time, stop the electromagnetic stirring, let it stand for 20s, and then use the constant pressure high-pressure tank 14 to pass the upper chamber 1 and the lower chamber 12 into the high-purity argon with a purity greater than 99.99% at the same time. gas;
6、利用所述恒压低压罐18使所述上腔体1减压,利用所述下腔体12和所述上腔体1之间的氩气压力差将铝合金熔液压入所述铸型2进行浇铸,浇铸时间为10-25s,保压时间为5~15min;待熔液凝固形成铸件后卸压,打开上腔取出铸件。6. Use the constant pressure and low pressure tank 18 to decompress the upper cavity 1, and use the argon pressure difference between the lower cavity 12 and the upper cavity 1 to press the aluminum alloy melt into the casting Type 2 is cast, the casting time is 10-25s, and the pressure holding time is 5-15min; after the melt solidifies to form a casting, the pressure is relieved, and the upper cavity is opened to take out the casting.
实施例3Example 3
1、将ZL104A或A357铝合金原料或纯铝及Al-Si、Al-Mg等中间合金烘干和除去表面杂质后投入所述熔炼坩埚7,启动所述感应熔炼装置9将原料熔化成710~720℃液体,然后利用所述液压升降平台10将所述熔炼坩埚7升起至如图2所示位置,利用变质剂进行变质,利用纯度大于99.99%的高纯氩气旋转喷吹进行除气,然后进行除渣;1. Put ZL104A or A357 aluminum alloy raw materials or pure aluminum and intermediate alloys such as Al-Si and Al-Mg into the melting crucible 7 after drying and removing surface impurities, and start the induction melting device 9 to melt the raw materials into 710~ 720 ° C liquid, and then use the hydraulic lifting platform 10 to lift the melting crucible 7 to the position shown in Figure 2, use a modifier for metamorphism, and use high-purity argon with a purity greater than 99.99%. , and then carry out slag removal;
2、除渣后利用所述液压升降平台10将所述熔炼坩埚7降至所述感应加热装置处,如图3所示,封闭所述中间板4,安装所述输液管5、所述铸型2和所述上腔体1后利用所述真空罐16将所述上腔体1和所述下腔体12同时 抽真空20-40Pa;2. After slag removal, use the hydraulic lifting platform 10 to lower the melting crucible 7 to the induction heating device, as shown in FIG. After type 2 and the upper cavity 1, the upper cavity 1 and the lower cavity 12 are simultaneously evacuated by 20-40 Pa using the vacuum tank 16;
3、启动所述感应熔炼装置9将金属液升至预定温度后保持等温静置22min;3. Start the induction smelting device 9 to raise the molten metal to a predetermined temperature and keep it at rest for 22 minutes at an isothermal temperature;
4、利用所述液压升降平台10将所述熔炼坩埚7升至外场作用区域所述电磁搅拌装置8处,启动所述电磁搅拌装置8对熔体进行处理3min,深度去除熔体中的气体,保持合金成分和熔体温度的均匀性;4. Use the hydraulic lifting platform 10 to lift the smelting crucible 7 to the electromagnetic stirring device 8 in the external field action area, start the electromagnetic stirring device 8 to process the melt for 3 minutes, and deeply remove the gas in the melt, Maintain uniformity of alloy composition and melt temperature;
5、外场作用一定时间后,停止电磁搅拌,静置25s,然后利用所述恒压高压罐14将所述上腔体1和所述下腔体12同时通入纯度大于99.99%的高纯氩气;5. After the external field acts for a certain period of time, stop the electromagnetic stirring, let it stand for 25s, and then use the constant pressure high-pressure tank 14 to pass the upper chamber 1 and the lower chamber 12 into high-purity argon with a purity greater than 99.99% at the same time. gas;
6、利用所述恒压低压罐18使所述上腔体1减压,利用所述下腔体12和所述上腔体1之间的氩气压力差将铝合金熔液压入所述铸型2进行浇铸,浇铸时间为10-25s,保压时间为5~15min;待熔液凝固形成铸件后卸压,打开上腔取出铸件。6. Use the constant pressure and low pressure tank 18 to decompress the upper cavity 1, and use the argon pressure difference between the lower cavity 12 and the upper cavity 1 to press the aluminum alloy melt into the casting Type 2 is cast, the casting time is 10-25s, and the pressure holding time is 5-15min; after the melt solidifies to form a casting, the pressure is relieved, and the upper cavity is opened to take out the casting.
本实施例利用交变旋转磁场促使ZL104A和A357铝合金熔体产生强制性对流,均匀了熔体温度场,加强了晶核形核和游离,实现了铸件组织的晶粒细化,减少了夹杂物,利用真空场和电磁长耦合作用实现了ZL104A铝合金熔体的深度净化,改善了铸件性能。In this embodiment, the alternating rotating magnetic field is used to promote forced convection of the ZL104A and A357 aluminum alloy melts, which uniformizes the melt temperature field, strengthens the nucleation and dissociation of the crystal nucleus, realizes the grain refinement of the casting structure, and reduces the inclusions. The deep purification of ZL104A aluminum alloy melt was realized by using the vacuum field and electromagnetic long coupling effect, and the performance of the casting was improved.
实施例4Example 4
1、将ZL101或A356铝合金原料或纯铝及Al-Si、Al-Mg等中间合金烘干和除去表面杂质后投入所述熔炼坩埚7,启动所述感应加热线圈9将原料熔化成710~715℃液体,然后利用所述液压升降平台10将坩埚升起至如图2所示位置,利用变质剂进行变质,利用纯度大于99.99%的高纯氩气旋转喷吹进行除气,然后进行除渣;1. Put ZL101 or A356 aluminum alloy raw materials or pure aluminum and intermediate alloys such as Al-Si and Al-Mg into the melting crucible 7 after drying and removing surface impurities, and start the induction heating coil 9 to melt the raw materials into 710~ 715 ° C liquid, then use the hydraulic lifting platform 10 to lift the crucible to the position shown in Figure 2, use a modifier for metamorphism, and use high-purity argon with a purity greater than 99.99% to rotate and spray to degas, and then degas slag;
2、除渣后利用所述液压升降平台10将所述熔炼坩埚7降至所述感应熔炼装置9处,如图3所示。封闭所述中间板4,安装所述输液管5、所述铸型2和所述上腔体1后利用所述真空罐16将所述上腔体1和所述下腔体12同时抽真空15-30Pa;2. After removing the slag, use the hydraulic lifting platform 10 to lower the melting crucible 7 to the induction melting device 9, as shown in FIG. 3 . Close the middle plate 4, install the infusion tube 5, the mold 2 and the upper cavity 1, and use the vacuum tank 16 to vacuum the upper cavity 1 and the lower cavity 12 at the same time 15-30Pa;
3、启动感应加热线圈将金属液升至预定温度后保持等温静置25min;3. Start the induction heating coil to raise the molten metal to the predetermined temperature and keep it at an isothermal temperature for 25 minutes;
4、利用所述液压升降平台10将所述熔炼坩埚7升至外场作用区域所述电磁搅拌装置8处,启动所述电磁搅拌装置8对熔体进行处理5min,深度去除熔体中的气体,保持合金成分和熔体温度的均匀性;4. Use the hydraulic lifting platform 10 to lift the smelting crucible 7 to the electromagnetic stirring device 8 in the external field action area, start the electromagnetic stirring device 8 to process the melt for 5 minutes, and deeply remove the gas in the melt, Maintain uniformity of alloy composition and melt temperature;
5、外场作用一定时间后,停止电磁搅拌,静置30s,然后利用所述恒压高压罐14将所述上腔体1和所述下腔体12同时通入纯度大于99.99%的高纯氩气;5. After the external field acts for a certain period of time, stop the electromagnetic stirring, let it stand for 30s, and then use the constant pressure high-pressure tank 14 to pass the upper chamber 1 and the lower chamber 12 into high-purity argon with a purity greater than 99.99% at the same time. gas;
6、利用所述恒压低压罐18使所述上腔体1减压,利用所述下腔体12和所铸型2进行浇铸,浇铸时间为10-25s,保压时间为5~15min;待熔液凝固形成铸件后卸压,打开上腔取出铸件。6. Use the constant pressure and low pressure tank 18 to depressurize the upper cavity 1, and use the lower cavity 12 and the casting mold 2 for casting, the casting time is 10-25s, and the pressure holding time is 5-15min; After the melt solidifies to form a casting, the pressure is relieved, and the upper cavity is opened to take out the casting.
本实施例利用交变旋转磁场促使ZL101和A356铝合金熔体产生强制性对流,均匀了熔体温度场,加强了晶核形核和游离,实现了铸件组织的晶粒细化,减少了夹杂物,利用真空场和电磁长耦合作用实现了ZL101和A356铝合金熔体的深度净化,改善了铸件性能。In this embodiment, the alternating rotating magnetic field is used to promote forced convection of the ZL101 and A356 aluminum alloy melts, which uniformizes the melt temperature field, strengthens the nucleation and dissociation of the crystal nucleus, realizes the grain refinement of the casting structure, and reduces the inclusions. The deep purification of ZL101 and A356 aluminum alloy melts was realized by using the vacuum field and electromagnetic long-coupling, and the performance of the castings was improved.
最后应说明的是:以上各实施例仅用以说明本发明的技术方案,而非对其限制;尽管参照前述各实施例对本发明进行了详细的说明,本领域的普通技术人员应当理解:其依然可以对前述各实施例所记载的技术方案进行修改,或者对其中部分或者全部技术特征进行等同替换;而这些修改或者替换,并不使相应技术方案的本质脱离本发明各实施例技术方案的范围。Finally, it should be noted that the above embodiments are only used to illustrate the technical solutions of the present invention, but not to limit them; although the present invention has been described in detail with reference to the foregoing embodiments, those of ordinary skill in the art should understand that: The technical solutions described in the foregoing embodiments can still be modified, or some or all of the technical features thereof can be equivalently replaced; and these modifications or replacements do not make the essence of the corresponding technical solutions deviate from the technical solutions of the embodiments of the present invention. scope.
Claims (8)
- 一种外场作用下差压反重力充型凝固装置,其特征在于,包括:凝固腔体、高压部、低压部和真空部,所述凝固腔体包括:上腔体和下腔体,所述上腔体内设有铸型,所述上腔体和下腔体通过中间板连接,所述上腔体和所述下腔体之间设有输液管,所述输液管穿过所述中间板的中心,所述下腔体的下端设有液压升降平台,所述液压升降平台的上端设有熔炼坩埚,所述下腔体底部设有感应熔炼装置,所述感应熔炼装置的上端设有电磁搅拌装置,所述下腔体在所述电磁搅拌装置和所述感应熔炼装置的对应位置设有感应电进口;所述高压部包括恒压高压罐和带阀导气管,所述恒压高压罐通过所述带阀导气管连接在所述上腔体和所述下腔体的下端;所述低压部包括恒压低压罐和所述带阀导气管,所述恒压低压罐通过所述带阀导气管连接在所述上腔体上;所述真空部包括真空泵、真空罐和所述带阀导气管,所述真空泵与所述真空罐连接,所述真空罐通过所述带阀导气管连接在所述上腔体的下端和所述下腔体的上端。A differential pressure anti-gravity filling and solidification device under the action of an external field is characterized in that it comprises: a solidification cavity, a high pressure part, a low pressure part and a vacuum part, the solidification cavity comprises: an upper cavity and a lower cavity, the The upper cavity is provided with a casting mold, the upper cavity and the lower cavity are connected by an intermediate plate, and an infusion tube is arranged between the upper cavity and the lower cavity, and the infusion tube passes through the intermediate plate The lower end of the lower cavity is provided with a hydraulic lifting platform, the upper end of the hydraulic lifting platform is provided with a melting crucible, the bottom of the lower cavity is provided with an induction melting device, and the upper end of the induction melting device is provided with an electromagnetic a stirring device, the lower cavity is provided with an induction electric inlet at the corresponding position of the electromagnetic stirring device and the induction melting device; the high pressure part includes a constant pressure high pressure tank and a valved air duct, the constant pressure high pressure tank The lower ends of the upper cavity and the lower cavity are connected through the valved air conduit; the low pressure part includes a constant pressure low pressure tank and the valved air conduit, and the constant pressure low pressure tank passes through the belt The valve air conduit is connected to the upper cavity; the vacuum part includes a vacuum pump, a vacuum tank and the valved air conduit, the vacuum pump is connected to the vacuum tank, and the vacuum tank passes through the valved air conduit connected to the lower end of the upper cavity and the upper end of the lower cavity.
- 根据权利要求1所述的一种外场作用下差压反重力充型凝固装置,其特征在于,所述电磁搅拌装置的水冷套的材料为奥氏体不锈钢;所述下腔体的上端设有石英玻璃观察孔。A differential pressure anti-gravity filling and solidification device under the action of an external field according to claim 1, wherein the material of the water cooling jacket of the electromagnetic stirring device is austenitic stainless steel; the upper end of the lower cavity is provided with Quartz glass viewing port.
- 根据权利要求1所述的一种外场作用下差压反重力充型凝固装置,其特征在于,所述恒压高压罐内为高压氩气;所述恒压低压罐内为低压氩气。A differential pressure anti-gravity filling and solidification device under the action of an external field according to claim 1, wherein the constant pressure high pressure tank contains high pressure argon gas; the constant pressure low pressure tank contains low pressure argon gas.
- 一种如权利要求1-3任意权利要求所述一种外场作用下差压反重力充型凝固装置的凝固工艺,其特征在于该凝固工艺步骤包括:A solidification process of a differential pressure anti-gravity filling solidification device under the action of an external field as described in any of claims 1-3, wherein the solidification process step comprises:步骤S1:将铝合金原料或纯铝及相关元素的中间合金烘干和除去表面杂质后投入所述熔炼坩埚,启动所述感应熔炼装置将原料熔化成液体,然后利用所述液压升降平台将所述熔炼坩埚升起,利用变质剂进行变质,利用纯度大于99.99%的高纯氩气旋转喷吹进行除气,然后进行除渣;Step S1: put the aluminum alloy raw material or the intermediate alloy of pure aluminum and related elements into the smelting crucible after drying and removing surface impurities, start the induction melting device to melt the raw material into liquid, and then use the hydraulic lifting platform to melt the raw material into a liquid. The smelting crucible is lifted up, metamorphic agent is used for metamorphism, and high-purity argon gas with a purity greater than 99.99% is used for degassing, and then slag removal is carried out;步骤S2:除渣后利用所述液压升降平台将所述熔炼坩埚降至所述感应熔炼装置处,封闭所述中间板,安装所述输液管、所述铸型和所述上部腔体后抽真空;Step S2: After slag removal, use the hydraulic lifting platform to lower the melting crucible to the induction melting device, close the middle plate, install the infusion pipe, the mold and the upper cavity, and then pump vacuum;步骤S3:启动所述感应熔炼装置将金属液升至预定温度后保持等温静置一段时间;Step S3: start the induction smelting device to raise the molten metal to a predetermined temperature and keep it isothermally for a period of time;步骤S4:利用所述液压升降平台将所述熔炼坩埚升至外场作用区域,启动电磁场对熔体进行处理,深度去除熔体中的气体,保持合金成分和熔体温度的均匀性;Step S4: using the hydraulic lifting platform to lift the smelting crucible to the external field action area, start the electromagnetic field to process the melt, deeply remove the gas in the melt, and maintain the uniformity of alloy composition and melt temperature;步骤S5:外场作用一定时间后,停止电磁搅拌,静置一段时间,然后利用所述恒压高压罐将所述上腔体和所述下腔体同时通入纯度大于99.99%的高纯氩气;Step S5: After the external field acts for a certain period of time, stop the electromagnetic stirring, let it stand for a period of time, and then use the constant pressure high-pressure tank to pass high-purity argon gas with a purity greater than 99.99% into the upper cavity and the lower cavity at the same time ;步骤S6:利用所述恒压低压罐使所述上腔体减压,利用所述下腔体和所述上腔体之间的氩气压力差将铝合金熔液压入所述铸型进行浇铸,浇铸时间为10-25s,保压时间为5~15min;待熔液凝固形成铸件后卸压,打开上腔取出铸件。Step S6: use the constant-pressure low-pressure tank to decompress the upper cavity, and use the argon pressure difference between the lower cavity and the upper cavity to pour aluminum alloy melt into the mold for casting , the casting time is 10-25s, and the pressure holding time is 5-15min; after the melt solidifies to form a casting, the pressure is relieved, and the upper cavity is opened to take out the casting.
- 根据权利要求4所述的一种外场作用下差压反重力充型凝固装置的凝固工艺,其特征在于,步骤S1中合金熔体变质剂可采用Al-Ti-B、Al-Sr或Al-RE中间合金。铝合金可以采用ZL114A、ZL205A、ZL104A、ZL101、A356和A357等铝合金。The solidification process of a differential pressure anti-gravity filling solidification device under the action of an external field according to claim 4, characterized in that in step S1, the alloy melt modifier can be Al-Ti-B, Al-Sr or Al- RE master alloy. Aluminum alloys such as ZL114A, ZL205A, ZL104A, ZL101, A356 and A357 can be used.
- 根据权利要求4所述的一种外场作用下差压反重力充型凝固装置的凝固工艺,其特征在于,步骤S2中真空度为10-40Pa。The solidification process of a differential pressure anti-gravity filling solidification device under the action of an external field according to claim 4, wherein the degree of vacuum in step S2 is 10-40 Pa.
- 根据权利要求4所述的一种外场作用下差压反重力充型凝固装置的凝固工艺,其特征在于,步骤S3中真空条件下铝合金熔体等温静置时间为18-25min。The solidification process of a differential pressure antigravity filling and solidification device under the action of an external field according to claim 4, wherein the isothermal standing time of the aluminum alloy melt under the vacuum condition in step S3 is 18-25min.
- 根据权利要求4所述的一种外场作用下差压反重力充型凝固装置的凝固工艺,其特征在于,步骤S4中熔体达到TL以上80~100℃时启动电磁搅拌装置对熔体进行电磁搅拌,中心磁感应强度为0~30mT,电磁场作用时间1~5min。The solidification process of a differential pressure anti-gravity filling and solidifying device under the action of an external field according to claim 4, wherein in step S4, when the melt reaches 80-100°C above TL, an electromagnetic stirring device is started to electromagnetically conduct the melt on the melt. Stir, the central magnetic induction intensity is 0 ~ 30mT, and the electromagnetic field action time is 1 ~ 5min.
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