WO2022041624A1 - 一种卷烟接装纸粘唇力的检测方法 - Google Patents
一种卷烟接装纸粘唇力的检测方法 Download PDFInfo
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- WO2022041624A1 WO2022041624A1 PCT/CN2020/141631 CN2020141631W WO2022041624A1 WO 2022041624 A1 WO2022041624 A1 WO 2022041624A1 CN 2020141631 W CN2020141631 W CN 2020141631W WO 2022041624 A1 WO2022041624 A1 WO 2022041624A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- tipping paper
- lip
- cigarette tipping
- grade
- artificial saliva
- Prior art date
Links
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 88
- 238000000034 method Methods 0.000 title claims abstract description 50
- 239000000120 Artificial Saliva Substances 0.000 claims abstract description 69
- 238000007639 printing Methods 0.000 claims abstract description 27
- 239000011248 coating agent Substances 0.000 claims abstract description 15
- 238000000576 coating method Methods 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- 238000005259 measurement Methods 0.000 claims abstract 2
- 239000000123 paper Substances 0.000 claims description 147
- 238000012360 testing method Methods 0.000 claims description 73
- 230000002745 absorbent Effects 0.000 claims description 38
- 239000002250 absorbent Substances 0.000 claims description 38
- 238000005520 cutting process Methods 0.000 claims description 20
- 238000004049 embossing Methods 0.000 claims description 11
- 230000008569 process Effects 0.000 claims description 10
- 230000035699 permeability Effects 0.000 claims description 9
- 239000011111 cardboard Substances 0.000 claims description 7
- 239000011087 paperboard Substances 0.000 claims description 7
- 238000007790 scraping Methods 0.000 claims description 7
- 230000035945 sensitivity Effects 0.000 claims description 7
- 210000003296 saliva Anatomy 0.000 claims description 6
- 238000010008 shearing Methods 0.000 claims description 5
- 238000005303 weighing Methods 0.000 claims description 5
- 239000004753 textile Substances 0.000 claims description 3
- 238000011156 evaluation Methods 0.000 abstract description 9
- 238000001514 detection method Methods 0.000 abstract description 8
- 239000000463 material Substances 0.000 abstract description 6
- 241000208125 Nicotiana Species 0.000 abstract description 4
- 235000002637 Nicotiana tabacum Nutrition 0.000 abstract description 4
- 238000010521 absorption reaction Methods 0.000 abstract description 4
- 238000012545 processing Methods 0.000 abstract description 3
- 238000003908 quality control method Methods 0.000 abstract description 3
- 230000001953 sensory effect Effects 0.000 abstract description 3
- 238000004458 analytical method Methods 0.000 abstract description 2
- 238000005516 engineering process Methods 0.000 abstract description 2
- 230000000391 smoking effect Effects 0.000 abstract 2
- 238000009472 formulation Methods 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- 230000000694 effects Effects 0.000 description 3
- 239000003205 fragrance Substances 0.000 description 3
- 238000012216 screening Methods 0.000 description 3
- 238000004364 calculation method Methods 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 230000001681 protective effect Effects 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical class [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 235000008331 Pinus X rigitaeda Nutrition 0.000 description 1
- 235000011613 Pinus brutia Nutrition 0.000 description 1
- 241000018646 Pinus brutia Species 0.000 description 1
- 229920006221 acetate fiber Polymers 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000740 bleeding effect Effects 0.000 description 1
- 238000012512 characterization method Methods 0.000 description 1
- 239000007799 cork Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N5/00—Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid
- G01N5/02—Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid by absorbing or adsorbing components of a material and determining change of weight of the adsorbent, e.g. determining moisture content
Definitions
- the invention belongs to the technical field of analysis and detection, and in particular relates to a method for detecting the lip sticking force of cigarette tipping paper.
- the cigarette filter is mainly composed of three layers of acetate fiber, forming paper and tipping paper.
- the tipping paper also known as tipping paper, is used to wrap around the filter tip and bond the filter tip to the end of the tobacco rod.
- the tipping paper is a kind of decorative paper obtained by printing, coating and other processing on the base paper. It is usually cork color or opaque white, and has the effect of improving the appearance.
- the tipping paper is in direct contact with the lips of the smoker. Generally, only paint or ink is used for printing on the tipping paper. When the weather is dry, when consumers smoke cigarettes, there may be a small amount of saliva that will wet the tipping paper.
- the research hotspots of cigarette filter tipping paper at home and abroad mostly focus on its pyrolysis properties, low ignition properties, harmful element content, modification of cigarette paper and the release ability of modified carbon monoxide, toxicity and safety evaluation etc.
- the lip sticking aspect is all about improving the formulation and process of the butt-loading paper, and there is no specific screening method or judgment method.
- the invention patent "a fragrance and health tipping paper that prevents the lips and tongue from drying out and its preparation method” describes the technological formula of tipping paper, but only the longitudinal tensile strength and air permeability of the base paper are detected in the effect test. , there is no mention of whether there is a sticky lip force.
- the utility model patent "a filter with anti-sticking lip and anti-pollution” is coated with a protective film on the tipping paper and "a multifunctional tipping paper” for the purpose of anti-sticking lip, fragrance, flame retardant, etc.
- the outer layer of the pine paper is compounded with a fruit fragrance waterproof layer and a protective film layer, but the judgment result of the anti-stick lip is not mentioned.
- the purpose of the present invention is to solve the deficiencies of the prior art and provide a method for detecting the lip sticking force of cigarette tipping paper.
- the lip stickiness of cigarette tipping paper is closely related to the processing technology. Adding a certain waterproof material to the printed coating surface can effectively prevent the tipping paper from sticking to the lip. Therefore, its stickiness can be objectively characterized by the water absorption/waterproof performance of the printed surface.
- the lip stickiness grade of cigarette tipping paper is obtained.
- the method is simple, feasible and easy to popularize and apply. At the same time, this method can well avoid the influence of subjective factors and differential characterization brought by the traditional artificial sensory evaluation, and has advantages in material access, quality control, and upgraded products in the tobacco industry.
- a method for detecting lip sticking force of cigarette tipping paper comprising the following steps:
- Step (1) cutting the cigarette tipping paper
- Step (2) the cut test sample is weighed
- Step (3) place the cut test sample flat on the coating platform covered with absorbent paper, with the printing surface facing up, accurately pipette a certain amount of artificial saliva, evenly smear it on the printing surface of the tipping paper, and finish scraping. Time to start timing, let it stand for a while;
- Step (4) when the specified time of standing is reached, place a piece of absorbent paper on the surface of the test sample, then immediately press a certain weight on the absorbent paper and time, and let it stand for a period of time;
- Step (5) when reaching the specified time, the test sample penetrated by artificial saliva is weighed;
- Step (6) after artificial saliva penetrates on the surface of the cigarette tipping paper, the mass increase percentage of the cigarette tipping paper is calculated according to formula (1);
- step (7) the lip sticking force grade is measured according to the artificial saliva permeability.
- the sample is placed on a shearing board for cutting, and it is cut into rectangular strips with a length of 50-300 mm and a width of 10-50 mm, and the size deviation should be within ⁇ 0.05 mm. , the cut test sample shall not cover the perforated part of the cigarette tipping paper.
- step (2) and step (5) an analytical balance is used for weighing, and the sensitivity of the analytical balance is not less than 0.1 mg.
- step (3) and step (4) a stopwatch is used for timekeeping.
- the coating platform is an embossing bed, and the area size of the embossing bed is larger than the size of the cut sample, and is placed horizontally with a flat surface.
- the absorbent paper meets the requirements of the absorbent paper in "GB/T1540 Determination of Water Absorbency of Paper and Cardboard, Kebo Method”; Artificial saliva formulation and process preparation in Color Fastness to Saliva.
- the suction amount of artificial saliva is determined according to the size of the cut sample, ranging from 10 to 1000 ⁇ L, which can evenly smear the printing surface of the cut sample.
- step (3) the standing time is 5-30 s; in step (4), the standing time is 5-30 s.
- the size of the weight can completely cover the size of the test sample, and the weight is 500-3000 g.
- the determination of the lip sticking force grade is: when the mass increase percentage is less than 4.0%, the result of the lip stickiness grade is determined to be 0, showing that the lip does not stick; when the mass increase percentage is When 4.0% to 7.0%, the result of the lip stickiness grade is determined to be grade 1, showing mild lip stickiness; when the mass increase percentage is 7.0% to 10.0%, the result of the lip stickiness grade is determined to be grade 2, showing moderate lip stickiness. Sticky lips; when the mass increase percentage is 10.0% to 13.0%, the result of the stickiness grade is determined to be grade 3, showing severe stickiness; when the mass increase percentage is greater than 13.0%, the result of the stickiness grade is determined to be grade 4, Severe sticky lips.
- Gloves should be worn throughout the detection operation of the present invention to avoid direct contact between hands and the test sample.
- the present invention has the following beneficial effects:
- the present invention provides a method for detecting the lip-sticking force of cigarette tipping paper, which can objectively and accurately detect whether the tipping paper has the lip-sticking force, and can effectively avoid the traditional sensory evaluation to obtain a sticky lip feeling and difficult to spit.
- the subjective factors have a greater influence, the results of the taste are very different, and it is harmful to human health.
- the present invention coats the artificial saliva on the printing surface of the cigarette tipping paper sample according to the prescribed amount, makes it absorb a certain amount of artificial saliva within the specified time, and respectively weighs the quality of the cigarette tipping paper surface before and after infiltration, and calculates.
- the mass increase percentage of the cigarette tipping paper, and the lip stickiness grade of the cigarette tipping paper is obtained according to the determination principle.
- the method is simple and feasible, and has certain advantages in material access, quality control and upgraded products in the tobacco industry.
- the method of the present invention is fast, objective, efficient, has good repeatability, is simple to operate, greatly saves detection costs, improves efficiency, and is easy to popularize and apply.
- a method for detecting lip sticking force of cigarette tipping paper comprising the following steps:
- Step (1) cutting the cigarette tipping paper
- Step (2) the cut test sample is weighed
- Step (3) place the cut test sample flat on the coating platform covered with absorbent paper, with the printing surface facing up, accurately pipette a certain amount of artificial saliva, evenly smear it on the printing surface of the tipping paper, and finish scraping. Time to start timing, let it stand for a while;
- Step (4) when the specified time of standing is reached, place a piece of absorbent paper on the surface of the test sample, then immediately press a certain weight on the absorbent paper and time, and let it stand for a period of time;
- Step (5) when reaching the specified time, the test sample penetrated by artificial saliva is weighed;
- Step (6) after artificial saliva penetrates on the surface of the cigarette tipping paper, the mass increase percentage of the cigarette tipping paper is calculated according to formula (1);
- step (7) the lip sticking force grade is measured according to the artificial saliva permeability.
- a method for detecting lip sticking force of cigarette tipping paper comprising the following steps:
- Step (1) cutting the cigarette tipping paper
- Step (2) the cut test sample is weighed
- Step (3) place the cut test sample flat on the coating platform covered with absorbent paper, with the printing surface facing up, accurately pipette a certain amount of artificial saliva, evenly smear it on the printing surface of the tipping paper, and finish scraping. Time to start timing, let it stand for a while;
- Step (4) when the specified time of standing is reached, place a piece of absorbent paper on the surface of the test sample, then immediately press a certain weight on the absorbent paper and time, and let it stand for a period of time;
- Step (5) when reaching the specified time, the test sample penetrated by artificial saliva is weighed;
- Step (6) after artificial saliva penetrates on the surface of the cigarette tipping paper, the mass increase percentage of the cigarette tipping paper is calculated according to formula (1);
- step (7) the lip sticking force grade is measured according to the artificial saliva permeability.
- step (1) put the sample on the shearing board for cutting, and cut it into a rectangular strip with a length of 50mm and a width of 10mm.
- the size deviation should be within ⁇ 0.05mm, and the test sample after cutting should have no Cover the punched area of the cigarette tipping paper.
- step (2) and step (5) an analytical balance is used for weighing, and the sensitivity of the analytical balance is not less than 0.1 mg.
- step (3) and step (4) a stopwatch is used for timing.
- the coating platform is an embossing bed, and the area size of the embossing bed is larger than the size of the cutting sample, and is placed horizontally with a flat surface.
- step (3) the absorbent paper meets the requirements of the absorbent paper in "GB/T1540 Determination of Water Absorbency of Paper and Cardboard"; Artificial saliva formulation and process preparation.
- step (3) the suction volume of artificial saliva is 10 ⁇ L.
- step (3) the standing time is 5s; in step (4), the standing time is 5s.
- step (4) the size of the weight can completely cover the size of the test sample, and the mass is 500g.
- the determination of the lip sticking force grade is as follows: when the mass increase percentage is less than 4.0%, the result of the lip stickiness grade is determined to be grade 0, indicating that the lip does not stick; when the mass increase percentage is 4.0% to 7.0% , the result of the lip stickiness grade is determined to be grade 1, showing mild lip stickiness; when the mass increase percentage is 7.0% to 10.0%, the result of the lip stickiness grade is determined to be grade 2, showing moderate stickiness; When the percentage is 10.0% to 13.0%, the lip stickiness grade is determined to be grade 3, showing severe lip stickiness; when the mass increase percentage is greater than 13.0%, the lip stickiness grade is determined to be grade 4, showing severe lip stickiness.
- a method for detecting lip sticking force of cigarette tipping paper comprising the following steps:
- Step (1) cutting the cigarette tipping paper
- Step (2) the cut test sample is weighed
- Step (3) place the cut test sample flat on the coating platform covered with absorbent paper, with the printing surface facing up, accurately pipette a certain amount of artificial saliva, evenly smear it on the printing surface of the tipping paper, and finish scraping. Time to start timing, let it stand for a while;
- Step (4) when the specified time of standing is reached, place a piece of absorbent paper on the surface of the test sample, then immediately press a certain weight on the absorbent paper and time, and let it stand for a period of time;
- Step (5) when reaching the specified time, the test sample penetrated by artificial saliva is weighed;
- Step (6) after artificial saliva penetrates on the surface of the cigarette tipping paper, the mass increase percentage of the cigarette tipping paper is calculated according to formula (1);
- step (7) the lip sticking force grade is measured according to the artificial saliva permeability.
- step (1) put the sample on the shearing board for cutting, and cut it into a wide rectangular strip with a length of 300mm and a width of 50mm.
- the size deviation should be within ⁇ 0.05mm, and the test sample after cutting should have no Cover the punched area of the cigarette tipping paper.
- step (2) and step (5) an analytical balance is used for weighing, and the sensitivity of the analytical balance is not less than 0.1 mg.
- step (3) and step (4) a stopwatch is used for timing.
- the coating platform is an embossing bed, and the area size of the embossing bed is larger than the size of the cut sample, and is placed horizontally with a flat surface.
- step (3) the absorbent paper meets the requirements of the absorbent paper in "GB/T1540 Determination of Water Absorbency of Paper and Cardboard"; Artificial saliva formulation and process preparation.
- step (3) the suction volume of artificial saliva is 1000 ⁇ L, and the printing surface of the cut sample is evenly smeared.
- step (3) the standing time is 5-30 s; in step (4), the standing time is 5-30 s.
- step (4) the size of the weight can completely cover the size of the test sample, and the weight is 500-3000 g.
- the determination of the lip sticking force grade is as follows: when the mass increase percentage is less than 4.0%, the result of the lip stickiness grade is determined to be grade 0, indicating that the lip does not stick; when the mass increase percentage is 4.0% to 7.0% , the result of the lip stickiness grade is determined to be grade 1, showing mild lip stickiness; when the mass increase percentage is 7.0% to 10.0%, the result of the lip stickiness grade is determined to be grade 2, showing moderate stickiness; When the percentage is 10.0% to 13.0%, the lip stickiness grade is determined to be grade 3, showing severe lip stickiness; when the mass increase percentage is greater than 13.0%, the lip stickiness grade is determined to be grade 4, showing severe lip stickiness.
- a method for detecting lip sticking force of cigarette tipping paper comprising the following steps:
- Step (1) cutting the cigarette tipping paper
- Step (2) the cut test sample is weighed
- Step (3) place the cut test sample flat on the coating platform covered with absorbent paper, with the printing surface facing up, accurately pipette a certain amount of artificial saliva, evenly smear it on the printing surface of the tipping paper, and finish scraping. Time to start timing, let it stand for a while;
- Step (4) when the specified time of standing is reached, place a piece of absorbent paper on the surface of the test sample, then immediately press a certain weight on the absorbent paper and time, and let it stand for a period of time;
- Step (5) when reaching the specified time, the test sample penetrated by artificial saliva is weighed;
- Step (6) after artificial saliva penetrates on the surface of the cigarette tipping paper, the mass increase percentage of the cigarette tipping paper is calculated according to formula (1);
- step (7) the lip sticking force grade is measured according to the artificial saliva permeability.
- step (1) put the sample on the shearing board for cutting, and cut it into a wide rectangular strip with a length of 200mm and a width of 30mm.
- the size deviation should be within ⁇ 0.05mm, and the test sample after cutting should have no Cover the punched area of the cigarette tipping paper.
- step (2) and step (5) an analytical balance is used for weighing, and the sensitivity of the analytical balance is not less than 0.1 mg.
- step (3) and step (4) a stopwatch is used for timing.
- the coating platform is an embossing bed, and the area size of the embossing bed is larger than the size of the cut sample, and is placed horizontally with a flat surface.
- step (3) the absorbent paper meets the requirements of the absorbent paper in "GB/T1540 Determination of Water Absorbency of Paper and Cardboard"; Artificial saliva formulation and process preparation.
- step (3) the suction amount of artificial saliva is determined according to the size of the cut sample, in the range of 10-1000 ⁇ L, which can evenly smear the printing surface of the cut sample.
- step (3) the standing time is 15s; in step (4), the standing time is 20s.
- step (4) the size of the weight can completely cover the size of the test sample, and the mass is 2000g.
- the determination of the lip sticking force grade is as follows: when the mass increase percentage is less than 4.0%, the result of the lip stickiness grade is determined to be grade 0, indicating that the lip does not stick; when the mass increase percentage is 4.0% to 7.0% , the result of the lip stickiness grade is determined to be grade 1, showing mild lip stickiness; when the mass increase percentage is 7.0% to 10.0%, the result of the lip stickiness grade is determined to be grade 2, showing moderate stickiness; When the percentage is 10.0% to 13.0%, the lip stickiness grade is determined to be grade 3, showing severe lip stickiness; when the mass increase percentage is greater than 13.0%, the sticky lip grade result is determined to be grade 4, showing severe lip stickiness
- a method for detecting lip sticking force of cigarette tipping paper comprising the following steps:
- Step (1) cut the cigarette tipping paper; put the sample on the cutting board, cut a number of rectangular strips with a sample size of 15mm ⁇ 100mm (the size deviation should be within ⁇ 0.5mm), and test the sample.
- the punched parts of the cigarette tipping paper should be avoided.
- Step (2) the cut test sample is weighed on an analytical balance with a sense of 0.1 mg
- Step (3) place the cut test sample flat on the imprinting bed (there is already a piece of absorbent paper), with the printing surface facing up, accurately remove 20 ⁇ L of artificial saliva, evenly smear it on the printing surface of the tipping paper, scrape coating At the end of the time, turn on the stopwatch and let it stand for 10s; among them, the absorbent paper meets the requirements of the absorbent paper in "GB/T1540 Determination of Water Absorption of Paper and Cardboard by Kebo Method".
- Artificial saliva prepared according to the formula and process of artificial saliva in "GBT18886-2002 Color fastness of textiles to color fastness to saliva”.
- Step (4) after reaching the time of 10s, place a piece of absorbent paper on the surface of the test sample, then immediately press the absorbent paper and the test sample with a 2000g weight, turn on the stopwatch, and let it stand for 10s;
- step (5) when the prescribed time reaches 10s, the test sample permeated by artificial saliva is weighed on an analytical balance with a sensitivity of 0.1 mg.
- Step (6) after the artificial saliva penetrates on the surface of the cigarette tipping paper, the mass increase percentage of the cigarette tipping paper is according to the formula:
- Step (7) according to the artificial saliva permeability, carry out the mensuration of the sticking lip force grade according to the measuring standard:
- the lip stickiness grade is judged to be grade 0, which means that the lip is not sticky.
- a method for measuring lip sticking force of cigarette tipping paper comprising the following steps:
- Step (1) cut the cigarette tipping paper; put the sample on the cutting board, cut a number of rectangular strips with a sample size of 20mm ⁇ 200mm (the size deviation should be within ⁇ 0.5mm), and test the sample.
- the punched parts of the cigarette tipping paper should be avoided.
- Step (2) the cut test sample is weighed on an analytical balance with a sense of 0.1 mg
- Step (3) place the cut test sample flat on the embossing bed covered with absorbent paper, with the printing surface facing up, accurately pipette 50 ⁇ L of artificial saliva, apply it evenly on the printing surface of the tipping paper, and open it at the end of scraping. Stopwatch time, let stand for 20s; Among them, absorbent paper, meet the requirements of absorbent paper in "GB/T1540 Determination of Water Absorption of Paper and Cardboard by Kebo Method". Artificial saliva, prepared according to the formula and process of artificial saliva in "GBT18886-2002 Color fastness of textiles to color fastness to saliva”.
- Step (4) after reaching the time of 20s, place a piece of absorbent paper on the surface of the test sample, then immediately press the absorbent paper and the test sample with a 3000g weight, turn on the stopwatch, and let it stand for 20s;
- step (5) when the prescribed time reaches 20s, the test sample permeated by artificial saliva is weighed on an analytical balance with a sensitivity of 0.1 mg.
- Step (6) after the artificial saliva penetrates on the surface of the cigarette tipping paper, the mass increase percentage of the cigarette tipping paper is according to the formula:
- M test the mass of the test sample after the artificial saliva penetrates the surface of the cigarette tipping paper, in grams (g);
- Step (7) according to the artificial saliva permeability, carry out the mensuration of the sticking lip force grade according to the measuring standard:
- the lip stickiness grade is judged to be grade 0, which means that the lip is not sticky.
- the detection method of the present invention is basically consistent with the manual suction test results.
- the method of the present invention can objectively and accurately detect whether the mounting paper has a lip sticking force, and is easy to popularize and apply.
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- General Health & Medical Sciences (AREA)
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Abstract
本发明涉及一种卷烟接装纸粘唇力的检测方法，属于分析检测技术领域。该方法经反复评吸和试样对比，发现卷烟接装纸粘唇性与加工工艺密切相关，印刷涂层面中加入一定的防水材料，可有效避免接装纸粘唇。因此可通过印刷面的吸水/防水性能客观表征其粘唇性。将人工唾液按照规定的用量涂布在卷烟接装纸试样印刷面，在规定时间内使其吸收一定量的人工唾液，分别称量卷烟接装纸表面渗透前后的质量，计算卷烟接装纸的质量增长百分比，得出卷烟接装纸粘唇性等级。本发明方法快速、简便，且重复性好，可以避免传统的借助人工感官评吸带来的主观因素影响和差异性表征，而且大大节省了检测成本，在烟草行业物料准入、质量管控、升级产品中具有优势。
Description
本发明属于分析检测技术领域，具体涉及一种卷烟接装纸粘唇力的检测方法。
卷烟滤嘴主要是由醋酸纤维、成型纸、接装纸三层组成。其中接装纸，又名水松纸，用于包裹在过滤嘴外面并将滤嘴粘接到烟条末端。接装纸是通过对接装原纸进行印刷涂布及其他方式加工后得到的一种装潢纸，常为软木色或不透明的白色，具有改善外观的作用。接装纸同吸烟者嘴唇直接接触，接装纸上一般仅使用涂料或者油墨进行印刷，在天气干燥时，消费者吸食卷烟的时候，由于可能会有少量唾液将接装纸蘸湿，在吸烟过程中又慢慢干燥，在嘴唇残留的唾液蛋白质会对接装纸有粘合作用，导致滤嘴上的接装纸粘连在嘴唇皮肤上，甚至粘扯嘴唇出现撕破、出血的现象，吸食完后不能将滤嘴顺利吐出，严重影响卷烟消费体验感。
目前，国内外卷烟滤嘴接装纸的研究热点多集中于其热解特性、低引燃性、有害元素含量、卷烟纸改性及改性后一氧化碳的释放能力、毒理性及安全性评价等方面。而其粘唇力的筛选或者判定没有相关的研究，涉及粘唇方面均是对接装纸的配方和工艺进行改进，并没有具体的筛选方法或者是判定方法。例如发明专利“一种不粘嘴防止唇舌干燥的香味保健水松纸及其制备方法”中描述了水松纸的工艺配方，但在效果检测上只是检测了原纸的纵向抗张强度和透气度，没有提及是否有粘唇力的判定。实用新型专利“一种防粘唇防污染的过滤嘴”在水松纸外涂上一层保护膜和“一种多功能水松纸”目的是防粘唇、赋香、阻燃等，在水松纸外层复合水果香防水层和防护膜层，但并未提及防粘唇的判定结果。行业内也没有相应的标准进行规范，各大企业仅凭专业人员的评吸判断，具有很大的主观性和不确定性，为了能判定不同工艺、不同类型接装纸是否对嘴唇有粘粘性/力，亟需建立相应客观的筛选检测方法。
发明内容
本发明的目的是为了解决现有技术的不足，提供一种卷烟接装纸粘唇力的检测方法。该方法经反复评吸和试样对比，发现卷烟接装纸粘唇性与加工工艺密切相关，印刷涂层面中加入一定的防水材料，可有效避免接装纸粘唇。因此可通过印刷面的吸水/防水性能客观表征其粘唇性。将人工唾液按照规定的用量 涂布在卷烟接装纸试样印刷面，在规定时间内使其吸收一定量的人工唾液，分别称量卷烟接装纸表面渗透前后的质量，计算卷烟接装纸的质量增长百分比，根据检测原则得出卷烟接装纸粘唇性等级。该方法简单可行，易于推广应用。同时，该方法可以很好的避免传统的借助人工感官评吸带来的主观因素影响和差异性表征，在烟草行业物料准入、质量管控、升级产品中具有优势。
为实现上述目的，本发明采用的技术方案如下：
一种卷烟接装纸粘唇力的检测方法，包括如下步骤：
步骤(1)，对卷烟接装纸进行剪裁；
步骤(2)，将裁好的测试样品进行称重；
步骤(3)，将裁好的测试样品平整放置于铺有吸水纸的涂布平台上，印刷面朝上，准确移取一定量的人工唾液，均匀涂抹于接装纸印刷面，刮涂结束时开始计时，静置一段时间；
步骤(4)，达到静置的规定时间时，在测试样品表面放置一张吸水纸，然后立即用一定重量砝码压在吸水纸上并计时，静置一段时间；
步骤(5)，达到规定时间时，将经人工唾液渗透过的测试样品进行称重；
步骤(6)，人工唾液在卷烟接装纸表面渗透后，卷烟接装纸的质量增长百分比按照公式(1)计算；
式(1)中：
ω——质量增长百分比；
M
测——人工唾液在卷烟接装纸表面渗透后测试样品的质量，单位为克(g)；
M
空——人工唾液在卷烟接装纸表面渗透前测试样品的质量，单位为克(g)；
步骤(7)，根据人工唾液渗透率进行粘唇力等级的测定。
进一步，优选的是，步骤(1)中，将样品放在剪切板上进行剪裁，裁切成长度为50～300mm和宽度为10～50mm的长方形宽条，尺寸偏差应在±0.05mm之内，剪裁完成后的测试样品应没有覆盖卷烟接装纸的打孔部位。
进一步，优选的是，步骤(2)和步骤(5)中，称重采用分析天平，分析天平的感量不低于0.1mg。
进一步，优选的是，步骤(3)和步骤(4)中，计时采用秒表计时。
进一步，优选的是，步骤(3)中，涂布平台为压印床，压印床的面积尺寸要大于裁剪样品的尺寸，且水平放置，表面平整。
进一步，优选的是，步骤(3)中，吸水纸满足《GB/T1540纸和纸板吸水性的测定法可勃法》中吸水纸的要求；人工唾液按照《GBT18886-2002纺织品色牢度试验耐唾液色牢度》中人工唾液配方和工艺制备。
进一步，优选的是，步骤(3)中，人工唾液的吸取量按照裁剪样品的尺寸大小定，范围10～1000μL，能均匀涂抹裁剪样品的印刷面。
进一步，优选的是，步骤(3)中，静置时间为5～30s；步骤(4)中，静置时间为5～30s。
进一步，优选的是，步骤(4)中，砝码大小能完全覆盖测试样品尺寸，且质量为500～3000g。
进一步，优选的是，步骤(7)中，粘唇力等级的测定为：当质量增长百分比小于4.0％时，确定粘唇性等级结果为0级，表现为不粘唇；当质量增长百分比为4.0％～7.0％时，确定粘唇性等级结果为1级，表现为轻度粘唇；当质量增长百分比为7.0％～10.0％时，确定粘唇性等级结果为2级，表现为中度粘唇；当质量增长百分比为10.0％～13.0％时，确定粘唇性等级结果为3级，表现为重度粘唇；当质量增长百分比大于13.0％时，确定粘唇性等级结果为4级，表现为严重粘唇。
本发明检测操作过程中应全程佩戴手套，避免手与测试样品直接接触。
本领域技术人员应该知晓卷烟接装纸上通常存在打孔部位，多数位于卷烟接装纸的两侧。
本发明与现有技术相比，其有益效果为：
1.本发明提供一种卷烟接装纸粘唇力的检测方法，能客观、准确对接装纸是否有粘唇力进行检测，能有效避免传统的借助感官评价得出有粘唇感、难吐感等模糊概念，且主观因素影响较大，品吸结果差异大，对人体健康有害等弊端。
2.本发明将人工唾液按照规定的用量涂布在卷烟接装纸试样印刷面，在规定时间内使其吸收一定量的人工唾液，分别称量卷烟接装纸表面渗透前后的质量，计算卷烟接装纸的质量增长百分比，根据测定原则得出卷烟接装纸粘唇性等级。方法简单可行，在烟草行业物料准入、质量管控、升级产品中具有一定优势。
3.本发明方法快速、客观、高效，且重复性好、操作简单，而且大大节省了检测成本，提高了效率，易于推广应用。
下面结合实施例对本发明作进一步的详细描述。
本领域技术人员将会理解，下列实施例仅用于说明本发明，而不应视为限定本发明的范围。实施例中未注明具体技术或条件者，按照本领域内的文献所描述的技术或条件或者按照产品说明书进行。所用材料或设备未注明生产厂商者，均为可以通过购买获得的常规产品。
以下实施例中未有特别说明，百分比均为重量百分比。
实施例1
一种卷烟接装纸粘唇力的检测方法，包括如下步骤：
步骤(1)，对卷烟接装纸进行剪裁；
步骤(2)，将裁好的测试样品进行称重；
步骤(3)，将裁好的测试样品平整放置于铺有吸水纸的涂布平台上，印刷面朝上，准确移取一定量的人工唾液，均匀涂抹于接装纸印刷面，刮涂结束时开始计时，静置一段时间；
步骤(4)，达到静置的规定时间时，在测试样品表面放置一张吸水纸，然后立即用一定重量砝码压在吸水纸上并计时，静置一段时间；
步骤(5)，达到规定时间时，将经人工唾液渗透过的测试样品进行称重；
步骤(6)，人工唾液在卷烟接装纸表面渗透后，卷烟接装纸的质量增长百分比按照公式(1)计算；
式(1)中：
ω——质量增长百分比；
M
测——人工唾液在卷烟接装纸表面渗透后测试样品的质量，单位为克；
M
空——人工唾液在卷烟接装纸表面渗透前测试样品的质量，单位为克；
步骤(7)，根据人工唾液渗透率进行粘唇力等级的测定。
实施例2
一种卷烟接装纸粘唇力的检测方法，包括如下步骤：
步骤(1)，对卷烟接装纸进行剪裁；
步骤(2)，将裁好的测试样品进行称重；
步骤(3)，将裁好的测试样品平整放置于铺有吸水纸的涂布平台上，印刷面朝上，准确移取一定量的人工唾液，均匀涂抹于接装纸印刷面，刮涂结束时开始计时，静置一段时间；
步骤(4)，达到静置的规定时间时，在测试样品表面放置一张吸水纸，然后立即用一定重量砝码压在吸水纸上并计时，静置一段时间；
步骤(5)，达到规定时间时，将经人工唾液渗透过的测试样品进行称重；
步骤(6)，人工唾液在卷烟接装纸表面渗透后，卷烟接装纸的质量增长百分比按照公式(1)计算；
式(1)中：
ω——质量增长百分比；
M
测——人工唾液在卷烟接装纸表面渗透后测试样品的质量，单位为克；
M
空——人工唾液在卷烟接装纸表面渗透前测试样品的质量，单位为克；
步骤(7)，根据人工唾液渗透率进行粘唇力等级的测定。
步骤(1)中，将样品放在剪切板上进行剪裁，裁切成长度为50mm和宽度为10mm的长方形宽条，尺寸偏差应在±0.05mm之内，剪裁完成后的测试样品应没有覆盖卷烟接装纸的打孔部位。
步骤(2)和步骤(5)中，称重采用分析天平，分析天平的感量不低于0.1mg。
步骤(3)和步骤(4)中，计时采用秒表计时。
步骤(3)中，涂布平台为压印床，压印床的面积尺寸要大于裁剪样品的尺寸，且水平放置，表面平整。
步骤(3)中，吸水纸满足《GB/T1540纸和纸板吸水性的测定法可勃法》中吸水纸的要求；人工唾液按照《GBT18886-2002纺织品色牢度试验耐唾液色牢度》中人工唾液配方和工艺制备。
步骤(3)中，人工唾液的吸取量为10μL。
步骤(3)中，静置时间为5s；步骤(4)中，静置时间为5s。
步骤(4)中，砝码大小能完全覆盖测试样品尺寸，且质量为500g。
步骤(7)中，粘唇力等级的测定为：当质量增长百分比小于4.0％时，确 定粘唇性等级结果为0级，表现为不粘唇；当质量增长百分比为4.0％～7.0％时，确定粘唇性等级结果为1级，表现为轻度粘唇；当质量增长百分比为7.0％～10.0％时，确定粘唇性等级结果为2级，表现为中度粘唇；当质量增长百分比为10.0％～13.0％时，确定粘唇性等级结果为3级，表现为重度粘唇；当质量增长百分比大于13.0％时，确定粘唇性等级结果为4级，表现为严重粘唇。
实施例3
一种卷烟接装纸粘唇力的检测方法，包括如下步骤：
步骤(1)，对卷烟接装纸进行剪裁；
步骤(2)，将裁好的测试样品进行称重；
步骤(3)，将裁好的测试样品平整放置于铺有吸水纸的涂布平台上，印刷面朝上，准确移取一定量的人工唾液，均匀涂抹于接装纸印刷面，刮涂结束时开始计时，静置一段时间；
步骤(4)，达到静置的规定时间时，在测试样品表面放置一张吸水纸，然后立即用一定重量砝码压在吸水纸上并计时，静置一段时间；
步骤(5)，达到规定时间时，将经人工唾液渗透过的测试样品进行称重；
步骤(6)，人工唾液在卷烟接装纸表面渗透后，卷烟接装纸的质量增长百分比按照公式(1)计算；
式(1)中：
ω——质量增长百分比；
M
测——人工唾液在卷烟接装纸表面渗透后测试样品的质量，单位为克；
M
空——人工唾液在卷烟接装纸表面渗透前测试样品的质量，单位为克；
步骤(7)，根据人工唾液渗透率进行粘唇力等级的测定。
步骤(1)中，将样品放在剪切板上进行剪裁，裁切成长度为300mm和宽度为50mm的长方形宽条，尺寸偏差应在±0.05mm之内，剪裁完成后的测试样品应没有覆盖卷烟接装纸的打孔部位。
步骤(2)和步骤(5)中，称重采用分析天平，分析天平的感量不低于0.1mg。
步骤(3)和步骤(4)中，计时采用秒表计时。
步骤(3)中，涂布平台为压印床，压印床的面积尺寸要大于裁剪样品的尺寸，且水平放置，表面平整。
步骤(3)中，吸水纸满足《GB/T1540纸和纸板吸水性的测定法可勃法》中吸水纸的要求；人工唾液按照《GBT18886-2002纺织品色牢度试验耐唾液色牢度》中人工唾液配方和工艺制备。
步骤(3)中，人工唾液的吸取量为1000μL，均匀涂抹裁剪样品的印刷面。
步骤(3)中，静置时间为5～30s；步骤(4)中，静置时间为5～30s。
步骤(4)中，砝码大小能完全覆盖测试样品尺寸，且质量为500～3000g。
步骤(7)中，粘唇力等级的测定为：当质量增长百分比小于4.0％时，确定粘唇性等级结果为0级，表现为不粘唇；当质量增长百分比为4.0％～7.0％时，确定粘唇性等级结果为1级，表现为轻度粘唇；当质量增长百分比为7.0％～10.0％时，确定粘唇性等级结果为2级，表现为中度粘唇；当质量增长百分比为10.0％～13.0％时，确定粘唇性等级结果为3级，表现为重度粘唇；当质量增长百分比大于13.0％时，确定粘唇性等级结果为4级，表现为严重粘唇。
实施例4
一种卷烟接装纸粘唇力的检测方法，包括如下步骤：
步骤(1)，对卷烟接装纸进行剪裁；
步骤(2)，将裁好的测试样品进行称重；
步骤(3)，将裁好的测试样品平整放置于铺有吸水纸的涂布平台上，印刷面朝上，准确移取一定量的人工唾液，均匀涂抹于接装纸印刷面，刮涂结束时开始计时，静置一段时间；
步骤(4)，达到静置的规定时间时，在测试样品表面放置一张吸水纸，然后立即用一定重量砝码压在吸水纸上并计时，静置一段时间；
步骤(5)，达到规定时间时，将经人工唾液渗透过的测试样品进行称重；
步骤(6)，人工唾液在卷烟接装纸表面渗透后，卷烟接装纸的质量增长百分比按照公式(1)计算；
式(1)中：
ω——质量增长百分比；
M
测——人工唾液在卷烟接装纸表面渗透后测试样品的质量，单位为克；
M
空——人工唾液在卷烟接装纸表面渗透前测试样品的质量，单位为克；
步骤(7)，根据人工唾液渗透率进行粘唇力等级的测定。
步骤(1)中，将样品放在剪切板上进行剪裁，裁切成长度为200mm和宽度为30mm的长方形宽条，尺寸偏差应在±0.05mm之内，剪裁完成后的测试样品应没有覆盖卷烟接装纸的打孔部位。
步骤(2)和步骤(5)中，称重采用分析天平，分析天平的感量不低于0.1mg。
步骤(3)和步骤(4)中，计时采用秒表计时。
步骤(3)中，涂布平台为压印床，压印床的面积尺寸要大于裁剪样品的尺寸，且水平放置，表面平整。
步骤(3)中，吸水纸满足《GB/T1540纸和纸板吸水性的测定法可勃法》中吸水纸的要求；人工唾液按照《GBT18886-2002纺织品色牢度试验耐唾液色牢度》中人工唾液配方和工艺制备。
步骤(3)中，人工唾液的吸取量按照裁剪样品的尺寸大小定，范围10～1000μL，能均匀涂抹裁剪样品的印刷面。
步骤(3)中，静置时间为15s；步骤(4)中，静置时间为20s。
步骤(4)中，砝码大小能完全覆盖测试样品尺寸，且质量为2000g。
步骤(7)中，粘唇力等级的测定为：当质量增长百分比小于4.0％时，确定粘唇性等级结果为0级，表现为不粘唇；当质量增长百分比为4.0％～7.0％时，确定粘唇性等级结果为1级，表现为轻度粘唇；当质量增长百分比为7.0％～10.0％时，确定粘唇性等级结果为2级，表现为中度粘唇；当质量增长百分比为10.0％～13.0％时，确定粘唇性等级结果为3级，表现为重度粘唇；当质量增长百分比大于13.0％时，确定粘唇性等级结果为4级，表现为严重粘唇
实施例5
一种卷烟接装纸粘唇力的检测方法，包括如下步骤：
步骤(1)，对卷烟接装纸进行剪裁；将样品放在剪切板上，裁切样品尺寸为15mm×100mm的长方形宽条(尺寸偏差应在±0.5mm之内)若干份，测试样品应避开卷烟接装纸的打孔部位。
步骤(2)，将裁好的测试样品在感量0.1mg的分析天平上进行称重；
步骤(3)，将裁好的测试样品平整放置于压印床(已有一张吸水纸)上， 印刷面朝上，准确移取20μL的人工唾液，均匀涂抹于接装纸印刷面，刮涂结束时打开秒表计时，静置10s；其中，吸水纸，满足《GB/T1540纸和纸板吸水性的测定法可勃法》中吸水纸的要求。人工唾液，按照《GBT18886-2002纺织品色牢度试验耐唾液色牢度》中人工唾液配方和工艺制备。
步骤(4)，达到10s时间后，在测试样表面放置一张吸水纸，然后立即用2000g砝码压在吸水纸和测试样上，打开秒表计时，静置10s；
步骤(5)，达到规定时间10s时，将经人工唾液渗透过的测试样在感量0.1mg分析天平上进行称重。
步骤(6)，人工唾液在卷烟接装纸表面渗透后，卷烟接装纸的质量增长百分比按照公式：
式中：
ω——质量增长百分比；
M测——人工唾液在卷烟接装纸表面渗透后测试样的质量，单位为克(g)；
M空——人工唾液在卷烟接装纸表面渗透前测试样的质量，单位为克(g)；
进行计算。
步骤(7)，根据人工唾液渗透率按照测定标准进行粘唇力等级的测定：
当质量增长百分比小于4.0％时，判定粘唇性等级结果为0级，表现为不粘唇。
当质量增长百分比为4.0％～7.0％时，判定粘唇性等级结果为1级，表现为轻度粘唇。
当质量增长百分比为7.0％～10.0％时，判定粘唇性等级结果为2级，表现为中度粘唇。
当质量增长百分比为10.0％～13.0％时，判定粘唇性等级结果为3级，表现为重度粘唇。
当质量增长百分比大于13.0％时，判定粘唇性等级结果为4级，表现为严重粘唇。
本实施例对19个不同样品采用本发明方法和现有人工评吸方法进行检测，检测结果如表1所示。
表1
实施例6
一种卷烟接装纸粘唇力的测定方法，包括如下步骤：
步骤(1)，对卷烟接装纸进行剪裁；将样品放在剪切板上，裁切样品尺寸为20mm×200mm的长方形宽条(尺寸偏差应在±0.5mm之内)若干份，测试样品应避开卷烟接装纸的打孔部位。
步骤(2)，将裁好的测试样品在感量0.1mg的分析天平上进行称重；
步骤(3)，将裁好的测试样品平整放置于铺有吸水纸的压印床上，印刷面朝上，准确移取50μL的人工唾液，均匀涂抹于接装纸印刷面，刮涂结束时打开秒表计时，静置20s；其中，吸水纸，满足《GB/T1540纸和纸板吸水性的测定法可勃法》中吸水纸的要求。人工唾液，按照《GBT18886-2002纺织品色牢度试验耐唾液色牢度》中人工唾液配方和工艺制备。
步骤(4)，达到20s时间后，在测试样表面放置一张吸水纸，然后立即用3000g砝码压在吸水纸和测试样上，打开秒表计时，静置20s；
步骤(5)，达到规定时间20s时，将经人工唾液渗透过的测试样在感量0.1mg分析天平上进行称重。
步骤(6)，人工唾液在卷烟接装纸表面渗透后，卷烟接装纸的质量增长百分比按照公式：
式中：
ω——质量增长百分比；
M测——人工唾液在卷烟接装纸表面渗透后测试样的质量，单位为克(g)；
M空——人工唾液在卷烟接装纸表面渗透前测试样的质量，单位为克(g)；
进行计算。
步骤(7)，根据人工唾液渗透率按照测定标准进行粘唇力等级的测定：
当质量增长百分比小于4.0％时，判定粘唇性等级结果为0级，表现为不粘唇。
当质量增长百分比为4.0％～7.0％时，判定粘唇性等级结果为1级，表现为轻度粘唇。
当质量增长百分比为7.0％～10.0％时，判定粘唇性等级结果为2级，表现为中度粘唇。
当质量增长百分比为10.0％～13.0％时，判定粘唇性等级结果为3级，表现 为重度粘唇。
当质量增长百分比大于13.0％时，判定粘唇性等级结果为4级，表现为严重粘唇。
本实施例对19个不同样品采用本发明方法和现有人工评吸方法进行检测，检测结果如表2所示。
表2
由表1和表2可知，本发明检测方法与人工评吸检测结果基本一致，本发明方法能客观、准确对接装纸是否有粘唇力进行检测，易于推广应用。
以上显示和描述了本发明的基本原理、主要特征和本发明的优点。本行业的技术人员应该了解，本发明不受上述实施例的限制，上述实施例和说明书中描述的只是说明本发明的原理，在不脱离本发明精神和范围的前提下，本发明还会有各种变化和改进，这些变化和改进都落入要求保护的本发明范围内。本发明要求保护范围由所附的权利要求书及其等效物界定。
Claims (10)
- 一种卷烟接装纸粘唇力的检测方法，其特征在于，包括如下步骤：步骤(1)，对卷烟接装纸进行剪裁；步骤(2)，将裁好的测试样品进行称重；步骤(3)，将裁好的测试样品平整放置于铺有吸水纸的涂布平台上，印刷面朝上，准确移取一定量的人工唾液，均匀涂抹于接装纸印刷面，刮涂结束时开始计时，静置一段时间；步骤(4)，达到静置的规定时间时，在测试样品表面放置一张吸水纸，然后立即用一定重量砝码压在吸水纸上并计时，静置一段时间；步骤(5)，达到规定时间时，将经人工唾液渗透过的测试样品进行称重；步骤(6)，人工唾液在卷烟接装纸表面渗透后，卷烟接装纸的质量增长百分比按照公式(1)计算；
式(1)中：ω——质量增长百分比；M 测——人工唾液在卷烟接装纸表面渗透后测试样品的质量，单位为克；M 空——人工唾液在卷烟接装纸表面渗透前测试样品的质量，单位为克；步骤(7)，根据人工唾液渗透率进行粘唇力等级的测定。 - 根据权利要求1所述的卷烟接装纸粘唇力的检测方法，其特征在于，步骤(1)中，将样品放在剪切板上进行剪裁，裁切成长度为50～300mm和宽度为10～50mm的长方形宽条，尺寸偏差应在±0.05mm之内，剪裁完成后的测试样品应没有覆盖卷烟接装纸的打孔部位。
- 根据权利要求1所述的卷烟接装纸粘唇力的检测方法，其特征在于，步骤(2)和步骤(5)中，称重采用分析天平，分析天平的感量不低于0.1mg。
- 根据权利要求1所述的卷烟接装纸粘唇力的检测方法，其特征在于，步骤(3)和步骤(4)中，计时采用秒表计时。
- 根据权利要求1所述的卷烟接装纸粘唇力的检测方法，其特征在于，步骤(3)中，涂布平台为压印床，压印床的面积尺寸要大于裁剪样品的尺寸，且水平放置，表面平整。
- 根据权利要求1所述的卷烟接装纸粘唇力的检测方法，其特征在于，步骤(3)中，吸水纸满足《GB/T1540纸和纸板吸水性的测定法可勃法》中吸水纸的要求；人工唾液按照《GBT18886-2002纺织品色牢度试验耐唾液色牢度》中人工唾液配方和工艺制备。
- 根据权利要求1所述的卷烟接装纸粘唇力的检测方法，其特征在于，步骤(3)中，人工唾液的吸取量范围为10～1000μL。
- 根据权利要求1所述的卷烟接装纸粘唇力的检测方法，其特征在于，步骤(3)中，静置时间为5～30s；步骤(4)中，静置时间为5～30s。
- 根据权利要求1所述的卷烟接装纸粘唇力的检测方法，其特征在于，步骤(4)中，砝码大小能完全覆盖测试样品尺寸，且质量为500～3000g。
- 根据权利要求1所述的卷烟接装纸粘唇力的检测方法，其特征在于，步骤(7)中，粘唇力等级的测定为：当质量增长百分比小于4.0％时，确定粘唇性等级结果为0级，表现为不粘唇；当质量增长百分比为4.0％～7.0％时，确定粘唇性等级结果为1级，表现为轻度粘唇；当质量增长百分比为7.0％～10.0％时，确定粘唇性等级结果为2级，表现为中度粘唇；当质量增长百分比为10.0％～13.0％时，确定粘唇性等级结果为3级，表现为重度粘唇；当质量增长百分比大于13.0％时，确定粘唇性等级结果为4级，表现为严重粘唇。
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