WO2020091607A1 - A continuous freeze dryer, hopper and method of freeze-drying - Google Patents

A continuous freeze dryer, hopper and method of freeze-drying Download PDF

Info

Publication number
WO2020091607A1
WO2020091607A1 PCT/NZ2019/050133 NZ2019050133W WO2020091607A1 WO 2020091607 A1 WO2020091607 A1 WO 2020091607A1 NZ 2019050133 W NZ2019050133 W NZ 2019050133W WO 2020091607 A1 WO2020091607 A1 WO 2020091607A1
Authority
WO
WIPO (PCT)
Prior art keywords
hopper
product
inlet
freeze
freeze dryer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/NZ2019/050133
Other languages
English (en)
French (fr)
Inventor
Alastair James Woodburn GASS
Austen Frank CHITTOCK
Brian Donald EDWARDS
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Freeze Dried Foods New Zealand Ltd
Original Assignee
Freeze Dried Foods New Zealand Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to CN201980072187.7A priority Critical patent/CN112955708A/zh
Priority to US17/289,505 priority patent/US20210386100A1/en
Priority to KR1020217016301A priority patent/KR20210084578A/ko
Priority to JP2021548499A priority patent/JP2022509481A/ja
Priority to EP19880225.8A priority patent/EP3874217A4/en
Priority to AU2019373054A priority patent/AU2019373054A1/en
Application filed by Freeze Dried Foods New Zealand Ltd filed Critical Freeze Dried Foods New Zealand Ltd
Priority to MX2021004831A priority patent/MX2021004831A/es
Priority to SG11202104361TA priority patent/SG11202104361TA/en
Priority to CA3118075A priority patent/CA3118075A1/en
Publication of WO2020091607A1 publication Critical patent/WO2020091607A1/en
Anticipated expiration legal-status Critical
Priority to ZA2021/03632A priority patent/ZA202103632B/en
Ceased legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23BPRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
    • A23B2/00Preservation of foods or foodstuffs, in general
    • A23B2/001Details of apparatus, e.g. pressure feed valves or for transport, or loading or unloading manipulation
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B5/00Drying solid materials or objects by processes not involving the application of heat
    • F26B5/04Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum
    • F26B5/06Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum the process involving freezing
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23BPRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
    • A23B2/00Preservation of foods or foodstuffs, in general
    • A23B2/90Preservation of foods or foodstuffs, in general by drying or kilning; Subsequent reconstitution
    • A23B2/92Freeze drying
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B15/00Machines or apparatus for drying objects with progressive movement; Machines or apparatus with progressive movement for drying batches of material in compact form
    • F26B15/10Machines or apparatus for drying objects with progressive movement; Machines or apparatus with progressive movement for drying batches of material in compact form with movement in a path composed of one or more straight lines, e.g. compound, the movement being in alternate horizontal and vertical directions
    • F26B15/12Machines or apparatus for drying objects with progressive movement; Machines or apparatus with progressive movement for drying batches of material in compact form with movement in a path composed of one or more straight lines, e.g. compound, the movement being in alternate horizontal and vertical directions the lines being all horizontal or slightly inclined
    • F26B15/14Machines or apparatus for drying objects with progressive movement; Machines or apparatus with progressive movement for drying batches of material in compact form with movement in a path composed of one or more straight lines, e.g. compound, the movement being in alternate horizontal and vertical directions the lines being all horizontal or slightly inclined the objects or batches of materials being carried by trays or racks or receptacles, which may be connected to endless chains or belts
    • F26B15/146Machines or apparatus for drying objects with progressive movement; Machines or apparatus with progressive movement for drying batches of material in compact form with movement in a path composed of one or more straight lines, e.g. compound, the movement being in alternate horizontal and vertical directions the lines being all horizontal or slightly inclined the objects or batches of materials being carried by trays or racks or receptacles, which may be connected to endless chains or belts applying multiple superimposed tray conveyors, the materials to be dried being dropped onto subsequent conveyor stretches, e.g. by allowing the trays to tilt at one point
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B17/00Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement
    • F26B17/02Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement with movement performed by belts carrying the materials; with movement performed by belts propelling the materials over stationary surfaces
    • F26B17/04Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement with movement performed by belts carrying the materials; with movement performed by belts propelling the materials over stationary surfaces the belts being all horizontal or slightly inclined
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B25/00Details of general application not covered by group F26B21/00 or F26B23/00
    • F26B25/001Handling, e.g. loading or unloading arrangements
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B25/00Details of general application not covered by group F26B21/00 or F26B23/00
    • F26B25/008Seals, locks, e.g. gas barriers or air curtains, for drying enclosures
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B3/00Drying solid materials or objects by processes involving the application of heat
    • F26B3/28Drying solid materials or objects by processes involving the application of heat by radiation, e.g. from the sun
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

Definitions

  • This invention relates to a continuous freeze dryer, a hopper for supplying product to the freeze dryer and a method of freeze-drying.
  • Products such as food products, may be dried using pure drying systems, which operate at atmospheric pressure and remove moisture by evaporation using heat, or freeze dryers, which operate by freezing a product, lowering the pressure in a vessel, and then removing the ice by sublimation.
  • Current freeze drying machines largely fall into the categories of small batch dryers or large and expensive "continuous" dryers.
  • Small batch dryers consist of a single vessel into which product is loaded, the dryer is closed and evacuated and temperature is cycled through the drying process. These systems have limited throughput, require a high amount of labour and have relatively high processing costs on a cost per weight of product basis.
  • a continuous freeze dryer comprising: a. freeze-drying chamber capable of at least partial evacuation having a continuous conveyor from an inlet to an outlet, wherein the inlet has an inlet valve; and b. a hopper for supplying product to the inlet of the freeze-drying chamber configured to form a sealed coupling with the inlet, wherein the hopper includes a hopper valve allowing the hopper to be sealed and evacuated with a product to be freeze-dried inside, wherein, when the hopper is coupled to the chamber, the inlet valve and hopper valve may both be opened to provide a pathway between the hopper and the chamber whilst the hopper and chamber are maintained in an evacuated condition.
  • a hopper for supplying product to a freeze dryer inlet including: a. an external shell; b. an internal shell within the external shell defining a cavity between the shells and including openings in the internal shell creating a fluid transfer path between the interior of the internal shell and the cavity; c. a product port for coupling to an inlet of a freeze dryer to provide a conduit for the supply of product to the freeze dryer; d. an evacuation port for evacuation of the cavity; and e. a hopper valve for opening and closing the product port.
  • a continuous freeze-drying method comprising the steps of: a. providing an evacuated freeze-drying chamber having an inlet and an outlet; b. loading product into a hopper; c. coupling the hopper with the inlet of the freeze-drying chamber; d. evacuating the hopper; e. opening a pathway between the hopper and the inlet to allow product to enter the evacuated freeze-drying chamber; and f. conveying the product through and freeze drying the product in the freeze-drying chamber.
  • Figure 1 is a cross-sectional side view of a freeze dryer supplied with product by a hopper
  • Figure 2 is a cross-section top view of the freeze dryer shown in figure 1;
  • Figure 3 is a cross-sectional side view of a hopper positioned above a freeze dryer inlet prior to coupling;
  • Figure 4 is a cross-sectional side view of a hopper coupled to a freeze dryer inlet
  • Figure 5 is a cross-sectional side view of a hopper coupled to a freeze dryer inlet with the freeze dryer inlet valve open;
  • Figure 6 is a cross-sectional side view of a hopper coupled to a freeze dryer inlet with the freeze dryer inlet valve and hopper cone valve open.
  • Figure 1 illustrates a freeze dryer including a chamber 1 with a hopper 2 coupled to it to supply a product 3 to the freeze dryer and a receptacle 4 for receiving processed product.
  • Product entering the freeze dryer is distributed onto a tray 5 by a rotary feeder 6 as the tray passes under it.
  • a number of trays are provided on each level depending upon the size of the chamber.
  • the trays are sequentially moved from the top to the bottom as illustrated by the arrows and at the bottom the tray 8 is tipped to release product via outlet 9 into receptacle 4 when butterfly valve 10 is open. Tray 8 is then moved to the top tray position (tray 5).
  • Radiating elements 7, in this case in the form of electrical resistances elements, are provided above each tray to heat the product on each tray.
  • Heating is controlled to decrease heating from the top tray to the bottom tray as the product heats and moisture is removed from the product.
  • a number of condensers 11 are provided in bays 12 within chamber 1.
  • the condensers trap water vapour removed from the product as ice which must be periodically removed, typically when a layer of ice about 3-5 mm thick forms on the surface of a condenser.
  • a screen 13 moves across a bay 12 during defrosting. The condenser is then heated and condensate and defrost water is then conveyed out of the chamber. After defrosting a condenser, the screen 13 may be moved to the next bay 12 to defrost the next condenser.
  • FIG 3 a side cross-sectional view of the hopper 2 and chamber inlet 14 are shown. All components have circular horizontal cross sections.
  • the hopper 2 is seen to be formed by an external shell 15 supporting a spaced apart internal shell 16 defining a cavity 17 between the walls of the shells.
  • the double wall construction provides insulation between the frozen product within the hopper and the external ambient temperature, reducing frosting and condensation, which may pose a biological hazard.
  • An opening at one end of the inner shell forms a product port 20 for supplying product to the chamber inlet 14.
  • the inner shell 16 has a number of openings 18 (enlarged for illustration) creating a fluid transfer path between the interior of the internal shell 16 and the cavity 17.
  • An annular opening 19 forms an evacuation port for evacuation of fluid from the hopper - fluid within internal shell 16 passes through openings 18 to the cavity 17 and then out through the annular opening 19 to evacuation port 24.
  • a hopper valve in the form of cone valve 21 is provided which may be closed to retain product within the hopper or opened to allow product to flow into the chamber inlet 14.
  • the chamber inlet 14 includes an inlet valve 22 that may be raised and lowered by a linear actuator, in this case a ram 23. In the closed position inlet valve 22 provides an airtight seal to chamber 1. In the open position inlet valve 22 is raised (into the hopper) a sufficient height to allow product to flow from the hopper 2 into the chamber inlet 14.
  • FIG 3 shows the chamber inlet 14 sealed by inlet valve 22 with the hopper 2 positioned above and apart from hopper 2.
  • Hopper 2 has been previously loaded with frozen product and cone valve 21 closed.
  • Hopper 2 is then lowered onto inlet 14 and coupled thereto as shown in Figure 4.
  • Hopper 2 is coupled to the inlet 14 so that annular opening 19 is aligned with evacuation port 24 and product port 20 is aligned with the product inlet 14.
  • the hopper is then evacuated via evacuation port 24 which draws fluid within internal shell 16 through openings 18 to the intermediate cavity 17 and then out through the annular opening 19 to evacuation port 24.
  • the hopper may be evacuated to a pressure close to or the same as the pressure within the chamber, preferably 2 mbar or less. This ensures that there is no significant variation of the conditions within the chamber 1 during loading which may adversely affect product processing and also minimizes the energy required and handling.
  • linear actuator 23 is extended to initially open the inlet valve 22 as shown in Figure 5.
  • the liner actuator is further extended to the position shown in Figure 6 to open the cone valve 21 too and is raised high enough allow product to be supplied to the freeze dryer via the chamber inlet 14.
  • product supplied via inlet 14 is evenly distributed by feeder 6 over the top tray.
  • the chamber is at least partially evacuated in use, preferably to 2 mbar or less.
  • Each tray is heated by radiating elements 7 positioned above the trays of each level to provide required heating.
  • the radiating elements are controlled to create a temperature gradient that decreases from the top to the bottom of the chamber 1.
  • the trays are continuously moved down from the top to the bottom.
  • the bottom tray 8 is ready to be emptied it is tilted so that product may be supplied to the chamber outlet 9. Once free of product the bottom tray 8 moves to the top to become the new top tray 5.
  • an alternative form of conveyor may be employed to convey the product from the inlet to the outlet through the chamber.
  • a receptacle 4 is coupled to outlet 9 and evacuated to a pressure of about 2 mbar.
  • Butterfly valve is then opened (the position shown in dashed line) so that product supplied from the bottom tray 8 may pass through outlet 9 into receptacle 4.
  • a trolley 25 may be provided within the receptacle to collect processed product and when the trolley 25 is full butterfly valve 10 may be closed, the receptacle 4 repressurised, a door of the receptacle 4 opened and trolley 25 removed and replaced with an empty trolley.
  • High throughput - continuous operation avoids delays in pressurising/ unloading/loading/depressurising each load.

Landscapes

  • Engineering & Computer Science (AREA)
  • General Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Molecular Biology (AREA)
  • Health & Medical Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Food Science & Technology (AREA)
  • Chemical & Material Sciences (AREA)
  • Zoology (AREA)
  • Wood Science & Technology (AREA)
  • Microbiology (AREA)
  • Drying Of Solid Materials (AREA)
PCT/NZ2019/050133 2018-10-29 2019-10-10 A continuous freeze dryer, hopper and method of freeze-drying Ceased WO2020091607A1 (en)

Priority Applications (10)

Application Number Priority Date Filing Date Title
MX2021004831A MX2021004831A (es) 2018-10-29 2019-10-10 Liofilizador continuo, tolva y metodo de liofilizacion.
US17/289,505 US20210386100A1 (en) 2018-10-29 2019-10-10 A continuous freeze dryer, hopper and method of freeze-drying
KR1020217016301A KR20210084578A (ko) 2018-10-29 2019-10-10 연속 동결 건조기, 호퍼 및 동결 건조 방법
JP2021548499A JP2022509481A (ja) 2018-10-29 2019-10-10 連続式冷凍乾燥器、ホッパ、及び冷凍乾燥方法
EP19880225.8A EP3874217A4 (en) 2018-10-29 2019-10-10 A continuous freeze dryer, hopper and method of freeze-drying
CN201980072187.7A CN112955708A (zh) 2018-10-29 2019-10-10 连续冷冻干燥机、料斗和冷冻干燥的方法
CA3118075A CA3118075A1 (en) 2018-10-29 2019-10-10 A continuous freeze dryer, hopper and method of freeze-drying
AU2019373054A AU2019373054A1 (en) 2018-10-29 2019-10-10 A continuous freeze dryer, hopper and method of freeze-drying
SG11202104361TA SG11202104361TA (en) 2018-10-29 2019-10-10 A continuous freeze dryer, hopper and method of freeze-drying
ZA2021/03632A ZA202103632B (en) 2018-10-29 2021-05-27 A continuous freeze dryer, hopper and method of freeze-drying

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
NZ747776 2018-10-29
NZ74777618 2018-10-29

Publications (1)

Publication Number Publication Date
WO2020091607A1 true WO2020091607A1 (en) 2020-05-07

Family

ID=70462472

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/NZ2019/050133 Ceased WO2020091607A1 (en) 2018-10-29 2019-10-10 A continuous freeze dryer, hopper and method of freeze-drying

Country Status (11)

Country Link
US (1) US20210386100A1 (https=)
EP (1) EP3874217A4 (https=)
JP (1) JP2022509481A (https=)
KR (1) KR20210084578A (https=)
CN (1) CN112955708A (https=)
AU (1) AU2019373054A1 (https=)
CA (1) CA3118075A1 (https=)
MX (1) MX2021004831A (https=)
SG (1) SG11202104361TA (https=)
WO (1) WO2020091607A1 (https=)
ZA (1) ZA202103632B (https=)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112849767A (zh) * 2021-02-03 2021-05-28 北京农科亿健蜂产品研究院 保质蜂皇浆冻干粉存放装置

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11287185B1 (en) * 2020-09-09 2022-03-29 Stay Fresh Technology, LLC Freeze drying with constant-pressure and constant-temperature phases
CN113790579B (zh) * 2021-09-30 2025-01-24 宁夏神耀科技有限责任公司 一种真空干化脱水装置及气化炉系统
CN114087864A (zh) * 2021-11-25 2022-02-25 安徽省邹师傅中药机械制造有限公司 一种中药材加工用药材循环节能烘干机及其使用方法
CN115615146B (zh) * 2022-11-10 2024-08-16 浙江同景冻干科技有限公司 一种连续加工的冻干设备

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US20170267466A1 (en) * 2011-08-12 2017-09-21 Cyclone Catalyst Properties, Llc Systems and methods for converter bed unloading and loading
CN207827042U (zh) * 2017-12-30 2018-09-07 郑州盛彤冶材有限公司 一种带粉尘回收装置的接料仓

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Publication number Priority date Publication date Assignee Title
CN112849767A (zh) * 2021-02-03 2021-05-28 北京农科亿健蜂产品研究院 保质蜂皇浆冻干粉存放装置

Also Published As

Publication number Publication date
EP3874217A4 (en) 2022-06-01
MX2021004831A (es) 2021-10-13
CA3118075A1 (en) 2020-05-07
AU2019373054A1 (en) 2021-06-10
KR20210084578A (ko) 2021-07-07
CN112955708A (zh) 2021-06-11
JP2022509481A (ja) 2022-01-20
ZA202103632B (en) 2022-10-26
US20210386100A1 (en) 2021-12-16
EP3874217A1 (en) 2021-09-08
SG11202104361TA (en) 2021-05-28

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