WO2019013668A8 - Способ разделения эмульсий - Google Patents

Способ разделения эмульсий Download PDF

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Publication number
WO2019013668A8
WO2019013668A8 PCT/RU2017/000753 RU2017000753W WO2019013668A8 WO 2019013668 A8 WO2019013668 A8 WO 2019013668A8 RU 2017000753 W RU2017000753 W RU 2017000753W WO 2019013668 A8 WO2019013668 A8 WO 2019013668A8
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WO
WIPO (PCT)
Prior art keywords
load
granules
layer
height
emulsion separation
Prior art date
Application number
PCT/RU2017/000753
Other languages
English (en)
French (fr)
Other versions
WO2019013668A1 (ru
Inventor
Петр Васильевич БЕЛОВ
Александр Дмитриевич ИШКОВ
Александр Викторович КОСЯКОВ
Сергей Владимирович КУЛИГИН
Михаил Владимирович ДЕМИН
Максим Петрович КИРИН
Андрей Владимирович БЛАГОВ
Евгений Павлович САЛЬНИКОВ
Вадим Витальевич РОВОВОЙ
Original Assignee
Общество с ограниченной ответственностью "Воронежпеностекло"
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Общество с ограниченной ответственностью "Воронежпеностекло" filed Critical Общество с ограниченной ответственностью "Воронежпеностекло"
Priority to EA201992671A priority Critical patent/EA037964B1/ru
Priority to KR1020207001153A priority patent/KR20200016971A/ko
Priority to EP17917858.7A priority patent/EP3513853B1/en
Priority to JP2019572774A priority patent/JP6975806B2/ja
Publication of WO2019013668A1 publication Critical patent/WO2019013668A1/ru
Publication of WO2019013668A8 publication Critical patent/WO2019013668A8/ru

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02—Separation of non-miscible liquids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02—Separation of non-miscible liquids
    • B01D17/0202—Separation of non-miscible liquids by ab- or adsorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02—Separation of non-miscible liquids
    • B01D17/04—Breaking emulsions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/08—Thickening liquid suspensions by filtration
    • B01D17/10—Thickening liquid suspensions by filtration with stationary filtering elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D27/00—Cartridge filters of the throw-away type
    • B01D27/02—Cartridge filters of the throw-away type with cartridges made from a mass of loose granular or fibrous material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/14—Diatomaceous earth
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/34—Regenerating or reactivating
    • B01J20/3433—Regenerating or reactivating of sorbents or filter aids other than those covered by B01J20/3408 - B01J20/3425
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/34—Regenerating or reactivating
    • B01J20/345—Regenerating or reactivating using a particular desorbing compound or mixture
    • B01J20/3475—Regenerating or reactivating using a particular desorbing compound or mixture in the liquid phase
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/28—Treatment of water, waste water, or sewage by sorption
    • C02F1/288—Treatment of water, waste water, or sewage by sorption using composite sorbents, e.g. coated, impregnated, multi-layered
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/40—Devices for separating or removing fatty or oily substances or similar floating material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/50—Aspects relating to the use of sorbent or filter aid materials
    • B01J2220/56—Use in the form of a bed
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/28—Treatment of water, waste water, or sewage by sorption
    • C02F1/286—Treatment of water, waste water, or sewage by sorption using natural organic sorbents or derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/34—Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32
    • C02F2103/36—Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32 from the manufacture of organic compounds
    • C02F2103/365—Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32 from the manufacture of organic compounds from petrochemical industry (e.g. refineries)

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Hydrology & Water Resources (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Inorganic Chemistry (AREA)
  • Filtration Of Liquid (AREA)
  • Filtering Materials (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Water Treatment By Sorption (AREA)

Abstract

Изобретение относится к области разделения эмульсий фильтрацией. Способ разделения эмульсий включает фильтрование эмульсии через слой гранулированной загрузки и регенерацию загрузки. Часть поверхности гранул загрузки выполнена несмачиваемой для дисперсной фазы за счет ее покрытия дисперсионной средой, при этом загрузку перед фильтрованием пропитывают дисперсионной средой. Регенерацию загрузки производят с помощью обратной промывки. В качестве гранул загрузки используют открытопористые гранулы, открытые поры которых обладают капиллярным эффектом по отношению к дисперсионной среде. По крайней мере внешний слой гранул загрузки содержит частицы абразивного материала и выполнен из материала на основе диатомита. Гранулы имеют округлую форму. Высота слоя загрузки находится в интервале от 0,3 до 5,0 м. Отношение высоты слоя загрузки к максимальному размеру его проходного сечения составляет не менее 0,2. Высота слоя загрузки составляет не менее 50 эквивалентных диаметров гранул. Технический результат: повышение эффективности процесса разделения эмульсий.
PCT/RU2017/000753 2017-07-11 2017-10-11 Способ разделения эмульсий WO2019013668A1 (ru)

Priority Applications (4)

Application Number Priority Date Filing Date Title
EA201992671A EA037964B1 (ru) 2017-07-11 2017-10-11 Способ разделения эмульсий
KR1020207001153A KR20200016971A (ko) 2017-07-11 2017-10-11 에멀젼 분리 방법
EP17917858.7A EP3513853B1 (en) 2017-07-11 2017-10-11 Method of emulsion separation
JP2019572774A JP6975806B2 (ja) 2017-07-11 2017-10-11 エマルションの分離方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
RU2017124417 2017-07-11
RU2017124417A RU2664936C1 (ru) 2017-07-11 2017-07-11 Способ разделения эмульсий

Publications (2)

Publication Number Publication Date
WO2019013668A1 WO2019013668A1 (ru) 2019-01-17
WO2019013668A8 true WO2019013668A8 (ru) 2019-04-11

Family

ID=63286906

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/RU2017/000753 WO2019013668A1 (ru) 2017-07-11 2017-10-11 Способ разделения эмульсий

Country Status (6)

Country Link
EP (1) EP3513853B1 (ru)
JP (1) JP6975806B2 (ru)
KR (1) KR20200016971A (ru)
EA (1) EA037964B1 (ru)
RU (1) RU2664936C1 (ru)
WO (1) WO2019013668A1 (ru)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2740064C2 (ru) * 2018-12-23 2020-12-31 Общество с ограниченной ответственностью "Воронежпеностекло" Фильтрующий слой
RU2767884C1 (ru) * 2021-03-13 2022-03-22 Общество с ограниченной ответственностью «Воронежпеностекло» Способ фильтрационного разделения водной эмульсии в слое гранул
WO2022197212A1 (ru) * 2021-03-13 2022-09-22 Общество с ограниченной ответственностью "Воронежпеностекло" Способ фильтрации воды через слой гранул
RU2767886C1 (ru) * 2021-03-13 2022-03-22 Общество с ограниченной ответственностью «Воронежпеностекло» Способ коалесценции нерастворимых в воде жидкостей

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1435936A (en) * 1972-05-26 1976-05-19 Hager & Elsaesser Method and apparatus for the purification of liquids
FR2340910A1 (fr) * 1976-02-11 1977-09-09 Inst Francais Du Petrole Procede de purification d'eaux contenant des produits organiques par extraction desdits produits organiques au moyen d'un solvant immobilise
GB1589901A (en) * 1976-11-16 1981-05-20 Teijin Ltd Emulsion breaking material
DE3372715D1 (en) * 1983-01-24 1987-09-03 Amsted Ind Inc Solvent addition to deep bed filter
SU1784256A1 (ru) * 1990-11-11 1992-12-30 Voronezh Inzh Str I Фильтр для очистки водь! 2 ·
US6764603B2 (en) * 1992-08-07 2004-07-20 Akzo Nobel Nv Material for extracting hydrophobic components dissolved in water
RU2077363C1 (ru) * 1994-09-27 1997-04-20 Татьяна Алексеевна Лакина Способ разделения эмульсий и устройство для его осуществления
BR9707371A (pt) * 1996-02-06 2000-01-04 Wolfgang Schenk Gmbh Processo e usina para tratamento de dejeto
RU2202519C1 (ru) * 2001-07-20 2003-04-20 Санкт-Петербургский государственный технологический институт (технический университет) Способ очистки жидкостей от маслонефтепродуктов
RU2182118C1 (ru) * 2001-08-09 2002-05-10 Татаренко Олег Федорович Способ очистки воды от нефтепродуктов
RU2327518C2 (ru) * 2006-08-14 2008-06-27 ЗАО "Северо-Западная Экологическая компания" Способ получения сорбента для жидких углеводородов
RU78436U1 (ru) * 2008-01-30 2008-11-27 ООО "Эко-Эксперт" Капиллярный сепаратор эмульсий
ES2746198T3 (es) * 2008-12-22 2020-03-05 Glatt Systemtechnik Gmbh Gránulo adsorbente de material compuesto, proceso para su producción y proceso de separación de gases
RU170334U1 (ru) * 2016-08-30 2017-04-21 Общество с ограниченной ответственностью "Воронежпеностекло" Гранулированный фильтрующий материал

Also Published As

Publication number Publication date
EA201992671A1 (ru) 2020-03-10
JP6975806B2 (ja) 2021-12-01
EP3513853B1 (en) 2020-12-02
RU2664936C1 (ru) 2018-08-23
KR20200016971A (ko) 2020-02-17
EP3513853A4 (en) 2019-07-24
EP3513853A1 (en) 2019-07-24
EA037964B1 (ru) 2021-06-16
JP2020527449A (ja) 2020-09-10
WO2019013668A1 (ru) 2019-01-17

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