WO2019004627A1 - Composition cosmétique de type émulsion huile dans l'eau pour les lèvres - Google Patents

Composition cosmétique de type émulsion huile dans l'eau pour les lèvres Download PDF

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Publication number
WO2019004627A1
WO2019004627A1 PCT/KR2018/006443 KR2018006443W WO2019004627A1 WO 2019004627 A1 WO2019004627 A1 WO 2019004627A1 KR 2018006443 W KR2018006443 W KR 2018006443W WO 2019004627 A1 WO2019004627 A1 WO 2019004627A1
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composition
cosmetic composition
weight
water
oil
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PCT/KR2018/006443
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English (en)
Korean (ko)
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채련
김세진
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(주)아모레퍼시픽
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Publication of WO2019004627A1 publication Critical patent/WO2019004627A1/fr

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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0216—Solid or semisolid forms
    • A61K8/0229—Sticks
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04—Dispersions; Emulsions
    • A61K8/06—Emulsions
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04—Dispersions; Emulsions
    • A61K8/06—Emulsions
    • A61K8/062—Oil-in-water emulsions
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02—Preparations containing skin colorants, e.g. pigments
    • A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
    • A61Q1/06—Lipsticks

Definitions

  • Lip cosmetic compositions of high emulsion type emulsion stick formulations are disclosed herein.
  • lipsticks are colored on the surface of the lips, but are not colored.
  • surface coloring and coloring are possible, but there is a limitation that they can be used only in a liquid phase.
  • various emulsion lipstick formulations have been developed to impart moisturization to the lips, but they have limitations in implementing hard stick formulations that are liquid, gel, or semi-solid formulations and that supply and moisturize simultaneously.
  • a cosmetic composition for lips which can provide both surface coloring and coloring as a solid stick formulation, and supply moisture and moisturize it.
  • cosmetic compositions for underwater type lips are mostly in the form of cream, gel or semi-solid, and the water is evaporated due to the water being in contact with water, which adversely affects the stability and appearance of the solid stick over time. Accordingly, when a cosmetic composition for underwater type lip is implemented as a solid stick formulation, there is a problem that the contents are shrunk or the stick shape is deformed.
  • a related prior art document is Korean Patent Laid-Open Publication No. 10-2013-0023542.
  • the object of the present invention is to provide a lip cosmetic composition of the solid stick formulation having excellent stability over time without shrinkage or collapse of contents as an underwater type.
  • the present invention aims to provide a cosmetic composition for lips of an underwater type emulsion stick formulation capable of providing a moisturizing and moisturizing film and capable of coloring and coloring.
  • the presently disclosed technology is a lip cosmetic composition, wherein the composition is a high in-water type water (O / W) emulsion comprising at least 75% by weight of an oily portion based on the total weight of the cosmetic composition, Wherein the composition is formulated as an oil-in-water emulsion stick formulation.
  • O / W high in-water type water
  • the oily portion may comprise 10 to 35 wt% of waxes based on the total weight of the cosmetic composition.
  • the wax may be at least one selected from the group consisting of hydrocarbon-based solid oils, ester-based solid oils, higher alcohol-based solid oils, and silicone-based solid oils.
  • the stick may be surface coated with a film former.
  • the film former may be a surface coating of the stick at 0.01 to 5% by weight based on the total weight of the cosmetic composition.
  • the film former is selected from the group consisting of an acrylate copolymer, a PVA / eicosin copolymer, an acrylate / stearyl acrylate / dimethicone methacrylate copolymer, trimethylsiloxysilicate, Methylsiloxysilicate / dimethicone crosspolymer, and dimethicone / vinyltrimethylsiloxysilicate crosspolymer.
  • the polymeric siloxysilicate / dimethicone / dimethicone / vinyltrimethylsiloxysilicate crosspolymer may be at least one selected from the group consisting of methylsiloxysilicate, trimethylsiloxysilicate / dimethicone crosspolymer and dimethicone /
  • the composition may have a hardness of 60 to 150 g as measured with a hardener (Model: CR-500DX).
  • the composition may comprise a water-soluble tar pigment on top of the water.
  • the composition comprises from 0.1 to 1.5% by weight, based on the total weight of the cosmetic composition, of a water-soluble pigment and from 2.0 to 10.0% by weight, based on the total weight of the cosmetic composition, .
  • the composition may be such that the pigment contained in the upper part of the liquid upon application to the lips is colored on the lips.
  • the art disclosed herein relates to a cosmetic composition
  • a cosmetic composition comprising: a core portion comprising a lip cosmetic composition; And a film forming agent, wherein the composition is a high in-water type water (O / W) emulsion comprising at least 75% by weight based on the total weight of the cosmetic composition.
  • O / W high in-water type water
  • the oily portion may comprise 10 to 35 wt% of waxes based on the total weight of the cosmetic composition.
  • the techniques disclosed herein have the effect of providing a lip cosmetic composition of high in-water type emulsion stick formulations.
  • the composition is effective to achieve an underwater type emulsion solid stick formulation without disturbing or deforming the stick shape by maintaining the stable hardness of the stick formulation.
  • the composition has the effect of securing appearance and stability over time by preventing the contents from being shrunk by evaporation of moisture of the trauma from the O / W formulation through outer wall coating of lipstick.
  • the composition has a moist feel and a finished feeling of oil at the same time, so that the composition has excellent spreadability and forms a moisturizing film, thereby providing an excellent feeling of use compared to conventional oil-dispersed lipstick formulations.
  • the composition of the present invention can provide dual colors of trauma and intraluminal color due to the dual coloration of the color of the trauma and the pigmentation of the internal phase.
  • the composition is capable of both coloring and coloring, .
  • FIG. 1 is a photograph showing the stability of the water-in-oil type emulsion stick formulation composition with time in the experimental example of the present invention.
  • FIG. 2 is a photograph comparing the results of forming an underwater type emulsion stick formulation according to the wax content in one experimental example of the present specification.
  • FIG. 2 is a photograph comparing the results of forming an underwater type emulsion stick formulation according to the wax content in one experimental example of the present specification.
  • FIG. 3 is a photograph comparing the color sustainability of the stick-forming composition in one experimental example of the present invention.
  • the presently disclosed technology is a lip cosmetic composition, wherein the composition is a high in-water type water (O / W) emulsion comprising at least 75% by weight of an oily portion based on the total weight of the cosmetic composition, Wherein the composition is formulated as an oil-in-water emulsion stick formulation.
  • O / W high in-water type water
  • the art disclosed herein relates to a cosmetic composition
  • a cosmetic composition comprising: a core portion comprising a lip cosmetic composition; And a film forming agent, wherein the composition is a high in-water type water (O / W) emulsion comprising at least 75% by weight based on the total weight of the cosmetic composition.
  • O / W high in-water type water
  • high internal phase means an emulsion in which the ratio of the internal phase in the water-in-water type emulsion whose water phase is water is higher than the ratio of the external phase, unlike the form of the emulsion in which the traumatic phase generally occupies a large proportion.
  • an oil-in-water type emulsion comprising 75% by weight or more of an inner phase portion, i.e., an oil phase portion, based on the total weight of the cosmetic composition.
  • the composition may comprise at least 75 wt%, or at least 80 wt%, or 75 to 85 wt%, or 80 to 85 wt% oily parts based on the total weight of the cosmetic composition.
  • the composition may comprise from 15 to 25% by weight of the water phase, based on the total weight of the cosmetic composition. In another aspect, the composition may comprise at least 15 weight percent, at least 18 weight percent, at least 20 weight percent, at least 25 weight percent, at most 23 weight percent, or at most 20 weight percent of the water- have.
  • composition according to the present invention can be a solid anti-emulsion containing 10 wt% or more of wax to realize a solid solid stick formulation of an underwater type emulsion, wherein the underwater type emulsion solid stick formulation has no breakdown phenomenon, There is an excellent effect of stability.
  • the oily portion may comprise 10 to 35 wt% of waxes based on the total weight of the cosmetic composition.
  • the oily phase is present in the cosmetic composition in an amount of at least 10 wt%, at least 15 wt%, at least 20 wt%, at least 25 wt%, or at least 30 wt%, but no more than 35 wt%, no more than 30 wt% By weight or less, 20% by weight or less, or 15% by weight or less.
  • the wax may be at least one selected from the group consisting of hydrocarbon-based solid oils, ester-based solid oils, higher alcohol-based solid oils, and silicone-based solid oils.
  • the hydrocarbon-based solid oil may be one or more selected from the group consisting of paraffin wax, ceresin wax, microcrystalline wax, polyethylene wax, ethylene propylene copolymer, and montan wax.
  • ester-based solid oil may be one or more selected from the group consisting of beeswax, carnauba wax, and candelilla wax.
  • the higher alcoholic base oil may be one or more selected from the group consisting of stearyl alcohol, cetyl alcohol, lauryl alcohol, and behenyl alcohol.
  • the waxes may be hydrocarbon-based semi-solid oil, ester-based semi-solid oil, ether-based semi-solid oil, silicone-based semi-solid oil, or the like.
  • the oily portion may comprise an oil and a surfactant.
  • the oil is selected from the group consisting of hexyl laurate, Dicaprylyl carbonate, Diisostearyl malate, butylene glycol dicaprylate / dicaprate ( Butylene glycol dicaprylate / dicaprate, cetyl ethylhexanoate, triethylhexanoin, dicetearyl dimer dilinoleate, caprylic / capric triglyceride, An ester-based oil selected from the group consisting of Capric Triglyceride, Polyglyceryl-2 Triisostearate and Pentaerythrityl Tetraisostearate; Hydrocarbon oils selected from the group consisting of polybutene, hydrogenated polyisobutene and phytosqualane; And at least one silicone oil selected from the group consisting of phenyl trimethicone and dimethicone.
  • the surfactant is selected from the group consisting of dextrin palmitate, sorbitan stearate, glyceryl monostearate / fat-100 stearate, phage-10 dimethicone and polysorbate Or more.
  • the stick may be surface coated with a film former.
  • the film former may be a surface coating of the stick at 0.01 to 5% by weight based on the total weight of the cosmetic composition. In another aspect, the film former is present in an amount of at least 0.01%, at least 0.1%, at least 0.5%, at least 1%, at least 1.5%, at least 2%, at least 2.5%
  • the surface of the stick may be coated with 3 wt% or more, 5 wt% or less, 4.5 wt% or less, 4 wt% or less, 3.5 wt% or less, 3 wt% or less, 2.5 wt% or less or 2 wt% or less. Accordingly, the external wall coating of the lipstick prevents the phenomenon that the contents of the O / W formulation are evaporated due to the evaporation of the moisture of the external surface, thereby securing appearance and stability over time.
  • the film former is selected from the group consisting of an acrylate copolymer, a PVA / eicosin copolymer, an acrylate / stearyl acrylate / dimethicone methacrylate copolymer, trimethylsiloxysilicate, Methylsiloxysilicate / dimethicone crosspolymer, and dimethicone / vinyltrimethylsiloxysilicate crosspolymer.
  • the polymeric siloxysilicate / dimethicone / dimethicone / vinyltrimethylsiloxysilicate crosspolymer may be at least one selected from the group consisting of methylsiloxysilicate, trimethylsiloxysilicate / dimethicone crosspolymer and dimethicone /
  • the composition may have a hardness of 60 to 150 g as measured with a hardener (Model: CR-500DX).
  • the lipstick may have a hardness of 60 to 150 g as measured with a hardness tester (Model: CR-500DX).
  • the composition may comprise pigments in the aqueous and / or oily phase.
  • the dye is a pigment commonly used in cosmetics, such as muscovite, synthetic mica, sericite, kaolin, titanium dioxide, titanium oxide coated mica, aluminum powder, iron oxide, Inorganic powders such as barium sulfate, silica and zeolite, and organic powders such as nylon, PMMA, polystyrene powder, polyethylene powder and cellulose powder, but are not limited thereto.
  • Barium or aluminum lake organic pigments such as red No. 227, blue No. 1, and blue No. 2, and pearl pigments, but are not limited thereto.
  • the composition comprises from 0.1 to 1.5% by weight, based on the total weight of the cosmetic composition, of a water-soluble pigment and from 2.0 to 10.0% by weight, based on the total weight of the cosmetic composition, .
  • the composition may comprise a water-soluble tar pigment on top of the water.
  • the oil-dispersed lipstick can contain only oil-dispersed pigments having no coloring effect.
  • the lipid-based cosmetic composition of the stick formulation according to the present invention may contain a water-soluble pigment having a coloring effect, have.
  • the composition may comprise an organic synthetic dye and / or an inorganic pigment in the oil phase.
  • the composition according to the present invention has an O / W formulation in which water is located in the periphery, thereby providing moisturizing ability and excellent moisturizing ability compared to conventional oil-dispersed lipstick formulations, enabling simultaneous implementation of various pigments having different solubilities, Not only is it possible, but the color persistence is also excellent.
  • the coloring effect refers to the effect of the lips on the color of the coloring matter, and the coloring effect means the coloring effect of the coloring on the coloring.
  • the composition may contain, in addition to the components described above, components used in cosmetics for ordinary lips, for example, emulsions, powders, polymer compounds, moisturizing agents, fragrances, antioxidants, preservatives, Can be appropriately compounded in such a range as not to impair the effect of the present invention.
  • components used in cosmetics for ordinary lips for example, emulsions, powders, polymer compounds, moisturizing agents, fragrances, antioxidants, preservatives, Can be appropriately compounded in such a range as not to impair the effect of the present invention.
  • the lipstick according to the present invention can be produced by preparing and warming an aqueous base and an oil base, mixing and emulsifying them to prepare a stick formulation, and then coating the film former through a spray process or a dipping process.
  • the water-in-oil emulsion stick (Comparative Example 2) containing the film forming agent in the content (Comparative Example 1) and the film forming agent in the contents (traumatic) .
  • a water-in-oil type emulsion stick (Example 1) coated with a film former on the outer surface of the stick was prepared according to the composition (% by weight) shown in Table 2 below.
  • the composition according to the present invention can prevent the contraction of the contents due to evaporation of moisture of the trauma from the O / W formulation through the outer wall coating of the lipstick, thereby securing appearance and stability over time.
  • Comparative Example 1 Comparative Example 2
  • Example 1 1 day (g) 3.81 3.74 3.98 3.52 3.98 3.91 3.88 3.98 3.57 7 days (g) -0.25 -0.21 -0.20 -0.18 -0.13 -0.15 -0.03 -0.08 -0.07 14 days (g) -0.16 -0.13 -0.13 -0.06 -0.09 -0.12 -0.04 -0.03 -0.02 Total moisture loss (g) -0.41 -0.34 -0.33 -0.24 -0.22 -0.27 -0.07 -0.11 -0.09
  • An underwater type emulsion stick was prepared in the same manner as in Example 1 except that the external coating was not performed by the coating agent component, and the hardness was determined according to the composition of the following Table 4 by changing the wax content. The hardness was measured by a physical property meter (Rheometer, CR-500DX) after storing the sample in a thermostatic chamber at 30 DEG C for 12 hours
  • the stick formulation of Comparative Example 4 which had a wax content of 5 to 7 wt% and Comparative Example 3, and a wax content of 7 to 12 wt%, had a low hardness
  • the stick formulation of Example 3 which had wax content of more than 12 to 17 wt%, and wax content of more than 17 to 20 wt%, showed stable hardness corresponding to a general stick formulation.
  • the hardness was 300 g or more, and the hardness was 60 to 150 g, which is the hardness of general lipstick formulations.
  • the pigment was not well distributed on the skin.
  • Comparative Example 6 in which the oil phase portion was less than 75% by weight, the content was crumbly crumbled and it was impossible to implement an underwater type emulsion stick formulation.
  • Comparative Example 7 in which the oil phase portion was more than 85% by weight, , Moisturizing ability and coloring power by water were lowered.
  • the high in-water type cosmetic composition according to the present invention maintains stable hardness as a stick formulation and can realize an underwater type emulsion solid stick formulation without collapsing or deforming the solid stick form.
  • Lipsticks of conventional oil dispersion form were prepared according to the composition (weight%) shown in Table 6 below to compare lipsticks and feelings of the liposome O / W formulation of Example 1.
  • the lipstick of the high inland type O / W formulation of Example 1 exhibited a cooling feeling and refreshing ability at the early stage of running, unlike the oil dispersed formulation, and the moisturizing film of oil was formed and the moisturizing effect was also excellent.
  • the lipstick of the high - internal O / W formulation showed a coloring effect similar to that of the tinted, unlike the oil - dispersed formulation, containing a water - soluble pigment in the upper part of the water.
  • Example 1 and Comparative Example 8 were applied to the lips and skin, and wiped with a tissue to observe the color persistence. It was confirmed that the lipstick of the high internal-phase O / W formulation of Example 1 was superior in color persistence to oil-dispersed formulations.

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Abstract

La présente invention concerne une composition cosmétique pour lèvres sous la forme d'un bâton de type émulsion huile dans l'eau à phase interne élevée. La composition cosmétique pour lèvres est une émulsion huile dans l'eau sous la forme d'un bâton solide, qui manifeste une excellente stabilité dans le temps sans aucun phénomène de retrait ou de délitage des ingrédients, et a pour effet d'être capable à la fois de coloration et développement de couleur et d'applicabilité humide et formation d'un film hydratant.
PCT/KR2018/006443 2017-06-30 2018-06-07 Composition cosmétique de type émulsion huile dans l'eau pour les lèvres WO2019004627A1 (fr)

Applications Claiming Priority (2)

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KR10-2017-0083786 2017-06-30
KR1020170083786A KR102371421B1 (ko) 2017-06-30 2017-06-30 수중유형 에멀젼 입술용 화장료 조성물

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US20200375875A1 (en) * 2019-05-29 2020-12-03 L'oréal Transfer-resistant topcoat composition
US20200375855A1 (en) * 2019-05-29 2020-12-03 L'oréal One-step liquid lip composition
KR20210028962A (ko) 2019-09-05 2021-03-15 (주)아모레퍼시픽 수중유형 입술용 화장료 조성물
KR20210132956A (ko) 2020-04-28 2021-11-05 (주)아모레퍼시픽 유중수형 입술용 화장료 조성물
KR102655365B1 (ko) * 2021-07-16 2024-04-09 코스맥스 주식회사 외곽 에멀전층을 포함하는 수중유형 화장료 조성물
KR20230086199A (ko) 2021-12-08 2023-06-15 숙명여자대학교산학협력단 피부 항산화 및 미백에 효능이 있는 신규한 페디오코쿠스 펜토사세우스(Pediococcus Pentosaceus) SMFM2016-NK2 균주 및 이의 유청 발효물
KR20230086200A (ko) 2021-12-08 2023-06-15 숙명여자대학교산학협력단 피부 항산화 및 미백에 효능이 있는 신규한 페디오코쿠스 펜토사세우스(Pediococcus Pentosaceus) SMFM2016-NK1 균주 및 이의 유청 발효물
KR20230123753A (ko) * 2022-02-17 2023-08-24 주식회사 엘지생활건강 묻어남을 개선한 수중유형 입술용 화장료

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