WO2017055192A3 - Verfahren zur selektiven entfernung von schwefelwasserstoff - Google Patents

Verfahren zur selektiven entfernung von schwefelwasserstoff Download PDF

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Publication number
WO2017055192A3
WO2017055192A3 PCT/EP2016/072785 EP2016072785W WO2017055192A3 WO 2017055192 A3 WO2017055192 A3 WO 2017055192A3 EP 2016072785 W EP2016072785 W EP 2016072785W WO 2017055192 A3 WO2017055192 A3 WO 2017055192A3
Authority
WO
WIPO (PCT)
Prior art keywords
hydrogen sulfide
absorbent
selective removal
fluid stream
carbon dioxide
Prior art date
Application number
PCT/EP2016/072785
Other languages
English (en)
French (fr)
Other versions
WO2017055192A2 (de
Inventor
Thomas Ingram
Georg Sieder
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to CN201680056411.XA priority Critical patent/CN108136317A/zh
Priority to BR112018003582A priority patent/BR112018003582A2/pt
Priority to EP16777611.1A priority patent/EP3356015A2/de
Priority to SG11201801409PA priority patent/SG11201801409PA/en
Application filed by Basf Se filed Critical Basf Se
Priority to MX2018004012A priority patent/MX2018004012A/es
Priority to US15/764,142 priority patent/US20180304191A1/en
Priority to AU2016330648A priority patent/AU2016330648A1/en
Priority to KR1020187008420A priority patent/KR20180058723A/ko
Priority to JP2018516575A priority patent/JP2018531147A/ja
Priority to CA3000286A priority patent/CA3000286A1/en
Publication of WO2017055192A2 publication Critical patent/WO2017055192A2/de
Publication of WO2017055192A3 publication Critical patent/WO2017055192A3/de
Priority to IL258344A priority patent/IL258344A/en
Priority to CONC2018/0003674A priority patent/CO2018003674A2/es
Priority to ZA2018/02685A priority patent/ZA201802685B/en

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/1493—Selection of liquid materials for use as absorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/1425—Regeneration of liquid absorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/1456—Removing acid components
    • B01D53/1468—Removing hydrogen sulfide
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L3/00—Gaseous fuels; Natural gas; Synthetic natural gas obtained by processes not covered by subclass C10G, C10K; Liquefied petroleum gas
    • C10L3/06—Natural gas; Synthetic natural gas obtained by processes not covered by C10G, C10K3/02 or C10K3/04
    • C10L3/10—Working-up natural gas or synthetic natural gas
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L3/00—Gaseous fuels; Natural gas; Synthetic natural gas obtained by processes not covered by subclass C10G, C10K; Liquefied petroleum gas
    • C10L3/06—Natural gas; Synthetic natural gas obtained by processes not covered by C10G, C10K3/02 or C10K3/04
    • C10L3/10—Working-up natural gas or synthetic natural gas
    • C10L3/101—Removal of contaminants
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L3/00—Gaseous fuels; Natural gas; Synthetic natural gas obtained by processes not covered by subclass C10G, C10K; Liquefied petroleum gas
    • C10L3/06—Natural gas; Synthetic natural gas obtained by processes not covered by C10G, C10K3/02 or C10K3/04
    • C10L3/10—Working-up natural gas or synthetic natural gas
    • C10L3/101—Removal of contaminants
    • C10L3/102—Removal of contaminants of acid contaminants
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L3/00—Gaseous fuels; Natural gas; Synthetic natural gas obtained by processes not covered by subclass C10G, C10K; Liquefied petroleum gas
    • C10L3/06—Natural gas; Synthetic natural gas obtained by processes not covered by C10G, C10K3/02 or C10K3/04
    • C10L3/10—Working-up natural gas or synthetic natural gas
    • C10L3/101—Removal of contaminants
    • C10L3/102—Removal of contaminants of acid contaminants
    • C10L3/103—Sulfur containing contaminants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2252/00—Absorbents, i.e. solvents and liquid materials for gas absorption
    • B01D2252/20—Organic absorbents
    • B01D2252/202—Alcohols or their derivatives
    • B01D2252/2023—Glycols, diols or their derivatives
    • B01D2252/2026—Polyethylene glycol, ethers or esters thereof, e.g. Selexol
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2252/00—Absorbents, i.e. solvents and liquid materials for gas absorption
    • B01D2252/20—Organic absorbents
    • B01D2252/204—Amines
    • B01D2252/2041—Diamines
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2252/00—Absorbents, i.e. solvents and liquid materials for gas absorption
    • B01D2252/20—Organic absorbents
    • B01D2252/204—Amines
    • B01D2252/20415—Tri- or polyamines
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2252/00—Absorbents, i.e. solvents and liquid materials for gas absorption
    • B01D2252/20—Organic absorbents
    • B01D2252/204—Amines
    • B01D2252/20431—Tertiary amines
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2252/00—Absorbents, i.e. solvents and liquid materials for gas absorption
    • B01D2252/20—Organic absorbents
    • B01D2252/204—Amines
    • B01D2252/20478—Alkanolamines
    • B01D2252/20489—Alkanolamines with two or more hydroxyl groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2252/00—Absorbents, i.e. solvents and liquid materials for gas absorption
    • B01D2252/20—Organic absorbents
    • B01D2252/205—Other organic compounds not covered by B01D2252/00 - B01D2252/20494
    • B01D2252/2056—Sulfur compounds, e.g. Sulfolane, thiols
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2252/00—Absorbents, i.e. solvents and liquid materials for gas absorption
    • B01D2252/40—Absorbents explicitly excluding the presence of water
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L2290/00—Fuel preparation or upgrading, processes or apparatus therefore, comprising specific process steps or apparatus units
    • C10L2290/54—Specific separation steps for separating fractions, components or impurities during preparation or upgrading of a fuel
    • C10L2290/541—Absorption of impurities during preparation or upgrading of a fuel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02C—CAPTURE, STORAGE, SEQUESTRATION OR DISPOSAL OF GREENHOUSE GASES [GHG]
    • Y02C20/00—Capture or disposal of greenhouse gases
    • Y02C20/40—Capture or disposal of greenhouse gases of CO2

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Gas Separation By Absorption (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Ein Absorptionsmittel zur selektiven Entfernung von Schwefelwasserstoff aus einem Kohlendioxid und Schwefelwasserstoff enthaltenden Fluidstrom enthält a) eine Aminverbindung der Formel (I) worin X, R1 bis R7, x, y und z wie in der Beschreibung definiert sind; und b) ein nicht- wässriges Lösungsmittel; wobei das Absorptionsmittel weniger als 20 Gew.-% Wasser enthält. Außerdem beschrieben ist ein Verfahren zur selektiven Entfernung von Schwefelwasserstoff aus einem Kohlendioxid und Schwefelwasserstoff enthaltenden Fluidstrom, wobei man den Fluidstrom dem Absorptionsmittel in Kontakt bringt. Das Absorptionsmittel zeichnet sich durch eine hohe Beladbarkeit, hohe zyklische Kapazität, gute Regenerierbarkeit und niedrige Viskosität aus.
PCT/EP2016/072785 2015-09-29 2016-09-26 Verfahren zur selektiven entfernung von schwefelwasserstoff WO2017055192A2 (de)

Priority Applications (13)

Application Number Priority Date Filing Date Title
US15/764,142 US20180304191A1 (en) 2015-09-29 2016-09-26 Method for the selective removal of hydrogen sulfide
EP16777611.1A EP3356015A2 (de) 2015-09-29 2016-09-26 Verfahren zur selektiven entfernung von schwefelwasserstoff
SG11201801409PA SG11201801409PA (en) 2015-09-29 2016-09-26 Method for the selective removal of hydrogen sulfide
KR1020187008420A KR20180058723A (ko) 2015-09-29 2016-09-26 황화수소의 선택적 제거 방법
MX2018004012A MX2018004012A (es) 2015-09-29 2016-09-26 Metodo para la remocion selectica de sulfuro de hidrogeno.
BR112018003582A BR112018003582A2 (pt) 2015-09-29 2016-09-26 absorvente e processo para a remoção seletiva de sulfeto de hidrogênio
AU2016330648A AU2016330648A1 (en) 2015-09-29 2016-09-26 Method for the selective removal of hydrogen sulfide
CN201680056411.XA CN108136317A (zh) 2015-09-29 2016-09-26 用于选择性移除硫化氢的方法
JP2018516575A JP2018531147A (ja) 2015-09-29 2016-09-26 硫化水素の選択的除去のための方法
CA3000286A CA3000286A1 (en) 2015-09-29 2016-09-26 Method for the selective removal of hydrogen sulfide
IL258344A IL258344A (en) 2015-09-29 2018-03-25 A method for the selective removal of hydrogen sulfide
CONC2018/0003674A CO2018003674A2 (es) 2015-09-29 2018-04-05 Método para la remoción selectiva de sulfuro de hidrógeno
ZA2018/02685A ZA201802685B (en) 2015-09-29 2018-04-23 Method for the selective removal of hydrogen sulfide

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP15187408 2015-09-29
EP15187408.8 2015-09-29

Related Child Applications (2)

Application Number Title Priority Date Filing Date
US16/638,727 A-371-Of-International US11498919B2 (en) 2017-08-23 2018-08-23 Azaindolylpyridone and diazaindolylpyridone compounds
US18/045,605 Continuation US20230322772A1 (en) 2017-08-23 2022-10-11 Azaindolylpyridone and diazaindolylpyridone compounds

Publications (2)

Publication Number Publication Date
WO2017055192A2 WO2017055192A2 (de) 2017-04-06
WO2017055192A3 true WO2017055192A3 (de) 2017-05-26

Family

ID=54251358

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2016/072785 WO2017055192A2 (de) 2015-09-29 2016-09-26 Verfahren zur selektiven entfernung von schwefelwasserstoff

Country Status (14)

Country Link
US (1) US20180304191A1 (de)
EP (1) EP3356015A2 (de)
JP (1) JP2018531147A (de)
KR (1) KR20180058723A (de)
CN (1) CN108136317A (de)
AU (1) AU2016330648A1 (de)
BR (1) BR112018003582A2 (de)
CA (1) CA3000286A1 (de)
CO (1) CO2018003674A2 (de)
IL (1) IL258344A (de)
MX (1) MX2018004012A (de)
SG (1) SG11201801409PA (de)
WO (1) WO2017055192A2 (de)
ZA (1) ZA201802685B (de)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3579946B1 (de) 2017-02-10 2021-04-07 Basf Se Verfahren zur entfernung von sauergasen aus einem fluidstrom sowie entsprechende verwendungen
US11241652B2 (en) * 2017-05-15 2022-02-08 Basf Se (Reitstötter, Kinzebach & Partner) Absorbent and process for selectively removing hydrogen sulfide
CN107051122A (zh) * 2017-06-03 2017-08-18 王丽燕 一种醇胺类复合酸性气体净化剂及其应用
CN110876878A (zh) * 2018-09-06 2020-03-13 中国石油化工股份有限公司 So2吸收剂及吸收so2的方法
CN115010631A (zh) * 2021-03-05 2022-09-06 中国石油化工股份有限公司 一种从天然气中脱除硫化氢及硫醇的化合物及其制备方法

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EP0087856A1 (de) * 1982-01-18 1983-09-07 Exxon Research And Engineering Company Verfahren zur Entfernung von H2S aus Gasmischungen unter Verwendung von Diaminoäthern
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FR2986442A1 (fr) * 2012-02-06 2013-08-09 IFP Energies Nouvelles Procede de captage du co2 par absorption avec deux sections d'absorption et utilisation de vapeur basse temperature pour la regeneration

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Publication number Priority date Publication date Assignee Title
US2161663A (en) * 1933-12-20 1939-06-06 Ig Farbenindustrie Ag Removal of hydrogen sulphide and hydrocyanic acid and of readily volatile liquids from gases
EP0087856A1 (de) * 1982-01-18 1983-09-07 Exxon Research And Engineering Company Verfahren zur Entfernung von H2S aus Gasmischungen unter Verwendung von Diaminoäthern
US4405582A (en) * 1982-01-18 1983-09-20 Exxon Research And Engineering Co. Process for selective removal of H2 S from mixtures containing H22 using diaminoether solutions
DE19548009A1 (de) * 1995-12-21 1996-06-13 Linde Ag Verfahren zur selektiven Entfernung anorganischer und/oder organischer Schwefelverbindungen
DE102005043142A1 (de) * 2004-10-22 2006-04-27 Basf Ag Verfahren zum Entsäuern eines Fluidstroms und Absorptionsmittel hierfür
FR2986442A1 (fr) * 2012-02-06 2013-08-09 IFP Energies Nouvelles Procede de captage du co2 par absorption avec deux sections d'absorption et utilisation de vapeur basse temperature pour la regeneration

Also Published As

Publication number Publication date
IL258344A (en) 2018-05-31
CA3000286A1 (en) 2017-04-06
US20180304191A1 (en) 2018-10-25
AU2016330648A1 (en) 2018-03-29
MX2018004012A (es) 2018-05-23
CO2018003674A2 (es) 2018-08-10
KR20180058723A (ko) 2018-06-01
BR112018003582A2 (pt) 2018-09-25
WO2017055192A2 (de) 2017-04-06
ZA201802685B (en) 2019-07-31
EP3356015A2 (de) 2018-08-08
JP2018531147A (ja) 2018-10-25
CN108136317A (zh) 2018-06-08
SG11201801409PA (en) 2018-04-27

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