WO2017052161A1 - Transparent formulation composition for hair - Google Patents

Transparent formulation composition for hair Download PDF

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Publication number
WO2017052161A1
WO2017052161A1 PCT/KR2016/010481 KR2016010481W WO2017052161A1 WO 2017052161 A1 WO2017052161 A1 WO 2017052161A1 KR 2016010481 W KR2016010481 W KR 2016010481W WO 2017052161 A1 WO2017052161 A1 WO 2017052161A1
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Prior art keywords
hair
composition
weight
less
surfactant
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PCT/KR2016/010481
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French (fr)
Korean (ko)
Inventor
배우리
강병하
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(주)아모레퍼시픽
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Priority to CN201680054897.3A priority Critical patent/CN108024934A/en
Publication of WO2017052161A1 publication Critical patent/WO2017052161A1/en
Priority to HK18107953.0A priority patent/HK1249012A1/en

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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/41—Amines
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/02—Preparations for cleaning the hair

Definitions

  • the present specification relates to a transparent formulation composition for hair comprising polyquaternium-73 (PQ-73).
  • Shampoo a hair cleaner, makes hair clean by removing contaminants and sebum from the hair and scalp, but the shampoo process removes the moisturizing ingredients of the sebum and hair, making the hair soft and dry, making the hair tangled and difficult to handle.
  • a hair conditioning agent in the case of a general opaque shampoo to increase the flexibility of the hair by including a hair conditioning agent, in the case of a transparent shampoo there is a constraint that the formulation becomes opaque when using a conventional hair conditioner.
  • Transparent shampoos are preferred as infant or child shampoos with a clean and mild image, and offer aesthetic benefits with a beautiful appearance, but the product performance is also unsatisfactory because the formulation is opaque due to the limited amount of conditioning ingredients to be added when using conventional hair conditioners.
  • the problem is that there is a lack of air bubbles and a lack of function as a shampoo.
  • Adult hair is damaged by contamination, frequent perm, hair dry, dyeing, and combing, so it needs a hair cleanser that has a certain level of conditioning effect. have.
  • One aspect of the present invention is to provide a composition for hair in a transparent formulation.
  • One aspect of the present invention is to provide a hair composition of a transparent formulation comprising a polyquaternium-73 (PQ-73) as a cationic polymer as a hair composition.
  • PQ-73 polyquaternium-73
  • One aspect of the present invention is to provide a composition for hair of a transparent formulation having excellent foaming force, excellent conditioning effect, excellent hair glossiness enhancing effect.
  • One aspect of the present invention is to provide a composition for hair of a transparent formulation further comprises a surfactant in the composition.
  • One aspect of the present invention is to provide a composition for hair in a transparent formulation excellent in foaming, excellent in the conditioning effect, excellent hair shine enhancement effect.
  • One aspect of the present invention provides a composition for hair in a transparent formulation comprising polyquaternium-73 (PQ-73).
  • compositions for hair in a transparent dosage form wherein the composition further comprises a surfactant.
  • the surfactant may be at least one surfactant selected from the group consisting of sodium laureth sulfate, sodium lauroyl sarcosinate, and cocamidopropyl betaine. Can be.
  • composition for hair of the transparent formulation of the polyquaternium-73 is 0.01 to 5% by weight based on the total composition.
  • Another aspect of the present invention provides a composition for hair in a transparent formulation wherein the surfactant is 1 to 30% by weight based on the total composition, preferably the surfactant is 10 to 20% by weight relative to the total composition To provide.
  • compositions for hair in a transparent formulation comprising the polyquaternium-73 and the surfactant in a weight ratio of 1:20 to 40.
  • the surfactant comprises sodium laureth sulfate, sodium lauroyl sarcosinate and cocamidopropyl betaine, for the whole composition
  • the sodium laureth sulfate is 5 to 10% by weight
  • the sodium lauroyl salcosinate is 5 to 10% by weight
  • the cocamidopropyl betaine is 0.1 to 5% by weight to provide a composition for hair in a transparent formulation.
  • the surfactant includes sodium laureth sulfate, cocamidopropyl betaine, and sodium lauroyl sarcosinate
  • the polyquaternium -73, Sodium Laureth Sulfate, Cocamidopropyl Betaine, and Sodium Lauroyl Salcosinate provide a composition for hair in a transparent formulation comprising a weight ratio of 1: 10 to 20: 10 to 20: 1 to 7.
  • the polyquaternium-73, sodium laureth sulfate, cocamidopropyl betaine and sodium lauroyl salcosinate may be included in a weight ratio of 1:12 to 16:12 to 16: 3 to 5.
  • composition for the hair composition of the transparent formulation is a cleaning composition.
  • composition according to one aspect of the present invention has the effect of providing a transparent formulation.
  • composition according to one aspect of the present invention when using the composition according to one aspect of the present invention as a transparent shampoo has the effect of providing a clean and gentle image, has the effect of providing a beautiful appearance.
  • the hair softness at the time of rinsing has an excellent effect.
  • composition according to one aspect of the present invention When the composition according to one aspect of the present invention is applied to hair, hair softness in the wet state has an excellent effect.
  • composition according to one aspect of the present invention When the composition according to one aspect of the present invention is applied to hair, hair softness after drying has an excellent effect.
  • composition according to one aspect of the present invention When the composition according to one aspect of the present invention is applied to hair, the conditioning effect is excellent.
  • composition according to one aspect of the present invention When the composition according to one aspect of the present invention is applied to hair, light has less scattering in the hair and has the effect of increasing hair clarity.
  • composition according to one aspect of the invention When applying the composition according to one aspect of the invention to the hair has the effect of increasing the gloss of the hair.
  • composition according to one aspect of the present invention When the composition according to one aspect of the present invention is applied to hair, the foaming force and the amount of foam have an excellent effect.
  • composition according to one aspect of the present invention provides a clear formulation to provide a beautiful appearance and clean and gentle image, and at the same time, when applied to the hair shows an excellent effect on the conditioning effect and hair glossiness.
  • Figure 2 is a photograph when the present invention Comparative Example and Example 4 applied to normal hair and dyed hair.
  • FIG. 3 shows comparative examples of the present specification and Examples 1 to 4 showing data evaluated by each panelist in terms of amount of foam, softness during rinsing, softness in wet state, softness after drying, and hair shine. will be.
  • One aspect of the present invention provides a composition for hair in a transparent formulation comprising polyquaternium-73 (PQ-73) as the cationic polymer.
  • PQ-73 polyquaternium-73
  • One aspect of the invention is a method for hair cleansing, the method comprising applying a composition of a clear formulation comprising polyquaternium-73 (PQ-73) as a cationic polymer to a subject in need thereof Provide a method.
  • PQ-73 polyquaternium-73
  • polyquaternium-73 (PQ-73) as a cationic polymer in preparing a composition of a clear formulation for hair cleaning.
  • the cationic polymer is a conditioning agent, and generally Called polyquaternium, it provides improved conditioning effects and at the same time enables the formulation to be transparent.
  • Poly quaternium-73 is a polymeric quaternary ammonium salt consisting of monomers of propyltrimonium chloride acrylamide, ethyltrimonium chloride methacrylate and dimethylacrylamide.
  • the composition provides a composition for hair of a transparent formulation further comprises a surfactant.
  • the surfactant may be at least one surfactant selected from the group consisting of sodium laureth sulfate, sodium lauroyl sarcosinate, and cocamidopropyl betaine. Can be.
  • the surfactant may include any one or more of sodium laureth sulfate and sodium lauroyl sarcosinate as an anionic surfactant.
  • the surfactant may include cocamidopropyl betaine as an amphoteric surfactant.
  • the polyquaternium-73 may provide a composition for hair in a transparent formulation of 0.01 to 5% by weight based on the total composition.
  • the polyquaternium-73 is 0.01% by weight, 0.05% by weight, 0.10% by weight, 0.15% by weight, 0.20% by weight, 0.25% by weight, 0.30% by weight, 0.35% by weight based on the total composition.
  • the polyquaternium-73 is less than 5% by weight, 4.5% by weight, 4.0% by weight, 3.5% by weight, 3% by weight, 2.5% by weight, 2.0% by weight, 1.5% by weight based on the total composition. % Or less, 1.0% or less, 0.9% or less, 0.8% or less, 0.7% or less, 0.6% or less, 0.59% or less, 0.58% or less, 0.57% or less, 0.56% or less, or 0.55% or less It may be up to 0.54% by weight, up to 0.53% by weight, up to 0.52% by weight, up to 0.51% by weight or up to 0.50% by weight.
  • the surfactant is 0.1 to 30% by weight based on the total composition, preferably the surfactant is 10 to 20% by weight relative to the total composition To provide.
  • the surfactant is 0.1% by weight, 0.5% by weight, 1% by weight, 1.5% by weight, 1.6% by weight, 1.7% by weight, 1.8% by weight, 1.9% by weight, At least 2 wt%, at least 2.1 wt%, at least 2.2 wt%, at least 2.3 wt%, at least 2.4 wt%, at least 2.5 wt%, at least 3 wt%, at least 4 wt%, at least 5 wt%, at least 6 wt%, At least 6.5%, at least 6.6%, at least 6.7%, at least 6.8%, at least 6.9%, at least 7%, at least 7.1%, at least 7.2%, at least 7.3%, at least 7.4%, 7.5% by weight, 8% by weight, 9% by weight, 10%
  • the surfactant is 30% by weight, 25% by weight, 20% by weight, 19% by weight, 18% by weight, 17% by weight, 16.9% by weight, 16.8% by weight, 16.7 wt% or less, 16.6 wt% or less, 16.5 wt% or less, 16.4 wt% or less, 16.3 wt% or less, 16.2 wt% or less, 16.1 wt% or less, 16 wt% or less, 13 wt% or less, 10 wt% or less, 9 wt% or less, 8 wt% or less, 7.9 wt% or less, 7.8 wt% or less, 7.7 wt% or less, 7.6 wt% or less, 7.5 wt% or less, 7.4 wt% or less, 7.3 wt% or less, 7.2 wt% or less, It can be 7.1 wt% or less, 7 wt% or less, 5 wt% or less, 3 wt% or less
  • the content of the surfactant is in the above range, it is excellent in the foaming force, excellent in the conditioning effect and softness when applied to the hair, it is excellent in the hair shiny effect.
  • Another aspect of the invention provides a composition for hair of a transparent formulation comprising the polyquaternium-73 and the surfactant in a weight ratio of 1:20 to 40.
  • the weight ratio of the polyquaternium-73 and the surfactant is 1:20 or more, 1:21 or more, 1:22 or more, 1:23 or more, 1:24 or more, 1:25 or more, 1:26 or more, 1:27 or more, 1:28 or more, 1:29 or more, 1:30 or more, 1:31 or more, 1: 31.2 or more, 1: 31.4 or more, 1: 31.6 or more, 1: 31.8 or more, 1:32 or more, 1: 32.2 or greater, 1: 32.6 or greater, or 1:33 or greater.
  • the weight ratio of the polyquaternium-73 and the surfactant is 1:40 or less, 1:39 or less, 1:38 or less, 1:37 or less, 1:36 or less, 1:35 or less, 1:34 or less, 1:33 or less, 1: 32.8 or less, 1: 32.6 or less, 1: 32.4 or less, 1: 32.2 or less, 1:32 or less, 1: 31.8 or less, 1: 31.6 or less, or 1:30 or less.
  • the weight ratio of the polyquaternium-73 and the surfactant is in the above range, it is excellent in the foaming force, excellent in the conditioning effect and softness when applied to the hair, it is excellent in the hair shiny effect.
  • the surfactant includes sodium laureth sulfate, cocamidopropyl betaine, and sodium lauroyl sarcosinate.
  • the sodium laureth sulfate is 5 to 10% by weight
  • the cocamidopropyl betaine is 5 to 10% by weight
  • the sodium lauroyl salcosinate is 0.1 to 5% by weight to provide a hair composition.
  • the surfactant includes sodium laureth sulfate, cocamidopropyl betaine, and sodium lauroyl sarcosinate
  • the polyquaternium -73, Sodium Laureth Sulfate, Cocamidopropyl Betaine, and Sodium Lauroyl Salcosinate provide a composition for hair in a transparent formulation comprising a weight ratio of 1: 10 to 20: 10 to 20: 1 to 7.
  • the polyquaternium-73, sodium laureth sulfate, cocamidopropyl betaine and sodium lauroyl salcosinate may be in a weight ratio of 1:12 to 16:12 to 16: 3 to 5.
  • the surfactant comprises sodium laureth sulfate, cocamidopropyl betaine and sodium lauroyl sarcosinate, polyquaternium-73 and
  • the weight ratio of sodium laureth sulfate and the weight ratio of polyquaternium-73 and cocamidopropyl betaine are 1:10 or more, 1:11 or more, 1:12 or more, 1:13 or more, 1: 13.2 or more, 1: 13.4 Or greater than 1: 13.6, greater than or equal to 1: 13.8, greater than or equal to 1:14, or greater than or equal to 1:15, and the weight ratio of polyquaternium-73 to sodium laureth sulfate and polyquaternium-73 to cocamidopropyl betaine.
  • Each weight ratio is 1:20 or less, 1:19 or less, 1:18 or less, 1:17 or less, 1:16 or less, 1:15 or less, 1: 14.8 or less, 1: 14.6 or less, 1: 14.4 or less, 1 : 14.2 or less, 1:14 or less, 1: 13.8 or less, 1: 13.6 or less, 1: 13.4 or less, or 1:13 or less.
  • the weight ratio of polyquaternium-73 and sodium lauroyl salcosinate is 1: 1 or more, 1: 2 or more, 1: 3 or more, 1: 3.2 or more, 1: 3.4 or more, 1: 3.6 or more, 1: 3.8 or more, 1: 4.0 or more, 1: 4.2 or more, 1: 4.4 or more, 1: 4.6 or more, or 1: 5 or more.
  • the weight ratio of polyquaternium-73 and sodium lauroyl salcosinate is 1: 7 or less, 1: 6 or less, 1: 5 or less, 1: 4.8 or less, 1: 4.6 or less, 1: 4.4 or less, 1: 4.2 or less, 1: 4 or less, 1: 3.8 or less, 1: 3.6 or less, or 1: 3.4 or less.
  • the shampoo composition according to the present invention may further contain additives such as preservatives, thickeners, viscosity adjusters, pH adjusters, flavorings, dyes, conditioning agents that can be used as a component of the shampoo composition.
  • preservative sodium benzoate, phenoxyethanol and the like can be used.
  • thickener and viscosity modifier include carbomer, hydroxypropylmethylcellulose, hydroxymethylcellulose, sodium chloride, ammonium chloride and the like.
  • Citric acid, sodium hydroxide, triethanolamine, etc. are mentioned as a pH adjuster.
  • the dyes include water-soluble tar pigments.
  • additional conditioning agents include animal and vegetable extracts, proteins and protein variants.
  • Example 2 Example 3
  • Example 4 Purified water 81.80 81.80 81.80 81.80 81.80 81.80 81.80 81.80 Polyquaternium-10 0.50 - - - - Polyquaternium-73 - 0.50 0.50 0.50 0.50 Sodium citrate 0.20 0.20 0.20 0.20 0.20 Sodium laureth sulfate 7.00 16.00 - - 7.00 Cocamidopropyl betaine 7.00 - 16.00 - 7.00 Sodium Lauroyl Sarcosinate 2.00 - - 16.00 2.00 fragrance 1.00 1.00 1.00 1.00 1.00 Sodium benzoate 0.50 0.50 0.50 0.50 0.50 Unit (% by weight) 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00
  • the composition of the present invention In order to measure the hair softness at the time of rinsing the composition of the present invention, it is immersed in a 10% dilution solution of the Comparative Examples and Examples 1 to 3 for 3 minutes and then mounted on a combine machine (water) in a shower machine while rinsing hair The force taken during combing was measured and the results are shown in Table 2 below.
  • the Combing test is a general test method performed in the art, and means that the higher the value of the force required when combing the hair, the poor the conditioning effect.
  • Example 4 As a result of the experiment, compared to the comparative example using PQ-10, the case of Examples 1 to 4 using PQ-73 has a small force when combing, it was confirmed that the softness in dry hair is better. In particular, in Example 4, the softness in the dry hair was the best.
  • composition of the present invention When the composition of the present invention is applied, normal hair and dyed hair tress are prepared to compare the shine in hair.
  • the compositions of Comparative Example and Example 4 above were used five times in each tress. 30 °C, 40% relative humidity) was incubated in a constant temperature room for one day and completely dried. Dried hair is shown in FIG. 2. The hair was fixed to a gloss measurement device and the results of measuring the gloss are shown in Table 4 below as Luster Values.
  • the Luster Value was excellent in both the dyed hair and the normal hair during the treatment of Example 4 compared to the comparative example, and the dyed hair and the normal hair treated in Example 4 had less light scattering and excellent hair clarity as shown in FIG.
  • the composition of the present invention it was confirmed that the gloss of the hair is enhanced.
  • Example 2 Example 3
  • Example 4 Amount of foam 4.57 6.86 6.14 5.57 7.29 Soft when rinsing 3.71 4.00 7.29 6.86 8.14 Softness in wet conditions 4.43 4.71 7.00 6.43 7.86 Softness after drying 4.14 4.86 6.57 6.71 8.00 Hair shine 4.86 5.29 5.29 6.14 6.86
  • Example 1 to 4 are superior to the comparative example, 2) in rinsing, soft in wet and soft after drying, Examples 1 to 4 were superior to the comparative example, and 3) Examples 1 to 4 were superior to the comparative example even in hair shine. In particular, Example 4 showed the best in all of the above evaluation items.

Abstract

The present specification relates to a composition for hair having a transparent formulation comprising polyquaternium-73. The composition may further comprise a surfactant in addition to the polyquaternium-73, wherein the surfactant is at least one surfactant selected from a group consisting of sodium laureth sulfate, sodium lauroyl sarcosinate and cocamidopropyl betaine. The composition according to one aspect of the present invention provides a transparent formulation and exhibits excellent effects in terms of foaming ability, conditioning effect, and hair gloss enhancement.

Description

모발용 투명 제형 조성물Transparent formulation composition for hair
본 명세서는 폴리쿼터늄-73(PQ-73)을 포함하는 모발용 투명 제형 조성물에 관한 것이다.The present specification relates to a transparent formulation composition for hair comprising polyquaternium-73 (PQ-73).
모발세정제인 샴푸는 모발 및 두피의 오염물과 피지를 제거함으로써 모발을 깨끗하게 만들어 주지만 샴푸과정을 통해 피지 및 모발의 보습성분이 제거되어 모발의 부드러움이 약해지고 건조해져 모발이 엉키고 다루기 힘든 상태가 된다. 이를 보완하기 위하여 일반적인 불투명 샴푸의 경우에는 모발 컨디셔닝제를 포함시켜 모발의 유연성을 증가시키고 있지만, 투명 샴푸의 경우에는 통상적인 모발 컨디셔닝제 사용시 제형이 불투명해 지는 제약이 있다.Shampoo, a hair cleaner, makes hair clean by removing contaminants and sebum from the hair and scalp, but the shampoo process removes the moisturizing ingredients of the sebum and hair, making the hair soft and dry, making the hair tangled and difficult to handle. In order to compensate for this, in the case of a general opaque shampoo to increase the flexibility of the hair by including a hair conditioning agent, in the case of a transparent shampoo there is a constraint that the formulation becomes opaque when using a conventional hair conditioner.
투명 샴푸는 청결하고 순한 이미지로 유아 또는 어린이용 샴푸로 선호되고, 미려한 외관으로 심미적인 장점을 제공하나, 통상적인 모발 컨디셔닝제 사용시 제형이 불투명해져 첨가하여야 할 컨디셔닝 성분들이 제한적이기 때문에 제품 성능도 불만족스럽고 기포량도 부족하여 샴푸로서의 기능이 부족한 것이 문제이다. 성인들의 모발은 오염, 잦은 퍼머, 헤어 드라이, 염색, 빗질 등에 의한 손상이 심해 일정수준 이상의 컨디셔닝 효과를 가지는 모발세정제가 필요하고, 투명 샴푸의 경우 제형의 제약으로 인하여 소비자들이 원하는 수준을 만족시키지 못하고 있다.Transparent shampoos are preferred as infant or child shampoos with a clean and mild image, and offer aesthetic benefits with a beautiful appearance, but the product performance is also unsatisfactory because the formulation is opaque due to the limited amount of conditioning ingredients to be added when using conventional hair conditioners. The problem is that there is a lack of air bubbles and a lack of function as a shampoo. Adult hair is damaged by contamination, frequent perm, hair dry, dyeing, and combing, so it needs a hair cleanser that has a certain level of conditioning effect. have.
종래 투명샴푸에 사용되는 양이온성 폴리머는 PQ-10이 주로 사용되어 왔으며, 상기와 같은 문제점으로 인해 모발에 부드러움을 부여하고 윤기를 부여하는데 한계가 있었다.Conventional cationic polymers used in transparent shampoos have been mainly used PQ-10, there is a limit to give the hair softness and shine due to the above problems.
따라서, 투명성을 유지하여 청결한 느낌을 주는 미관을 유지하면서도, 샴푸 본연의 역할인 세정력이 저하되지 않고, 기포가 풍부하고, 빌드업이 없는 우수한 컨디셔닝 효과를 낼 수 있는 투명 샴푸 조성물에 대한 연구가 더욱 필요하다.Therefore, while maintaining aesthetics to maintain a clean feeling while maintaining transparency, research on a transparent shampoo composition that can produce excellent conditioning effects without deterioration of cleaning power, which is a role of the shampoo, and rich bubbles, and no build-up is further studied. need.
선행기술문헌Prior art literature
한국 공개특허 10-2009-0112120 호Korea Patent Publication No. 10-2009-0112120
본 발명의 일측면은 투명한 제형의 모발용 조성물을 제공하고자 한다.One aspect of the present invention is to provide a composition for hair in a transparent formulation.
본 발명의 일측면은 모발용 조성물로서, 양이온성 폴리머로 폴리쿼터늄-73(PQ-73)을 포함하는 투명한 제형의 모발용 조성물을 제공하고자 한다.One aspect of the present invention is to provide a hair composition of a transparent formulation comprising a polyquaternium-73 (PQ-73) as a cationic polymer as a hair composition.
본 발명의 일측면은 기포력이 우수하고, 컨디셔닝 효과가 우수하며, 모발 윤기 증진효과가 우수한 투명한 제형의 모발용 조성물을 제공하고자 한다.One aspect of the present invention is to provide a composition for hair of a transparent formulation having excellent foaming force, excellent conditioning effect, excellent hair glossiness enhancing effect.
본 발명의 일측면은 상기 조성물에 계면활성제를 더 포함하는 투명한 제형의 모발용 조성물을 제공하고자 한다.One aspect of the present invention is to provide a composition for hair of a transparent formulation further comprises a surfactant in the composition.
본 발명의 일측면은 투명한 제형의 모발용 조성물로 기포력이 우수하고, 컨디셔닝 효과가 우수하며, 모발 윤기 증진효과가 우수한 모발용 조성물을 제공하고자 한다.One aspect of the present invention is to provide a composition for hair in a transparent formulation excellent in foaming, excellent in the conditioning effect, excellent hair shine enhancement effect.
본 발명의 일측면은 폴리쿼터늄-73(PQ-73)을 포함하는 투명한 제형의 모발용 조성물을 제공한다.One aspect of the present invention provides a composition for hair in a transparent formulation comprising polyquaternium-73 (PQ-73).
본 발명의 일측면은 상기 조성물은 계면활성제를 더 포함하는 투명한 제형의 모발용 조성물을 제공한다.One aspect of the present invention provides a composition for hair in a transparent dosage form wherein the composition further comprises a surfactant.
구체적으로, 상기 계면활성제는 소듐 라우레스 설페이트(sodium laureth sulfate), 소듐 라우로일 살코시네이트(sodium lauroyl sarcosinate) 및 코카미도프로필 베타인(cocamidopropyl betaine) 로 이루어진 군에서 선택된 어느 하나 이상의 계면활성제일 수 있다.Specifically, the surfactant may be at least one surfactant selected from the group consisting of sodium laureth sulfate, sodium lauroyl sarcosinate, and cocamidopropyl betaine. Can be.
본 발명의 다른 측면은 상기 폴리쿼터늄-73은 전체 조성물에 대하여 0.01 내지 5 중량%인 투명한 제형의 모발용 조성물을 제공한다.Another aspect of the present invention provides a composition for hair of the transparent formulation of the polyquaternium-73 is 0.01 to 5% by weight based on the total composition.
본 발명의 다른 측면은 상기 계면 활성제는 전체 조성물에 대하여 1 내지 30 중량%인 투명한 제형의 모발용 조성물을 제공하며, 바람직하게 상기 계면 활성제는 전체 조성물에 대하여 10 내지 20 중량%인 투명한 제형의 모발용 조성물을 제공한다.Another aspect of the present invention provides a composition for hair in a transparent formulation wherein the surfactant is 1 to 30% by weight based on the total composition, preferably the surfactant is 10 to 20% by weight relative to the total composition To provide.
본 발명의 다른 측면은 상기 폴리쿼터늄-73과 상기 계면활성제를 1:20 내지 40의 중량비로 포함하는, 투명 제형의 모발용 조성물을 제공한다.Another aspect of the present invention provides a composition for hair in a transparent formulation comprising the polyquaternium-73 and the surfactant in a weight ratio of 1:20 to 40.
본 발명의 다른 측면은 상기 계면 활성제는 소듐 라우레스 설페이트(sodium laureth sulfate), 소듐 라우로일 살코시네이트(sodium lauroyl sarcosinate) 및 코카미도프로필 베타인(cocamidopropyl betaine)를 포함하고, 전체 조성물에 대하여 상기 소듐 라우레스 설페이트는 5 내지 10중량%이며, 상기 소듐 라우로일 살코시네이트는 5 내지 10중량%이고, 상기 코카미도프로필 베타인는 0.1 내지 5중량%인, 투명 제형의 모발용 조성물을 제공한다.Another aspect of the present invention, the surfactant comprises sodium laureth sulfate, sodium lauroyl sarcosinate and cocamidopropyl betaine, for the whole composition The sodium laureth sulfate is 5 to 10% by weight, the sodium lauroyl salcosinate is 5 to 10% by weight, and the cocamidopropyl betaine is 0.1 to 5% by weight to provide a composition for hair in a transparent formulation.
본 발명의 다른 측면은 상기 계면 활성제는 소듐 라우레스 설페이트(sodium laureth sulfate), 코카미도프로필 베타인(cocamidopropyl betaine) 및 소듐 라우로일 살코시네이트(sodium lauroyl sarcosinate)를 포함하고, 상기 폴리쿼터늄-73, 소듐 라우레스 설페이트, 코카미도프로필 베타인 및 소듐 라우로일 살코시네이트는 1 : 10 내지 20 : 10 내지 20 : 1 내지 7 의 중량비로 포함되는 투명 제형의 모발용 조성물을 제공한다. 구체적으로, 상기 폴리쿼터늄-73, 소듐 라우레스 설페이트, 코카미도프로필 베타인 및 소듐 라우로일 살코시네이트는 1 : 12 내지 16 : 12 내지 16 : 3 내지 5 의 중량비로 포함될 수 있다.In another aspect of the present invention, the surfactant includes sodium laureth sulfate, cocamidopropyl betaine, and sodium lauroyl sarcosinate, and the polyquaternium -73, Sodium Laureth Sulfate, Cocamidopropyl Betaine, and Sodium Lauroyl Salcosinate provide a composition for hair in a transparent formulation comprising a weight ratio of 1: 10 to 20: 10 to 20: 1 to 7. Specifically, the polyquaternium-73, sodium laureth sulfate, cocamidopropyl betaine and sodium lauroyl salcosinate may be included in a weight ratio of 1:12 to 16:12 to 16: 3 to 5.
본 발명의 또 다른 측면은 상기 투명 제형의 모발용 조성물은 세정용 조성물인 조성물을 제공한다.Another aspect of the present invention provides a composition for the hair composition of the transparent formulation is a cleaning composition.
본 발명의 일측면에 따른 조성물은 투명한 제형을 제공하는 효과를 가진다.The composition according to one aspect of the present invention has the effect of providing a transparent formulation.
본 발명의 일측면에 따른 조성물을 투명 샴푸로 사용하는 경우 청결하고 순한 이미지를 제공하는 효과가 있으며, 미려한 외관을 제공하는 효과가 있다.When using the composition according to one aspect of the present invention as a transparent shampoo has the effect of providing a clean and gentle image, has the effect of providing a beautiful appearance.
본 발명의 일측면에 따른 조성물을 모발에 적용하는 경우 헹굼 시 모발 부드러움이 우수한 효과를 가진다. When the composition according to one aspect of the present invention is applied to the hair, the hair softness at the time of rinsing has an excellent effect.
본 발명의 일측면에 따른 조성물을 모발에 적용하는 경우 젖은 상태에서의 모발 부드러움이 우수한 효과를 가진다.When the composition according to one aspect of the present invention is applied to hair, hair softness in the wet state has an excellent effect.
본 발명의 일측면에 따른 조성물을 모발에 적용하는 경우 건조 후 모발 부드러움이 우수한 효과를 가진다.When the composition according to one aspect of the present invention is applied to hair, hair softness after drying has an excellent effect.
본 발명의 일측면에 따른 조성물을 모발에 적용하는 경우 컨디셔닝 효과가 우수하다.When the composition according to one aspect of the present invention is applied to hair, the conditioning effect is excellent.
본 발명의 일측면에 따른 조성물을 모발에 적용하는 경우 모발에서 빛의 산란이 적고 모발 선명도가 증가하는 효과를 가진다.When the composition according to one aspect of the present invention is applied to hair, light has less scattering in the hair and has the effect of increasing hair clarity.
본 발명의 일측면에 따른 조성물을 모발에 적용하는 경우 모발의 윤기를 증가하는 효과를 가진다.When applying the composition according to one aspect of the invention to the hair has the effect of increasing the gloss of the hair.
본 발명의 일측면에 따른 조성물을 모발에 적용하는 경우 기포력 및 거품의 양이 우수한 효과를 가진다.When the composition according to one aspect of the present invention is applied to hair, the foaming force and the amount of foam have an excellent effect.
본 발명의 일측면에 따른 조성물을 투명한 제형을 제공하여 미려한 외관과 청결하고 순한 이미지를 제공함과 동시에, 모발에 적용하는 경우 컨디셔닝 효과 및 모발 윤기 증진에 있어서 우수한 효과를 나타낸다.The composition according to one aspect of the present invention provides a clear formulation to provide a beautiful appearance and clean and gentle image, and at the same time, when applied to the hair shows an excellent effect on the conditioning effect and hair glossiness.
도 1은 본 명세서 실시예 1 내지 4에 따라 제조된 투명 제형의 사진이다.1 is a photograph of a transparent formulation prepared according to Examples 1 to 4 of the present specification.
도 2는 본 명세서 비교예와 실시예 4를 정상모와 염색모에 적용한 경우의 사진이다.Figure 2 is a photograph when the present invention Comparative Example and Example 4 applied to normal hair and dyed hair.
도 3은 본 명세서 비교예와 실시예 1 내지 4를 전문 패널리스트가 거품의 양, 헹굼 시 부드러움, 젖은 상태에서의 부드러움, 건조 후 부드러움 및 모발윤기의 측면에서 각 조성물별로 평가한 데이터를 도시화한 것이다.FIG. 3 shows comparative examples of the present specification and Examples 1 to 4 showing data evaluated by each panelist in terms of amount of foam, softness during rinsing, softness in wet state, softness after drying, and hair shine. will be.
이하에서는, 본 발명이 속하는 기술분야에서 통상의 지식을 가진 자가 본 발명을 용이하게 실시할 수 있도록 하기 위하여, 본 발명에 관하여 상세히 설명하기로 한다.Hereinafter, in order to enable those skilled in the art to easily carry out the present invention, the present invention will be described in detail.
본 발명의 일측면은 양이온성 폴리머로서 폴리쿼터늄-73(PQ-73)을 포함하는 투명 제형의 모발용 조성물을 제공한다. One aspect of the present invention provides a composition for hair in a transparent formulation comprising polyquaternium-73 (PQ-73) as the cationic polymer.
본 발명의 일측면은 모발 세정을 위한 방법으로, 상기 방법은 양이온성 폴리머로서 폴리쿼터늄-73(PQ-73)을 포함하는 투명 제형의 조성물을 이를 필요로 하는 대상에 적용하는 단계를 포함하는 방법을 제공한다.One aspect of the invention is a method for hair cleansing, the method comprising applying a composition of a clear formulation comprising polyquaternium-73 (PQ-73) as a cationic polymer to a subject in need thereof Provide a method.
본 발명의 일측면은 모발 세정을 위한 투명 제형의 조성물을 제조하는데 있어서의 양이온성 폴리머로서 폴리쿼터늄-73(PQ-73)의 용도를 제공한다.상기 양이온성 폴리머는 컨디셔닝제로서, 일반적으로 폴리쿼터늄으로 불리고 있으며, 향상된 컨디셔닝 효과를 제공함과 동시에 제형의 투명화를 가능케 한다. 폴리쿼터늄-73(Poly quaternium-73)은 프로필트리모늄 클로라이드 아크릴아마이드, 에틸트리모늄 클로라이드 메타아크릴레이트 및 디메틸아크릴아마이드의 단량체들로 이루어진 폴리머릭 퀀터너리 암모늄 염이다.One aspect of the present invention provides the use of polyquaternium-73 (PQ-73) as a cationic polymer in preparing a composition of a clear formulation for hair cleaning. The cationic polymer is a conditioning agent, and generally Called polyquaternium, it provides improved conditioning effects and at the same time enables the formulation to be transparent. Poly quaternium-73 is a polymeric quaternary ammonium salt consisting of monomers of propyltrimonium chloride acrylamide, ethyltrimonium chloride methacrylate and dimethylacrylamide.
본 발명의 일측면에서, 상기 조성물은 계면활성제를 더 포함하는 투명 제형의 모발용 조성물을 제공한다.In one aspect of the invention, the composition provides a composition for hair of a transparent formulation further comprises a surfactant.
구체적으로, 상기 계면활성제는 소듐 라우레스 설페이트(sodium laureth sulfate), 소듐 라우로일 살코시네이트(sodium lauroyl sarcosinate) 및 코카미도프로필 베타인(cocamidopropyl betaine) 로 이루어진 군에서 선택된 어느 하나 이상의 계면활성제일 수 있다.Specifically, the surfactant may be at least one surfactant selected from the group consisting of sodium laureth sulfate, sodium lauroyl sarcosinate, and cocamidopropyl betaine. Can be.
상기 계면활성제는 음이온 계면활성제로서, 소듐 라우레스 설페이트(sodium laureth sulfate) 및 소듐 라우로일 살코시네이트(sodium lauroyl sarcosinate) 중 어느 하나 이상을 포함할 수 있다. 상기 계면활성제는 양쪽성 계면활성제로서 코카미도프로필 베타인(cocamidopropyl betaine)을 포함할 수 있다.The surfactant may include any one or more of sodium laureth sulfate and sodium lauroyl sarcosinate as an anionic surfactant. The surfactant may include cocamidopropyl betaine as an amphoteric surfactant.
본 발명의 다른 측면에서, 상기 폴리쿼터늄-73은 전체 조성물에 대하여 0.01 내지 5 중량%인 투명 제형의 모발용 조성물을 제공할 수 있다. 구체적으로 상기 폴리쿼터늄-73은 전체 조성물에 대하여 0.01 중량% 이상, 0.05중량% 이상, 0.10중량% 이상, 0.15중량% 이상, 0.20중량% 이상, 0.25중량% 이상, 0.30중량% 이상, 0.35중량% 이상, 0.40중량% 이상, 0.45중량% 이상, 0.46중량% 이상, 0.47중량% 이상, 0.48중량% 이상, 0.49중량% 이상, 0.50중량% 이상, 0.51중량% 이상, 0.52중량% 이상, 0.53중량% 이상, 0.54중량% 이상, 0.55중량% 이상, 0.60중량% 이상, 0.70중량% 이상, 0.80중량% 이상, 0.90중량% 이상 또는 1.00중량% 이상일 수 있다. In another aspect of the invention, the polyquaternium-73 may provide a composition for hair in a transparent formulation of 0.01 to 5% by weight based on the total composition. Specifically, the polyquaternium-73 is 0.01% by weight, 0.05% by weight, 0.10% by weight, 0.15% by weight, 0.20% by weight, 0.25% by weight, 0.30% by weight, 0.35% by weight based on the total composition. Or more, 0.40 or more, 0.45 or more, 0.46 or more, 0.47 or more, 0.48 or more, 0.49 or more, 0.50 or more, 0.51 or more, 0.52 or more, 0.53 or more Or at least 0.54 wt%, at least 0.55 wt%, at least 0.60 wt%, at least 0.70 wt%, at least 0.80 wt%, at least 0.90 wt% or at least 1.00 wt%.
또한, 상기 폴리쿼터늄-73은 전체 조성물에 대하여 5중량%이하, 4.5중량%이하, 4.0중량%이하, 3.5중량%이하, 3중량%이하, 2.5중량%이하, 2.0중량%이하, 1.5중량%이하, 1.0중량%이하, 0.9중량%이하, 0.8중량%이하, 0.7중량%이하, 0.6중량%이하, 0.59중량%이하, 0.58중량%이하, 0.57중량%이하, 0.56중량%이하, 0.55중량%이하, 0.54중량%이하, 0.53중량%이하, 0.52중량%이하, 0.51중량%이하 또는 0.50중량%이하일 수 있다.In addition, the polyquaternium-73 is less than 5% by weight, 4.5% by weight, 4.0% by weight, 3.5% by weight, 3% by weight, 2.5% by weight, 2.0% by weight, 1.5% by weight based on the total composition. % Or less, 1.0% or less, 0.9% or less, 0.8% or less, 0.7% or less, 0.6% or less, 0.59% or less, 0.58% or less, 0.57% or less, 0.56% or less, or 0.55% or less It may be up to 0.54% by weight, up to 0.53% by weight, up to 0.52% by weight, up to 0.51% by weight or up to 0.50% by weight.
양이온성 폴리머인 폴리쿼터늄-73의 함량이 상기 범위 내 일때, 투명한 제형의 형성이 가능하다. When the content of the cationic polymer polyquaternium-73 is within the above range, the formation of a transparent formulation is possible.
본 발명의 다른 측면은 상기 계면 활성제는 전체 조성물에 대하여 0.1 내지 30 중량%인 투명 제형의 모발용 조성물을 제공하며, 바람직하게 상기 계면 활성제는 전체 조성물에 대하여 10 내지 20 중량%인 투명 제형의 모발용 조성물을 제공한다. 구체적으로 상기 계면 활성제는 전체 조성물에 대하여 0.1 중량% 이상, 0.5중량% 이상, 1중량% 이상, 1.5중량% 이상, 1.6중량% 이상, 1.7중량% 이상, 1.8중량% 이상, 1.9중량% 이상, 2중량% 이상, 2.1중량% 이상, 2.2중량% 이상, 2.3중량% 이상, 2.4중량% 이상, 2.5중량% 이상, 3중량% 이상, 4중량% 이상, 5중량% 이상, 6중량% 이상, 6.5중량% 이상, 6.6중량% 이상, 6.7중량% 이상, 6.8중량% 이상, 6.9중량% 이상, 7중량% 이상, 7.1중량% 이상, 7.2중량% 이상, 7.3중량% 이상, 7.4중량% 이상, 7.5중량% 이상, 8중량% 이상, 9중량% 이상, 10중량% 이상, 11중량% 이상, 12중량% 이상, 13중량% 이상, 14중량% 이상, 15중량% 이상, 15.5중량% 이상, 15.6중량% 이상, 15.7중량% 이상, 15.8중량% 이상, 15.9중량% 이상, 16중량% 이상, 16.1중량% 이상, 16.2중량% 이상, 16.3중량% 이상, 16.4중량% 이상, 16.5중량% 이상 또는 17중량% 이상일 수 있다.Another aspect of the present invention provides a composition for hair in a transparent formulation wherein the surfactant is 0.1 to 30% by weight based on the total composition, preferably the surfactant is 10 to 20% by weight relative to the total composition To provide. Specifically, the surfactant is 0.1% by weight, 0.5% by weight, 1% by weight, 1.5% by weight, 1.6% by weight, 1.7% by weight, 1.8% by weight, 1.9% by weight, At least 2 wt%, at least 2.1 wt%, at least 2.2 wt%, at least 2.3 wt%, at least 2.4 wt%, at least 2.5 wt%, at least 3 wt%, at least 4 wt%, at least 5 wt%, at least 6 wt%, At least 6.5%, at least 6.6%, at least 6.7%, at least 6.8%, at least 6.9%, at least 7%, at least 7.1%, at least 7.2%, at least 7.3%, at least 7.4%, 7.5% by weight, 8% by weight, 9% by weight, 10% by weight, 11% by weight, 12% by weight, 13% by weight, 14% by weight, 15% by weight, 15.5% by weight, 15.6% by weight, 15.7% by weight, 15.8% by weight, 15.9% by weight, 16% by weight, 16.1% by weight, 16.2% by weight, 16.3% by weight, 16.4% by weight, 16.5% by weight or Can be more than 17% by weight have.
또한, 상기 계면 활성제는 전체 조성물에 대하여 30중량% 이하, 25중량% 이하, 20중량% 이하, 19중량% 이하, 18중량% 이하, 17중량% 이하, 16.9중량% 이하, 16.8중량% 이하, 16.7중량% 이하, 16.6중량% 이하, 16.5중량% 이하, 16.4중량% 이하, 16.3중량% 이하, 16.2중량% 이하, 16.1중량% 이하, 16중량% 이하, 13중량% 이하, 10중량% 이하, 9중량% 이하, 8중량% 이하, 7.9중량% 이하, 7.8중량% 이하, 7.7중량% 이하, 7.6중량% 이하, 7.5중량% 이하, 7.4중량% 이하, 7.3중량% 이하, 7.2중량% 이하, 7.1중량% 이하, 7중량% 이하, 5중량% 이하, 3중량% 이하, 2.5중량% 이하, 2.4중량% 이하, 2.3중량% 이하, 2.2중량% 이하, 2.1중량% 이하 또는 2.0중량% 이하일 수 있다.In addition, the surfactant is 30% by weight, 25% by weight, 20% by weight, 19% by weight, 18% by weight, 17% by weight, 16.9% by weight, 16.8% by weight, 16.7 wt% or less, 16.6 wt% or less, 16.5 wt% or less, 16.4 wt% or less, 16.3 wt% or less, 16.2 wt% or less, 16.1 wt% or less, 16 wt% or less, 13 wt% or less, 10 wt% or less, 9 wt% or less, 8 wt% or less, 7.9 wt% or less, 7.8 wt% or less, 7.7 wt% or less, 7.6 wt% or less, 7.5 wt% or less, 7.4 wt% or less, 7.3 wt% or less, 7.2 wt% or less, It can be 7.1 wt% or less, 7 wt% or less, 5 wt% or less, 3 wt% or less, 2.5 wt% or less, 2.4 wt% or less, 2.3 wt% or less, 2.2 wt% or less, 2.1 wt% or less or 2.0 wt% or less. have.
계면 활성제의 함량이 상기 범위 내 일 때, 기포력이 우수하고, 컨디셔닝 효과 및 모발에 적용 시 부드러움이 우수하며, 모발의 윤기증진 효과가 우수하다.When the content of the surfactant is in the above range, it is excellent in the foaming force, excellent in the conditioning effect and softness when applied to the hair, it is excellent in the hair shiny effect.
본 발명의 다른 측면은 상기 폴리쿼터늄-73과 상기 계면활성제를 1:20 내지 40의 중량비로 포함하는, 투명 제형의 모발용 조성을 제공한다. 구체적으로 상기 폴리쿼터늄-73과 상기 계면활성제의 중량비는 1:20 이상, 1:21 이상, 1:22 이상, 1:23 이상, 1:24 이상, 1:25 이상, 1:26 이상, 1:27 이상, 1:28 이상, 1:29 이상, 1:30 이상, 1:31 이상, 1:31.2 이상, 1:31.4 이상, 1:31.6 이상, 1:31.8 이상, 1:32 이상, 1:32.2 이상, 1:32.6 이상 또는 1:33 이상일 수 있다.Another aspect of the invention provides a composition for hair of a transparent formulation comprising the polyquaternium-73 and the surfactant in a weight ratio of 1:20 to 40. Specifically, the weight ratio of the polyquaternium-73 and the surfactant is 1:20 or more, 1:21 or more, 1:22 or more, 1:23 or more, 1:24 or more, 1:25 or more, 1:26 or more, 1:27 or more, 1:28 or more, 1:29 or more, 1:30 or more, 1:31 or more, 1: 31.2 or more, 1: 31.4 or more, 1: 31.6 or more, 1: 31.8 or more, 1:32 or more, 1: 32.2 or greater, 1: 32.6 or greater, or 1:33 or greater.
또한, 상기 폴리쿼터늄-73과 상기 계면활성제의 중량비는 1:40 이하, 1:39 이하, 1:38 이하, 1:37 이하, 1:36 이하, 1:35 이하, 1:34 이하, 1:33 이하, 1:32.8 이하, 1:32.6 이하, 1:32.4 이하, 1:32.2 이하, 1:32 이하, 1:31.8 이하, 1:31.6 이하 또는 1:30 이하일 수 있다. In addition, the weight ratio of the polyquaternium-73 and the surfactant is 1:40 or less, 1:39 or less, 1:38 or less, 1:37 or less, 1:36 or less, 1:35 or less, 1:34 or less, 1:33 or less, 1: 32.8 or less, 1: 32.6 or less, 1: 32.4 or less, 1: 32.2 or less, 1:32 or less, 1: 31.8 or less, 1: 31.6 or less, or 1:30 or less.
폴리쿼터늄-73과 계면 활성제의 중량비가 상기 범위 내 일 때, 기포력이 우수하고, 컨디셔닝 효과 및 모발에 적용 시 부드러움이 우수하며, 모발의 윤기증진 효과가 우수하다.When the weight ratio of the polyquaternium-73 and the surfactant is in the above range, it is excellent in the foaming force, excellent in the conditioning effect and softness when applied to the hair, it is excellent in the hair shiny effect.
본 발명의 다른 측면은 상기 계면 활성제는 소듐 라우레스 설페이트(sodium laureth sulfate), 코카미도프로필 베타인(cocamidopropyl betaine) 및 소듐 라우로일 살코시네이트(sodium lauroyl sarcosinate)를 포함하고, 전체 조성물에 대하여 상기 소듐 라우레스 설페이트는 5 내지 10중량%이며, 상기 코카미도프로필 베타인은 5 내지 10중량%이고, 상기 소듐 라우로일 살코시네이트는 0.1 내지 5중량%인, 모발용 조성물을 제공한다.According to another aspect of the present invention, the surfactant includes sodium laureth sulfate, cocamidopropyl betaine, and sodium lauroyl sarcosinate. The sodium laureth sulfate is 5 to 10% by weight, the cocamidopropyl betaine is 5 to 10% by weight, the sodium lauroyl salcosinate is 0.1 to 5% by weight to provide a hair composition.
본 발명의 다른 측면은 상기 계면 활성제는 소듐 라우레스 설페이트(sodium laureth sulfate), 코카미도프로필 베타인(cocamidopropyl betaine) 및 소듐 라우로일 살코시네이트(sodium lauroyl sarcosinate)를 포함하고, 상기 폴리쿼터늄-73, 소듐 라우레스 설페이트, 코카미도프로필 베타인 및 소듐 라우로일 살코시네이트는 1 : 10 내지 20 : 10 내지 20 : 1 내지 7 의 중량비로 포함되는 투명 제형의 모발용 조성물을 제공한다. 바람직하게는, 상기 폴리쿼터늄-73, 소듐 라우레스 설페이트, 코카미도프로필 베타인 및 소듐 라우로일 살코시네이트는 1 : 12 내지 16 : 12 내지 16 : 3 내지 5 의 중량비일 수 있다.In another aspect of the present invention, the surfactant includes sodium laureth sulfate, cocamidopropyl betaine, and sodium lauroyl sarcosinate, and the polyquaternium -73, Sodium Laureth Sulfate, Cocamidopropyl Betaine, and Sodium Lauroyl Salcosinate provide a composition for hair in a transparent formulation comprising a weight ratio of 1: 10 to 20: 10 to 20: 1 to 7. Preferably, the polyquaternium-73, sodium laureth sulfate, cocamidopropyl betaine and sodium lauroyl salcosinate may be in a weight ratio of 1:12 to 16:12 to 16: 3 to 5.
구체적으로, 상기 계면 활성제가 소듐 라우레스 설페이트(sodium laureth sulfate), 코카미도프로필 베타인(cocamidopropyl betaine) 및 소듐 라우로일 살코시네이트(sodium lauroyl sarcosinate)를 포함하는 경우, 폴리쿼터늄-73과 소듐 라우레스 설페이트의 중량비와 폴리쿼터늄-73과 코카미도프로필 베타인의 각각의 중량비는 1:10 이상, 1:11 이상, 1:12 이상, 1:13 이상, 1:13.2 이상, 1:13.4 이상, 1:13.6 이상, 1:13.8 이상, 1:14 이상 또는 1:15 이상일 수 있으며, 또한, 폴리쿼터늄-73과 소듐 라우레스 설페이트의 중량비와 폴리쿼터늄-73과 코카미도프로필 베타인의 각각의 중량비는 1:20 이하, 1:19 이하, 1:18 이하, 1:17 이하, 1:16 이하, 1:15 이하, 1:14.8 이하, 1:14.6 이하, 1:14.4 이하, 1:14.2 이하, 1:14 이하, 1:13.8 이하, 1:13.6 이하, 1:13.4 이하 또는 1:13 이하일 수 있다. 또한, 폴리쿼터늄-73와 소듐 라우로일 살코시네이트의 중량비는 1:1 이상, 1:2 이상, 1:3 이상, 1:3.2 이상, 1:3.4 이상, 1:3.6 이상, 1:3.8 이상, 1:4.0 이상, 1:4.2 이상, 1:4.4 이상, 1:4.6 이상 또는 1:5 이상일 수 있다. 또한, 폴리쿼터늄-73와 소듐 라우로일 살코시네이트의 중량비는 1:7 이하, 1:6 이하, 1:5 이하, 1:4.8 이하, 1:4.6 이하, 1:4.4 이하, 1:4.2 이하, 1:4 이하, 1:3.8 이하, 1:3.6 이하 또는 1:3.4 이하일 수 있다.Specifically, when the surfactant comprises sodium laureth sulfate, cocamidopropyl betaine and sodium lauroyl sarcosinate, polyquaternium-73 and The weight ratio of sodium laureth sulfate and the weight ratio of polyquaternium-73 and cocamidopropyl betaine are 1:10 or more, 1:11 or more, 1:12 or more, 1:13 or more, 1: 13.2 or more, 1: 13.4 Or greater than 1: 13.6, greater than or equal to 1: 13.8, greater than or equal to 1:14, or greater than or equal to 1:15, and the weight ratio of polyquaternium-73 to sodium laureth sulfate and polyquaternium-73 to cocamidopropyl betaine. Each weight ratio is 1:20 or less, 1:19 or less, 1:18 or less, 1:17 or less, 1:16 or less, 1:15 or less, 1: 14.8 or less, 1: 14.6 or less, 1: 14.4 or less, 1 : 14.2 or less, 1:14 or less, 1: 13.8 or less, 1: 13.6 or less, 1: 13.4 or less, or 1:13 or less. In addition, the weight ratio of polyquaternium-73 and sodium lauroyl salcosinate is 1: 1 or more, 1: 2 or more, 1: 3 or more, 1: 3.2 or more, 1: 3.4 or more, 1: 3.6 or more, 1: 3.8 or more, 1: 4.0 or more, 1: 4.2 or more, 1: 4.4 or more, 1: 4.6 or more, or 1: 5 or more. In addition, the weight ratio of polyquaternium-73 and sodium lauroyl salcosinate is 1: 7 or less, 1: 6 or less, 1: 5 or less, 1: 4.8 or less, 1: 4.6 or less, 1: 4.4 or less, 1: 4.2 or less, 1: 4 or less, 1: 3.8 or less, 1: 3.6 or less, or 1: 3.4 or less.
상기 폴리쿼터늄-73, 소듐 라우레스 설페이트, 코카미도프로필 베타인 및 소듐 라우로일 살코시네이트의 중량비가 상기 범위 내 일 때, 기포력이 우수하고, 컨디셔닝 효과 및 모발에 적용 시 부드러움이 우수하며, 모발의 윤기증진 효과가 우수하다.When the weight ratio of the polyquaternium-73, sodium laureth sulfate, cocamidopropyl betaine and sodium lauroyl salcosinate is within the above range, excellent foaming power, excellent conditioning effect and softness when applied to hair It is excellent in hair's luster enhancement effect.
이 외에도, 본 발명에 따른 샴푸 조성물에는 통상적으로 샴푸 조성물의 성분으로 사용될 수 있는 방부제, 점증제, 점도조정제, pH조정제, 향료, 염료, 컨디셔닝제 등의 첨가제가 더 함유될 수 있다. 방부제로는 소듐벤조에이트, 페녹시에탄올 등이 사용될 수 있다. 점증제와 점도 조정제로는 카보머, 하이드록시프로필메틸셀룰로오스, 하이드록시 메틸셀룰로오스, 염화나트륨, 염화암모늄 등을 들 수 있다. pH조정제로는 구연산, 수산화나트륨, 트리에탄올아민 등을 들 수 있다. 염료로는 수용성 타르색소 등을 들 수 있다. 그리고 추가 컨디셔닝제로는 동식물성 추출물, 단백질 및 단백질 변형체등을 들 수 있다.In addition, the shampoo composition according to the present invention may further contain additives such as preservatives, thickeners, viscosity adjusters, pH adjusters, flavorings, dyes, conditioning agents that can be used as a component of the shampoo composition. As the preservative, sodium benzoate, phenoxyethanol and the like can be used. Examples of the thickener and viscosity modifier include carbomer, hydroxypropylmethylcellulose, hydroxymethylcellulose, sodium chloride, ammonium chloride and the like. Citric acid, sodium hydroxide, triethanolamine, etc. are mentioned as a pH adjuster. Examples of the dyes include water-soluble tar pigments. And additional conditioning agents include animal and vegetable extracts, proteins and protein variants.
이하, 본 발명의 내용을 실시예 및 비교예를 통하여 보다 구체적으로 설명한다. 이들 실시예는 본 발명의 내용을 이해하기 위해 제시되는 것일 뿐 본 발명의 권리 범위가 이들 실시예와 시험예로 한정되는 것은 아니고, 당업계에서 통상적으로 주지된 변형, 치환 및 삽입 등을 수행할 수 있으며, 이에 대한 것도 본 발명의 범위에 포함된다.Hereinafter, the content of the present invention will be described in more detail through examples and comparative examples. These examples are provided only for understanding the contents of the present invention, but the scope of the present invention is not limited to these examples and test examples, and modifications, substitutions, and insertions commonly known in the art may be performed. It may be included in the scope of the present invention.
실시예Example 1 내지 4 및  1 to 4 and 비교예Comparative example
하기 표 1에 기재된 조성으로 실시예 1 내지 4 모발용 샴푸 조성물 및 비교예를 제조하였다. 하기 PQ-73(Mitsubishi Chemical Corporation, Diasleek C-802), PQ-10(KCI, POLYQUAT3000KC) , 소듐 라우레스 설페이트(Sodium laureth sulfate)(Miwon, MICOLIN ES628), Cocamidopropyl betaine(Miwon, MITAINE CA) 및 Sodium lauryl Sarcosinate(Miwon, Miami L-30)은 시판되는 제품들을 구입하여 사용하였다. 제조된 실시예 1 내지 4의 제형 사진은 도1과 같이 투명한 제형임을 확인하였다.To the composition shown in Table 1 to Examples 1 to 4 hair shampoo composition and Comparative Example were prepared. PQ-73 (Mitsubishi Chemical Corporation, Diasleek C-802), PQ-10 (KCI, POLYQUAT3000KC), Sodium laureth sulfate (Miwon, MICOLIN ES628), Cocamidopropyl betaine (Miwon, MITAINE CA) and Sodium Lauryl Sarcosinate (Miwon, Miami L-30) purchased and used commercially available products. Formulation pictures of Examples 1 to 4 were confirmed to be a transparent formulation as shown in FIG.
원료명Raw material name 비교예Comparative example 실시예1Example 1 실시예2Example 2 실시예3Example 3 실시예4Example 4
정제수Purified water 81.8081.80 81.8081.80 81.8081.80 81.8081.80 81.8081.80
Polyquaternium-10Polyquaternium-10 0.500.50 -- -- -- --
Polyquaternium-73Polyquaternium-73 -- 0.500.50 0.500.50 0.500.50 0.500.50
Sodium citrateSodium citrate 0.200.20 0.200.20 0.200.20 0.200.20 0.200.20
Sodium laureth sulfateSodium laureth sulfate 7.007.00 16.0016.00 -- -- 7.007.00
Cocamidopropyl betaineCocamidopropyl betaine 7.007.00 -- 16.0016.00 -- 7.007.00
Sodium Lauroyl SarcosinateSodium Lauroyl Sarcosinate 2.002.00 -- -- 16.0016.00 2.002.00
fragrancefragrance 1.001.00 1.001.00 1.001.00 1.001.00 1.001.00
Sodium benzoateSodium benzoate 0.500.50 0.500.50 0.500.50 0.500.50 0.500.50
단위(중량%)Unit (% by weight) 100.00100.00 100.00100.00 100.00100.00 100.00100.00 100.00100.00
[[ 시험예Test Example 1] 모발 부드러움 비교 1] hair softness comparison
(( 시험예1Test Example 1 -1) 헹굼 시의 모발 부드러움 실험-1) Hair softness test during rinsing
본 발명 조성물의 헹굼 시의 모발 부드러움을 측정하기 위하여, 상기 비교예와 실시예 1 내지 4의 10% 희석액에 3분간 담지 후 콤바인 기계(combining machine)에 장착하고, 샤워기에 물을 틀어 모발 헹굼 중 빗질 시 걸리는 힘을 측정하였고, 그 결과를 하기 표 2에 나타내었다. 상기 Combing test란 당업계에서 실시하는 일반적인 테스트 방법으로서, 모발을 빗질할 때 소요되는 힘의 수치가 높을수록 컨디셔닝 효과가 좋지 않음을 의미한다.In order to measure the hair softness at the time of rinsing the composition of the present invention, it is immersed in a 10% dilution solution of the Comparative Examples and Examples 1 to 3 for 3 minutes and then mounted on a combine machine (water) in a shower machine while rinsing hair The force taken during combing was measured and the results are shown in Table 2 below. The Combing test is a general test method performed in the art, and means that the higher the value of the force required when combing the hair, the poor the conditioning effect.
걸리는 힘(N)Force required (N)
비교예Comparative example 284.30284.30
실시예 1Example 1 280.05280.05
실시예 2Example 2 258.40258.40
실시예 3Example 3 268.42268.42
실시예 4Example 4 233.09233.09
실험 결과 PQ-10을 사용한 비교예에 비하여, PQ-73을 사용한 실시예 1 내지 4의 경우가 모발 헹굼 중 빗질 시 걸리는 힘이 작으므로, 헹굼 시 모발에서의 부드러움이 더 우수함을 확인하였다. 특히, 실시예 4의 경우 그 헹굼 시 모발에서의 부드러움이 가장 우수하였다.Experimental results Compared to the comparative example using the PQ-10, the case of Examples 1 to 4 using the PQ-73 has a small force during combing during hair rinsing, it was confirmed that the softness in the hair during rinsing is better. In particular, in the case of Example 4, the softness in the hair during the rinsing was the best.
(( 시험예1Test Example 1 -2) 건조 모발의 빗질 실험-2) combing dry hair
본 발명 조성물을 사용한 모발의 건조 시 모발 부드러움을 측정하기 위하여, 상기 비교예와 실시예 1 내지 4의 10% 희석액으로 트레스를 세정한 후 하루 동안 완전히 건조하였다. 드라이 콤바인 기계(dry combining machine)를 이용하여 빗질 시 걸리는 힘을 측정하였고, 그 결과를 하기 표 3에 나타내었다.In order to measure hair softness when drying the hair using the composition of the present invention, the tresses were washed with 10% dilution of Comparative Examples and Examples 1 to 4 and then completely dried for one day. The force taken when combing was measured using a dry combine machine, and the results are shown in Table 3 below.
걸리는 힘(N)Force required (N)
비교예Comparative example 133.96133.96
실시예 1Example 1 122.84122.84
실시예 2Example 2 98.0598.05
실시예 3Example 3 104.80104.80
실시예 4Example 4 89.5389.53
실험 결과 PQ-10을 사용한 비교예에 비하여, PQ-73을 사용한 실시예 1 내지 4의 경우가 빗질 시 걸리는 힘이 작으므로, 건조모발에서의 부드러움이 더 우수함을 확인하였다. 특히, 실시예 4의 경우 건조모발에서의 부드러움이 가장 우수하였다.As a result of the experiment, compared to the comparative example using PQ-10, the case of Examples 1 to 4 using PQ-73 has a small force when combing, it was confirmed that the softness in dry hair is better. In particular, in Example 4, the softness in the dry hair was the best.
[[ 시험예Test Example 2] 모발의 윤기 비교 2] hair gloss comparison
본 발명 조성물을 적용하는 경우, 모발에서의 윤기를 비교하기 위해, 정상모와 염색모 트레스를 준비한다. 상기의 비교예와 실시예 4의 조성물을 각각의 트레스에 5회씩 반복하여 사용하였다. 30℃, 40%상대습도)의 항온실에 하루동안 인큐베이팅 시켜 완전 건조하였다. 건조된 모발은 도 2에 도시하였다. 모발을 윤기 측정 기기에 고정시키고 윤기를 측정한 결과를 Luster Value로 하기 표 4에 나타내었다.When the composition of the present invention is applied, normal hair and dyed hair tress are prepared to compare the shine in hair. The compositions of Comparative Example and Example 4 above were used five times in each tress. 30 ℃, 40% relative humidity) was incubated in a constant temperature room for one day and completely dried. Dried hair is shown in FIG. 2. The hair was fixed to a gloss measurement device and the results of measuring the gloss are shown in Table 4 below as Luster Values.
염색모Dyed hair 비교예Comparative example 12.5812.58
실시예 4Example 4 14.8314.83
정상모Normal mother 비교예Comparative example 30.6930.69
실시예 4Example 4 39.5639.56
실험 결과, 비교예에 비해 실시예 4 처리 시에 염색모와 정상모 모두에서 Luster Value가 우수하였으며, 하기 도 2와 같이 실시예 4로 처리한 염색모와 정상모는 빛의 산란이 적고 모발 선명도가 우수하였으므로, 본원발명의 조성물을 사용 시 모발의 윤기가 증진됨을 확인하였다.As a result, the Luster Value was excellent in both the dyed hair and the normal hair during the treatment of Example 4 compared to the comparative example, and the dyed hair and the normal hair treated in Example 4 had less light scattering and excellent hair clarity as shown in FIG. When using the composition of the present invention it was confirmed that the gloss of the hair is enhanced.
[[ 시험예Test Example 3] 패널 테스트 3] panel testing
샴푸 전문 패널 7인을 대상으로 비교예와 실시예1 내지 4를 평소 샴푸를 사용하듯이 사용하도록 한 후 각 항목에 대하여 1-10점 사이의 점수를 매기도록 하였다.(1점 매우나쁨 - 5점 보통 - 10점 매우좋음) 7인의 점수를 평균하여 패널테스트 결과를 산출하였고, 각 평가 항목에 대한 결과를 표 5 및 도 3에 나타내었다.Seven comparative panel of shampoo specialists and Examples 1 to 4 were to be used as usual shampoo, and then scored between 1-10 points for each item. (1 point very bad-5 Point Average-10 points Very good) The panel test results were calculated by averaging the scores of 7 people, and the results for each evaluation item are shown in Table 5 and FIG. 3.
평가항목 Evaluation item 비교예 Comparative example 실시예1Example 1 실시예2Example 2 실시예3Example 3 실시예4Example 4
거품의양 Amount of foam 4.57          4.57 6.86          6.86 6.14          6.14 5.57          5.57 7.29          7.29
헹굼 시 부드러움  Soft when rinsing 3.71          3.71 4.00          4.00 7.29          7.29 6.86          6.86 8.14          8.14
젖은 상태에서의 부드러움  Softness in wet conditions 4.43          4.43 4.71          4.71 7.00          7.00 6.43          6.43 7.86          7.86
건조 후 부드러움  Softness after drying 4.14          4.14 4.86          4.86 6.57          6.57 6.71          6.71 8.00          8.00
모발 윤기 Hair shine 4.86          4.86 5.29          5.29 5.29          5.29 6.14          6.14 6.86          6.86
상기 페널 테스트 결과를 보면, 1)거품의 양에 있어서, 비교예에 비해 실시예 1 내지 4가 더 우수함을 확인할 수 있으며, 2)헹굼 시 부드러움, 젖은 상태에서의 부드러움 및 건조 후 부드러움에 있어서, 비교예에 비해 실시예 1 내지 4가 더 우수하였고, 3)모발 윤기에 있어서도 비교예에 비해 실시예 1 내지 4가 더 우수함을 확인할 수 있었다. 특히 실시예 4는 상기 평가 항목 모두에서 가장 우수함을 나타내었다.Looking at the results of the panel test, 1) in the amount of bubbles, it can be seen that Examples 1 to 4 are superior to the comparative example, 2) in rinsing, soft in wet and soft after drying, Examples 1 to 4 were superior to the comparative example, and 3) Examples 1 to 4 were superior to the comparative example even in hair shine. In particular, Example 4 showed the best in all of the above evaluation items.

Claims (11)

  1. 폴리쿼터늄-73(PQ-73)을 포함하는 투명 제형의 모발용 조성물.A composition for hair of a transparent formulation comprising polyquaternium-73 (PQ-73).
  2. 제 1항에 있어서,The method of claim 1,
    상기 조성물은 계면활성제를 더 포함하는 투명 제형의 모발용 조성물.The composition is a composition for hair of a transparent formulation further comprises a surfactant.
  3. 제 2항에 있어서,The method of claim 2,
    상기 계면활성제는 소듐 라우레스 설페이트(sodium laureth sulfate), 소듐 라우로일 살코시네이트(sodium lauroyl sarcosinate) 및 코카미도프로필 베타인(cocamidopropyl betaine)으로 이루어진 군에서 선택된 어느 하나 이상의 계면활성제인, 투명 제형의 모발용 조성물.The surfactant is any one or more surfactants selected from the group consisting of sodium laureth sulfate, sodium lauroyl sarcosinate and cocamidopropyl betaine, transparent formulation. Composition for hair.
  4. 제 1항에 있어서,The method of claim 1,
    상기 폴리쿼터늄-73은 전체 조성물에 대하여 0.01 내지 5 중량%인 투명 제형의 모발용 조성물.The polyquaternium-73 is a hair composition of the transparent formulation of 0.01 to 5% by weight based on the total composition.
  5. 제 3항에 있어서,The method of claim 3, wherein
    상기 계면 활성제는 전체 조성물에 대하여 0.1 내지 30 중량%인 투명 제형의 모발용 조성물.The surfactant is 0.1-30% by weight of the total composition of the composition for hair of the transparent formulation.
  6. 제 5항에 있어서,The method of claim 5,
    상기 계면 활성제는 전체 조성물에 대하여 10 내지 20 중량%인 투명 제형의 모발용 조성물.The surfactant is 10 to 20% by weight of the total composition of the composition for hair of the transparent formulation.
  7. 제 2항에 있어서,The method of claim 2,
    상기 폴리쿼터늄-73과 상기 계면활성제를 1:20 내지 40의 중량비로 포함하는, 투명 제형의 모발용 조성물.The polyquaternium-73 and the surfactant in a weight ratio of 1:20 to 40, the composition for hair of a transparent formulation.
  8. 제 3항에 있어서,The method of claim 3, wherein
    상기 계면 활성제는 소듐 라우레스 설페이트(sodium laureth sulfate), 코카미도프로필 베타인(cocamidopropyl betaine) 및 소듐 라우로일 살코시네이트(sodium lauroyl sarcosinate)를 포함하고, 전체 조성물에 대하여 상기 소듐 라우레스 설페이트는 5 내지 10중량%이며, 상기 코카미도프로필 베타인는 5 내지 10중량%이고, 상기 소듐 라우로일 살코시네이트는 0.1 내지 5중량%인, 투명 제형의 모발용 조성물.The surfactant includes sodium laureth sulfate, cocamidopropyl betaine, and sodium lauroyl sarcosinate, and the sodium laureth sulfate for the whole composition 5 to 10% by weight, the cocamidopropyl betaine is 5 to 10% by weight, the sodium lauroyl salcosinate is 0.1 to 5% by weight, the composition for hair of a transparent formulation.
  9. 제 3항에 있어서,The method of claim 3, wherein
    상기 계면 활성제는 소듐 라우레스 설페이트(sodium laureth sulfate), 코카미도프로필 베타인(cocamidopropyl betaine) 및 소듐 라우로일 살코시네이트(sodium lauroyl sarcosinate)를 포함하고, The surfactant includes sodium laureth sulfate, cocamidopropyl betaine, and sodium lauroyl sarcosinate,
    상기 폴리쿼터늄-73, 소듐 라우레스 설페이트, 코카미도프로필 베타인 및 소듐 라우로일 살코시네이트는 1 : 10 내지 20 : 10 내지 20 : 1 내지 7 의 중량비로 포함되는 투명 제형의 모발용 조성물.Wherein said polyquaternium-73, sodium laureth sulfate, cocamidopropyl betaine and sodium lauroyl salcosinate are included in a weight ratio of 1: 10 to 20: 10 to 20: 1 to 7.
  10. 제 9항에 있어서,The method of claim 9,
    상기 폴리쿼터늄-73, 소듐 라우레스 설페이트, 코카미도프로필 베타인 및 소듐 라우로일 살코시네이트는 1 : 12 내지 16 : 12 내지 16 : 3 내지 5 의 중량비로 포함되는 투명 제형의 모발용 조성물.The polyquaternium-73, sodium laureth sulfate, cocamidopropyl betaine and sodium lauroyl salcosinate is a composition for hair of a transparent formulation comprising a weight ratio of 1: 12 to 16: 12 to 16: 3 to 5.
  11. 제 1항 내지 제 10항 중 어느 한 항에 있어서,The method according to any one of claims 1 to 10,
    상기 투명 제형의 모발용 조성물은 모발 세정용 조성물.The composition for hair of the transparent formulation is a hair cleaning composition.
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CN112891240A (en) * 2021-02-05 2021-06-04 纳爱斯浙江科技有限公司 Composition with cleaning power, foam experience, low tooth wear and low irritation to oral mucosa
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US11291616B2 (en) 2015-04-23 2022-04-05 The Procter And Gamble Company Delivery of surfactant soluble anti-dandruff agent
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US11679073B2 (en) 2017-06-06 2023-06-20 The Procter & Gamble Company Hair compositions providing improved in-use wet feel
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US10912732B2 (en) 2017-12-20 2021-02-09 The Procter And Gamble Company Clear shampoo composition containing silicone polymers
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US11819474B2 (en) 2020-12-04 2023-11-21 The Procter & Gamble Company Hair care compositions comprising malodor reduction materials
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US11771635B2 (en) 2021-05-14 2023-10-03 The Procter & Gamble Company Shampoo composition

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