WO2017003129A1 - Composition cosmétique de maquillage comprenant une structure lamellaire - Google Patents

Composition cosmétique de maquillage comprenant une structure lamellaire Download PDF

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Publication number
WO2017003129A1
WO2017003129A1 PCT/KR2016/006681 KR2016006681W WO2017003129A1 WO 2017003129 A1 WO2017003129 A1 WO 2017003129A1 KR 2016006681 W KR2016006681 W KR 2016006681W WO 2017003129 A1 WO2017003129 A1 WO 2017003129A1
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Prior art keywords
ceramide
polyquaternium
oil
cosmetic composition
makeup cosmetic
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PCT/KR2016/006681
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English (en)
Korean (ko)
Inventor
강유진
김경남
최경호
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(주)아모레퍼시픽
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Priority to CN201680038423.XA priority Critical patent/CN107735073B/zh
Publication of WO2017003129A1 publication Critical patent/WO2017003129A1/fr
Priority to HK18108265.1A priority patent/HK1248553A1/zh

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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/68—Sphingolipids, e.g. ceramides, cerebrosides, gangliosides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin

Definitions

  • the present specification relates to a makeup cosmetic composition in which ceramide is stabilized using an inorganic powder surface-treated with a hydrophilic coating agent.
  • Ceramide occupies about 40% or more of the keratinocyte lipids constituting the stratum corneum of the skin and is an essential ingredient for the formation or function of the stratum corneum, and has excellent moisturizing effect and barrier function.
  • ceramides are poorly soluble and are used in small amounts in cosmetic formulations, and in this case, the particle size of the formulation is reduced and gelation occurs.
  • the encapsulated ceramide may be used due to the large amount of encapsulating agent, and thus the content of the encapsulating agent of the saccharide-based or polymer-based encapsulation may be impaired.
  • the multi-layer lamellar liquid crystal stabilizes the surface energy in the state of raising the particle size in advance to prevent gelation of the ceramide by the coalescence of the particles. At this time, if you put the powder for the makeup effect there was a problem that the particles become unstable.
  • Patent Document 1 KR10-2011-0093634 A
  • One aspect of the present invention is to provide an oil-in-water makeup cosmetic composition comprising a stable lamellar liquid crystal while preventing the gelation of ceramide.
  • One aspect of the present invention is an oil-in-water type makeup cosmetic composition
  • an oil-in-water type makeup cosmetic composition comprising an aqueous phase and an oil phase, wherein the composition includes an inorganic powder surface-treated with a hydrophilic coating agent dispersed in the aqueous phase, and includes a multi-layer lamellar structure containing ceramide.
  • the composition includes an inorganic powder surface-treated with a hydrophilic coating agent dispersed in the aqueous phase, and includes a multi-layer lamellar structure containing ceramide.
  • Another aspect of the present invention is to provide a method for preparing an oil-in-water type makeup cosmetic composition
  • an oil-in-water type makeup cosmetic composition comprising an inorganic powder surface-treated with a hydrophilic coating agent, a multi-layered ceramide lamella structure.
  • One aspect of the present invention is an oil-in-water type makeup cosmetic composition
  • an oil-in-water type makeup cosmetic composition comprising an aqueous phase and an oil phase, wherein the composition includes an inorganic powder surface-treated with a hydrophilic coating agent dispersed in the aqueous phase, and includes a multi-layer lamellar structure containing ceramide.
  • the hydrophilic coating agent provides an oil-in-water makeup cosmetic composition that is a hydrophilic coating agent comprising any one or more of silica and cellulose.
  • the multilayer lamellar structure provides an oil-in-water makeup cosmetic composition that is a multilayer lamellar structure containing a glucoside surfactant.
  • the glucoside surfactant may be at least one selected from the group consisting of behenyl alcohol, arachidyl alcohol, arachidyl glucoside, C14-22 alcohol and C12-20 alkyl glucoside.
  • the ceramide provides an oil-in-water makeup cosmetic composition of any one or more of natural ceramide and similar ceramides.
  • the natural ceramide provides ceramide 1, ceramide 2, ceramide 3, ceramide 4, ceramide 5, ceramide 6, ceramide 7 and ceramide 8 any one or more oil-in-water makeup cosmetic composition.
  • the pseudo ceramide provides an oil-in-water makeup cosmetic composition of at least one of the compounds represented by the following formula (1) to (6).
  • R is a saturated or unsaturated aliphatic chain of C9-C21.
  • n 1 or 2; R and R 'are saturated or unsaturated aliphatic chains of C9-C21.
  • n and n are the same or different and are an integer from 1 to 3;
  • k and l are the same or different and are 1 or 2;
  • j 0 or 1
  • R and R ' are the same or different and are C1-C31 straight or branched chain saturated or unsaturated alkyl groups, with or without hydroxy groups;
  • a 1 , A 2 and A 3 are the same or different and are hydrogen or any of substituents of the following structure, except that A 1 , A 2 and A 3 are simultaneously hydrogen:
  • M, M 1 and M 2 are alkali metal, lysine, arginine, histidine, triethanolamine, ammonia, polyquaternium-4, polyquaternium-6, polyquaternium-7, polyquaternium-10, Polyquaternium-11, polyquaternium-16, lauryldimethylbenzylammonium chloride and stearyldimethylbenzylammonium chloride, L is a calitometal.
  • R and R ' are the same or different and are C 10 -C 32 straight or branched chain saturated or unsaturated alkyl groups, with or without a hydroxy group;
  • R 3 and R 4 are the same or different and are hydrogen or a C1-C4 alkyl or hydroxyalkyl group
  • R 5 is -A or -CH 2 CH 2 OA, wherein A is any of substituents of the following structure.
  • M, M 1 and M 2 are alkali metal, lysine, arginine, histidine, triethanolamine, ammonia, polyquaternium-4, polyquaternium-6, polyquaternium-7, polyquaternium-10, Polyquaternium-11, polyquaternium-16, lauryldimethylbenzylammonium chloride and stearyldimethylbenzylammonium chloride, L is an alkaline earth metal.
  • n and n are the same or different and are integers from 1 to 4; R and R 'are the same or different and are straight or branched chain saturated or unsaturated alkyl groups of C1-C31, with or without hydroxy groups.
  • A1 and A2 are the same or different and are either hydrogen or a substituent of the following structure;
  • M, M 1 and M 2 are alkali metal, lysine, arginine, histidine, triethanolamine, ammonia, polyquaternium-4, polyquaternium-6, polyquaternium-7, polyquaternium-10, Polyquaternium-11, polyquaternium-16, lauryldimethylbenzylammonium chloride and stearyldimethylbenzylammonium chloride, L is an alkaline earth metal.
  • n and n are the same or different and are an integer from 1 to 3;
  • k and l are the same or different and are 1 or 2;
  • j 0 or 1
  • a 1 , A 2 and A 3 are the same or different and are either hydrogen or a substituent of the following structure;
  • M. M 1 and M 2 are an alkali metal or an organic base containing nitrogen and L is an alkaline earth metal];
  • R is a substituent having the structure:
  • the inorganic powder surface-treated with the hydrophilic coating agent provides an oil-in-water makeup cosmetic composition is an inorganic powder containing any one or more of titanium oxide surface-treated with a hydrophilic coating agent and iron oxide surface-treated with a hydrophilic coating agent. do.
  • the inorganic powder surface-treated with the hydrophilic coating agent provides an oil-in-water makeup cosmetic composition of 0.01 to 25% by weight based on the total weight of the composition.
  • the ceramide provides an oil-in-water makeup cosmetic composition containing 0.01 to 20% by weight based on the total weight of the composition.
  • the size of the lamellar structure provides an oil-in-water makeup cosmetic composition is 2 ⁇ m to 30 ⁇ m.
  • Another aspect of the present invention is to prepare an oil phase comprising a ceramide and a glucoside surfactant; Mixing and dispersing the inorganic powder surface-treated with a hydrophilic coating agent in an aqueous phase; Mixing the prepared oil phase and the aqueous phase to prepare a mixture; It provides a method for producing an oil-in-water makeup cosmetic composition comprising; and leaving the mixture at 45 °C to 60 °C.
  • preparing an oil phase comprising a ceramide and a glucoside surfactant; Preparing an aqueous phase; Mixing the prepared oil phase and the aqueous phase to prepare a mixture; Leaving the mixture at 45 ° C. to 60 ° C .; And mixing and dispersing the inorganic powder surface-treated with a hydrophilic coating agent to the mixture.
  • Makeup cosmetic composition according to one aspect of the present invention is excellent in formulation stability.
  • Makeup cosmetic composition according to an aspect of the present invention comprises a stable ceramide lamella liquid crystal and at the same time contains an inorganic powder.
  • Makeup cosmetic composition according to one aspect of the present invention has excellent moisturizing power when applied to the skin.
  • Makeup cosmetic composition according to one aspect of the present invention has a barrier function recovery effect when applied to the skin.
  • Makeup cosmetic composition according to an aspect of the present invention has an excellent effect on improving the dry skin when applied to the skin.
  • One aspect of the present invention is an oil-in-water type makeup cosmetic composition
  • an oil-in-water type makeup cosmetic composition comprising an aqueous phase and an oil phase, wherein the composition includes an inorganic powder surface-treated with a hydrophilic coating agent dispersed in the aqueous phase, and includes a multi-layer lamellar structure containing ceramide.
  • the hydrophilic coating agent to the multi-layered ceramide lamella structure comprising a glucoside surfactant to produce a makeup cosmetic composition having excellent moisture retention and barrier function recovery effect hydrophilic coating agent comprising any one or more of silica and cellulose It characterized in that to use.
  • the silica and cellulose may be prepared by a conventional method, but if it does not depart from the scope of the present invention, it will be apparent to those skilled in the art that the scope of the silica is not limited. will be.
  • the ratio of the coating agent in the inorganic powder surface-treated with the hydrophilic coating agent may be an oil-in-water makeup cosmetic composition of 2 to 15% by weight.
  • the ratio of the coating agent in the inorganic powder surface-treated with the hydrophilic coating agent is 2% by weight, 3% by weight, 4% by weight, 5% by weight, 6% by weight, 7% by weight, 8% by weight More than 9% by weight or more than 10% by weight.
  • the proportion of the coating agent in the inorganic powder surface-treated with the hydrophilic coating agent is 12% by weight, 11% by weight, 10% by weight, 9% by weight, 8% by weight, 7% by weight, 6% by weight or less It may be up to 5% by weight, up to 4% by weight or up to 3% by weight.
  • the makeup cosmetic composition may contain a stable ceramide lamellar liquid crystal and at the same time contain an inorganic powder.
  • the coating agent when the coating agent is a silica coating, the titanium oxide and yellow iron oxide in the inorganic powder may be a coating ratio of 8 to 12% by weight, the red or black iron oxide may be a coating ratio of 10 to 15% by weight. have.
  • the coating agent is a cellulose coating
  • the titanium oxide, iron oxide yellow, red or black iron oxide may be a coating ratio of 2 to 8% by weight.
  • the multilayer lamellar structure provides an oil-in-water makeup cosmetic composition that is a multilayer lamellar structure containing a glucoside surfactant.
  • the glucoside surfactant may be at least one selected from the group consisting of behenyl alcohol, arachidyl alcohol, arachidyl glucoside, C14-22 alcohol and C12-20 alkyl glucoside.
  • the multilayer ceramide lamella structure used in the present invention may further include a wax or oil.
  • the wax may be one or more selected from the group consisting of alcohols, fatty acids, vegetable waxes, synthetic waxes, ozokerite, cetyl palmitate, bees waxes, lipids and lipid peptides.
  • the oil may be an ester oil, hydrocarbon oil or silicone oil.
  • the ceramide provides a makeup cosmetic composition is any one or more of natural ceramide and similar ceramides.
  • the ceramide used in the present invention may be any one or more of natural ceramide and similar ceramides.
  • the natural ceramide is a natural ceramide, ceramide 1, ceramide 2, ceramide 3, ceramide 4, ceramide 5, ceramide 6, ceramide 7, ceramide 8 and the like
  • the pseudo ceramide is a ceramide 104 and ceramide And 102.
  • Analogous ceramide in the present invention collectively refers to a compound having a double-chain lamellar structure, which is the structure of natural ceramide.
  • the lamellar structure prevents gelation of pseudoceramide at the outer shell, and when the macro-emulsion is formed surrounded by a multi-lamellar layer in which the lamellar structure forms a multilayer of two or more layers, the ceramide of the ceramide is formed. It contributes to stabilization and can realize excellent slipping property and light usability.
  • Rod type SAAs including ceramides, are generally known to be more stable with smaller curvature and larger radius of curvature. Therefore, macroemulsions with small curvatures are more stable than emulsions of small particle sizes with large curvatures.
  • the pseudo ceramide provides an oil-in-water makeup cosmetic composition of at least one of the compounds represented by the following formula (1) to (6).
  • R is a saturated or unsaturated aliphatic chain of C9-C21.
  • n 1 or 2; R and R 'are saturated or unsaturated aliphatic chains of C9-C21.
  • n and n are the same or different and are an integer from 1 to 3;
  • k and l are the same or different and are 1 or 2;
  • j 0 or 1
  • R and R ' are the same or different and are C1-C31 straight or branched chain saturated or unsaturated alkyl groups, with or without hydroxy groups;
  • a 1 , A 2 and A 3 are the same or different and are hydrogen or any of substituents of the following structure, except that A 1 , A 2 and A 3 are simultaneously hydrogen:
  • M, M 1 and M 2 are alkali metal, lysine, arginine, histidine, triethanolamine, ammonia, polyquaternium-4, polyquaternium-6, polyquaternium-7, polyquaternium-10, Polyquaternium-11, polyquaternium-16, lauryldimethylbenzylammonium chloride and stearyldimethylbenzylammonium chloride, L is a calitometal.
  • R and R ' are the same or different and are C 10 -C 32 straight or branched chain saturated or unsaturated alkyl groups, with or without a hydroxy group;
  • R 3 and R 4 are the same or different and are hydrogen or a C1-C4 alkyl or hydroxyalkyl group
  • R 5 is -A or -CH 2 CH 2 OA, wherein A is any of substituents of the following structure.
  • M, M 1 and M 2 are alkali metal, lysine, arginine, histidine, triethanolamine, ammonia, polyquaternium-4, polyquaternium-6, polyquaternium-7, polyquaternium-10, Polyquaternium-11, polyquaternium-16, lauryldimethylbenzylammonium chloride and stearyldimethylbenzylammonium chloride, L is an alkaline earth metal.
  • n and n are the same or different and are integers from 1 to 4; R and R 'are the same or different and are straight or branched chain saturated or unsaturated alkyl groups of C1-C31, with or without hydroxy groups.
  • A1 and A2 are the same or different and are either hydrogen or a substituent of the following structure;
  • M, M 1 and M 2 are alkali metal, lysine, arginine, histidine, triethanolamine, ammonia, polyquaternium-4, polyquaternium-6, polyquaternium-7, polyquaternium-10, Polyquaternium-11, polyquaternium-16, lauryldimethylbenzylammonium chloride and stearyldimethylbenzylammonium chloride, L is an alkaline earth metal.
  • n and n are the same or different and are an integer from 1 to 3;
  • k and l are the same or different and are 1 or 2;
  • j 0 or 1
  • a 1 , A 2 and A 3 are the same or different and are either hydrogen or a substituent of the following structure;
  • M. M 1 and M 2 are an alkali metal or an organic base containing nitrogen and L is an alkaline earth metal];
  • R is a substituent having the structure:
  • the compounds of Formulas 1 to 6 are pseudoceramides having an excellent effect on skin moisturizing and skin barrier function recovery.
  • the multilayer ceramide lamellar structure refers to a macroemulsion, and preferably, the average particle size of the multilayer ceramide lamellar structure, ie, the multilayer lamella liquid crystal, may be 2 ⁇ m to 30 ⁇ m.
  • the average particle size of the multilayer lamellar liquid crystal is 2 ⁇ m or more, 3 ⁇ m or more, 4 ⁇ m or more, 5 ⁇ m or more, 6 ⁇ m or more, 7 ⁇ m or more, 8 ⁇ m or more, 9 ⁇ m or more, 10 ⁇ m or more, or 11 ⁇ m or more.
  • the average particle size of the multilayer lamellar liquid crystal is 30 ⁇ m, 29 ⁇ m, 28 ⁇ m, 27 ⁇ m, 26 ⁇ m, 25 ⁇ m, 24 ⁇ m, 23 ⁇ m, 22 ⁇ m, 21 ⁇ m or less. 20 ⁇ m, 19 ⁇ m, 18 ⁇ m, 17 ⁇ m, 16 ⁇ m, or 15 ⁇ m.
  • the average particle size of the multilayer ceramide lamellar structure is formed to be 2 ⁇ m or more, it may lead to stabilization of pseudoceramide, and it may be possible to realize a special point of usability and to improve moisture retention.
  • the average particle size exceeds 30 mu m, the stability is deteriorated, so it is preferable to maintain the above range.
  • the inorganic powder surface-treated with the hydrophilic coating agent provides a makeup cosmetic composition is an inorganic powder comprising any one or more of titanium oxide surface-treated with a hydrophilic coating agent and iron oxide surface-treated with a hydrophilic coating agent.
  • the inorganic powder surface-treated with the hydrophilic coating agent provides a makeup cosmetic composition of 0.01 to 25% by weight based on the total weight of the composition.
  • the inorganic powder surface-treated with the hydrophilic coating agent is 0.01% by weight, 0.5% by weight, 1% by weight, 2% by weight, 3% by weight, 4% by weight, 5% by weight based on the total weight of the composition Or more, 6 or more, 7 or more, 8 or more, 9 or more, 10 or more, 11 or more, 12 or more, 13 or more, 14 or more, 15 or more Or at least 16%, at least 17%, at least 18%, at least 19%, at least 20%, or at least 21% by weight.
  • the inorganic powder surface-treated with the hydrophilic coating agent is 25% by weight, 24% by weight, 23% by weight, 22% by weight, 21% by weight, 20% by weight, 19% by weight with respect to the total weight of the composition Up to 18 weight percent, up to 17 weight percent, up to 16 weight percent, up to 15 weight percent, up to 14 weight percent, up to 13 weight percent, up to 12 weight percent and up to 11 weight percent.
  • the coverage is excellent, and does not deviate from the blending limit of titanium oxide, and the color is not too dark or light.
  • the inorganic pigment surface-treated with the silica or cellulose of the present invention can be prepared by a method known in the art, the method is not particularly limited. Generally, after dispersing the inorganic pigment, a precursor (for example, tetraethoxysilane, etc.) capable of forming silica is added to the inorganic pigment surface by hydrolysis by heat treatment for 1 to 6 hours at a temperature of 50 to 400 ° C. It can be treated with silica.
  • a precursor for example, tetraethoxysilane, etc.
  • the inorganic pigments include titanium oxide, yellow, red and black iron oxide, but are not limited thereto.
  • titanium oxide surface treated with silica or cellulose and yellow, red and black iron oxides can be used.
  • the particle size is preferably 400 to 600 nm, and preferably 0.5 to 25 wt% based on the total weight of the composition so as to give a covering power. If the content is less than 0.5% by weight, the coverage does not appear properly, and when the content exceeds 25% by weight, the compounding limit of titanium oxide is exceeded.
  • the content is determined according to the color, and the sum is preferably contained in an amount of 0.01 to 10% by weight based on the total weight of the composition. If used in less than 0.01% by weight, the desired color is not implemented properly, if it exceeds 10% by weight the color is too dark to be suitable as a makeup composition.
  • the ceramide provides a makeup cosmetic composition containing 0.01 to 20% by weight based on the total weight of the composition.
  • the ceramide is 0.01% by weight, 0.5% by weight, 1% by weight, 2% by weight, 3% by weight, 4% by weight, 5% by weight, 6% by weight based on the total weight of the composition 7% by weight, 8% by weight, 9% by weight, 10% by weight, 11% by weight, 12% by weight, 13% by weight, 14% by weight, 15% by weight, 16% by weight Or 17% by weight or more.
  • the ceramide is 20% by weight, 19% by weight, 18% by weight, 17% by weight, 16% by weight, 15% by weight, 14% by weight, 13% by weight or less based on the total weight of the composition. It may be up to 12% by weight and up to 11% by weight.
  • the content of ceramide is in the above range, when the composition is applied to the skin, the skin moisturizing ability is excellent, and it is possible to improve dry skin.
  • Another aspect of the present invention is to prepare an oil phase comprising a ceramide and a glucoside surfactant; Mixing and dispersing the inorganic powder surface-treated with a hydrophilic coating agent in an aqueous phase; Mixing the prepared oil phase and the aqueous phase to prepare a mixture; And leaving the mixture at 45 ° C. to 60 ° C .; It provides a method for producing an oil-in-water makeup cosmetic composition comprising a.
  • preparing an oil phase comprising a ceramide and a glucoside surfactant; Preparing an aqueous phase; Mixing the prepared oil phase and the aqueous phase to prepare a mixture; Leaving the mixture at 45 ° C. to 60 ° C .; And mixing and dispersing the inorganic powder surface-treated with a hydrophilic coating agent to the mixture.
  • the step of leaving the mixture plays an important role in forming the lamellae structure.
  • the temperature of the leaving step may be 45 ° C., 46 ° C., 47 ° C., 48 ° C., 49 ° C., 50 ° C., 51 ° C., 52 ° C., 53 ° C., or 54 ° C. or more. have.
  • the temperature of the leaving step is 60 °C or less, 59 °C or less, 58 °C or less, 57 °C or less, 56 °C or less, 55 °C or less, 54 °C or less, 53 °C or less, 52 °C or less, 51 °C or less or 50 It may be below °C.
  • the lamellar structure is formed stably.
  • the leaving step is at least 20 minutes, at least 25 minutes, at least 30 minutes, at least 35 minutes, at least 40 minutes, at least 50 minutes, at least 60 minutes, at least 70 minutes, at least 80 minutes or at least 100 minutes. It may be abnormal.
  • the lamellar structure is formed stably.
  • the hydrophilic coating agent provides a method comprising any one or more of silica and cellulose.
  • the glucoside surfactant provides a method of at least one selected from the group consisting of behenyl alcohol, arachidyl alcohol, arachidyl glucoside, C14-22 alcohol and C12-20 alkylglucoside.
  • the makeup cosmetic composition according to the present invention may be formulated with an oil-in-water makeup base or foundation containing a pigment, but is not limited thereto.
  • Examples 1,2 and Comparative Examples 1,2 were prepared using the compositions shown in Table 1 below.
  • Alkylsilane using Daito Kasei's OTS series, all 2% coated
  • silica using the Sympholight series from JGC Catalysts and Chemicals Ltd., titanium oxide and yellow iron oxide 10% coating, red / black iron oxide 12% coating
  • cellulose Inorganic powders surface-treated with Daito Kasei's C2 series, all 5% coated were purchased from commercially available products.
  • Example 2 Oily ingredient Butylene Glycol Dicaprylate / Dicaprate 4.00 4.00 4.00 4.00 Hydroxypropyl bisuraramide MB (Pc104) 0.70 0.70 0.70 0.70 Hydroxypropyl bispalmitamide MA (Pc102) 0.80 0.80 0.80 0.80 cholesterol 0.50 0.50 0.50 0.50 0.50 Stearic acid 1.50 1.50 1.50 1.50 Behenyl Alcohol 2.00 2.00 2.00 2.00 Behenyl alcohol, arachidyl alcohol, arachidyl glucoside 1.00 1.00 1.00 C14-22 alcohol, C12-20 alkylglucoside 1.00 1.00 1.00 1.00 1.00 Pentaerythritol tetraisostearate 3.00 3.00 3.00 3.00 3.00 Cetylethylhexanoate 2.00 2.00 2.00 2.00 Squalane 2.00 2.00 2.00 2.00 Cyclopentasiloxane 5.00 5.00 5.00 coloring agent Titanium oxide 4.25
  • An oily solution was prepared at 75 ° C. according to the composition ratio of Table 1.
  • pseudo ceramides it was intended to include hydroxypropylbispalmitamide M (Pc104) and hydroxypropylbispalmitamide M (AcP102).
  • step 1) The oily solution of step 1) was added to the aqueous solution of step 2) and mixed by stirring with a homomixer.
  • step 1) The oily solution of step 1) was added to the aqueous solution of step 2) and mixed by stirring with a homomixer.
  • the cooling temperature was maintained at about 52 ° C. for about 35 minutes, and then the colorant was mixed and dispersed.
  • Example 1-4 and Comparative Example 1-5 were each taken in 10g each, 4 ° C. low temperature thermostat, 30 ° C. thermostat, 45 ° C. high temperature thermostat, -10 ° C. to After placing the samples in a cycle chamber circulating at 45 °C for 24 hours, the stability of the formulation was observed by observing changes in the formulations, and the results are shown in Tables 3 and 4 below.
  • Comparative Example 1 was confirmed that the emulsion is not stable because the multilayer lamellar structure is broken by the uncoated (untreated) inorganic powder, it was confirmed that the stability is poor, coated with a hydrophobic alkylsilane In Comparative Example 2, the formulation itself was not formed while developing in preparation. In Examples 1 and 2 coated with hydrophilic cellulose and silica, multilayer lamellar liquid crystals having a particle size of 2 ⁇ m or more were formed, but showed an unstable appearance at 45 ° C. long term stability.
  • Table 4 shows the results of dispersing the pigments by type after making the multilayer lamellar liquid crystal by maintaining the manufacturing method at about 52 ° C. for about 35 minutes.
  • Comparative Example 3 the multilayer lamellar structure formed by the inorganic powder without surface treatment was broken, and the particle size was too small, resulting in gelation at 45 ° C., thereby degrading its value as a product.
  • Comparative Example 4 an inorganic powder coated with a hydrophobic alkylsilane was added after the oil-in-water emulsification was prepared, so that dispersion was not uniform.
  • Comparative Example 5 was stable without gelation because no ceramide was contained.
  • the makeup cosmetic composition of Examples 3, 4 and Comparative Example 5 was applied to 80 adult men and women in their 30s and 40s who complain of dryness or dry skin.
  • the moisture content of the skin was measured using a corneometer (CM820 courage Khazaka electronic GmbH, Germany) for 24 hours.
  • the skin moisture content was measured in advance using a conniometer at constant temperature and humidity conditions (24 ° C., 40% humidity) as the basic value, and immediately after application, the change after 2 hours, 4 hours, and 8 hours was measured. The results are shown in Table 5 below.
  • Moisture is measured by measuring the amount of moisture in the skin's epidermis using a sensor and quantifying the amount of moisture.
  • test subjects were surveyed about the effect of improving the dry skin after using each makeup cosmetic composition, and the average value of the evaluated values (five-point scale) is shown in Table 6 below.

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  • Cosmetics (AREA)

Abstract

La présente invention concerne une composition cosmétique de maquillage dans une forme d'huile-dans-eau comprenant une phase aqueuse et une phase huileuse, la composition cosmétique de maquillage d'huile-dans-eau comprenant une poudre inorganique dispersée dans la phase aqueuse et traitée en surface avec un agent de revêtement hydrophile et comprenant également une structure lamellaire multicouche comprenant des céramides. La composition cosmétique de maquillage selon un aspect de la présente invention a une excellente stabilité de formulation et hydrate parfaitement la peau lorsqu'elle est appliquée sur cette dernière.
PCT/KR2016/006681 2015-06-30 2016-06-23 Composition cosmétique de maquillage comprenant une structure lamellaire WO2017003129A1 (fr)

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CN201680038423.XA CN107735073B (zh) 2015-06-30 2016-06-23 包含层状结构的化妆用化妆品组合物
HK18108265.1A HK1248553A1 (zh) 2015-06-30 2018-06-27 包含層狀結構的化妝用化妝品組合物

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KR1020150093317A KR102418097B1 (ko) 2015-06-30 2015-06-30 라멜라 구조체를 포함하는 메이크업 화장료 조성물

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KR102453889B1 (ko) * 2017-09-29 2022-10-11 (주)아모레퍼시픽 에멀젼 화장료 조성물
JP2020026401A (ja) * 2018-08-10 2020-02-20 株式会社 資生堂 多層化粧料
CN109010083B (zh) * 2018-09-07 2021-11-02 广州华玺生物科技有限公司 一种具有两亲物质构成的层状结构体的二氧化碳复合面膜组合物及其制备方法
KR102576017B1 (ko) * 2021-10-07 2023-09-07 성균관대학교산학협력단 수분산성 세라마이드 파티클, 이의 제조방법, 및 이를 포함하는 에멀젼 조성물

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CN107735073B (zh) 2021-03-05
TW201713303A (zh) 2017-04-16
KR102418097B1 (ko) 2022-07-08
TWI701051B (zh) 2020-08-11
CN107735073A (zh) 2018-02-23
KR20170003097A (ko) 2017-01-09
HK1248553A1 (zh) 2018-10-19

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