WO2016107294A1 - Method for filling through hole by electroplating - Google Patents

Method for filling through hole by electroplating Download PDF

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Publication number
WO2016107294A1
WO2016107294A1 PCT/CN2015/094365 CN2015094365W WO2016107294A1 WO 2016107294 A1 WO2016107294 A1 WO 2016107294A1 CN 2015094365 W CN2015094365 W CN 2015094365W WO 2016107294 A1 WO2016107294 A1 WO 2016107294A1
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Prior art keywords
plating
asd
plated
current density
hole
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PCT/CN2015/094365
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French (fr)
Chinese (zh)
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谢添华
崔正丹
李志东
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广州兴森快捷电路科技有限公司
深圳市兴森快捷电路科技股份有限公司
宜兴硅谷电子科技有限公司
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Publication of WO2016107294A1 publication Critical patent/WO2016107294A1/en

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    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25DPROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D5/00Electroplating characterised by the process; Pretreatment or after-treatment of workpieces
    • C25D5/08Electroplating with moving electrolyte e.g. jet electroplating
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25DPROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D7/00Electroplating characterised by the article coated
    • HELECTRICITY
    • H05ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05KPRINTED CIRCUITS; CASINGS OR CONSTRUCTIONAL DETAILS OF ELECTRIC APPARATUS; MANUFACTURE OF ASSEMBLAGES OF ELECTRICAL COMPONENTS
    • H05K3/00Apparatus or processes for manufacturing printed circuits
    • H05K3/40Forming printed elements for providing electric connections to or between printed circuits
    • H05K3/42Plated through-holes or plated via connections

Definitions

  • This invention relates to electroplating techniques, and more particularly to a method of electroplating filled vias.
  • the through holes are usually filled by the plating through hole technology.
  • the electroplating apparatus comprises a plating tank, a plating solution, a power source, an anode, a plating solution is arranged in the plating tank, an anode is connected to the anode of the power source, and the anode is placed in the plating solution of the plating tank.
  • the electroplating apparatus is usually also provided with a jetting device connected to the plating tank, and the jetting device is provided with a nozzle, and the nozzle is provided with a nozzle.
  • the jetting device draws in the plating solution in the plating bath and ejects it from the nozzle into the plating bath to drive the plating solution to flow in the plating bath.
  • the member to be plated with the through hole is used as a cathode, connected to the negative electrode of the power source, and then the member to be plated with the through hole is placed in the plating solution of the plating bath.
  • the power supply is then controlled to supply power to the anode and cathode, and electroplating is performed at a constant current density for a constant time to complete the fill via.
  • the filling method is performed according to the current plating filling hole method. Hole, plating time should be 70-80min.
  • a method of plating a through hole comprising the steps of:
  • the electroplating device comprises a plating tank, a plating solution, a power source, an anode, a plating solution is arranged in the plating tank, an anode is connected to the anode of the power source, and the anode is placed in the plating solution of the plating tank;
  • control conditions are:
  • the current density J1 of the member to be plated is 2-3 ASD, 30% ⁇ T1/T ⁇ 50%,
  • the current density J2 of the parts to be plated is 0.5-1.5 ASD, 20% ⁇ T1/T ⁇ 40%,
  • the electroplating apparatus in step 1) further comprises a jetting device connected to the electroplating tank, the jetting device being provided with a nozzle located in the electroplating tank;
  • Step 3) Specifically, controlling the power supply operation according to the control condition and controlling the jet flow device to perform the side jet flow, and performing continuous plating for T time;
  • the control condition is:
  • the current density J1 of the material to be plated is 2-3 ASD
  • the nozzle flow rate q1 is 1.5-2 L/min, 30% ⁇ T1/T ⁇ 50%;
  • the current density J2 of the material to be plated is 0.5-1.5 ASD
  • the nozzle flow rate q2 is 3-5 L/min, 20% ⁇ T1/T ⁇ 40%
  • the current density J3 of the parts to be plated is 1.0-2.0 ASD
  • the nozzle flow rate q3 is 2-3 L/min
  • T3 T-T1-T2
  • the method of the present invention controls the power supply operation to perform electroplating correspondingly in the three stages of the electroplating process in accordance with the current density of the material to be plated.
  • the method of the present invention has the following good effects compared to the existing method: The same through-hole filling effect is achieved, and the plating time is small; the plating time is the same, and the through-hole filling effect is good. Therefore, the present invention can relatively reduce the filling time of the through holes, which is advantageous for improving production efficiency.
  • the method of the present invention cooperates with the operation of controlling the jet flow device in the case of controlling the operation of the power source, so that the through hole filling effect is further improved.
  • Figure 1 is a schematic view showing the structure of a plating apparatus for carrying out the method of the present invention.
  • a method of plating a through hole comprising the steps of:
  • an electroplating apparatus As shown in FIG. 1 , an electroplating apparatus is used.
  • the electroplating apparatus includes a plating tank 1, a plating solution 2, a power source 3, and an anode 4.
  • the plating tank 1 is provided with a plating solution 2, the anode 4 is connected to the anode of the power source 5, and the anode 4 is placed.
  • the member to be plated 6 with the through hole 61 is connected as a cathode to the power source 5, and the plate to be plated 6 forms a circuit with the power source 5 and the anode 4 under the action of the plating solution.
  • control conditions are:
  • the current density J1 of the member to be plated 6 is 2-3 ASD, 30% ⁇ T1/T ⁇ 50%,
  • the current density J2 of the member to be plated 6 is 0.5-1.5 ASD, 20% ⁇ T1/T ⁇ 40%,
  • step 3 the adjustment of the current density of the member to be plated 6 is achieved by controlling the output value of the power source.
  • the time required for electroplating under the same conditions is different; for the same piece to be plated, Different via fill effects are reached, and the time required to perform the plating under the same conditions is also different.
  • the size of the time T of continuous plating in the method needs to be determined in consideration of the final required through-hole filling effect.
  • the technical core of the method is to control the power supply 3 to perform electroplating according to the current density of the material to be plated 6 in three successive stages of the electroplating process. After testing, the method has the following advantages compared with the existing method. Effect: achieve the same through hole filling effect, less plating time; plating time phase Similarly, the through hole filling effect is good.
  • the through holes of the same size (the aperture is 80 ⁇ m and the hole depth is 100 ⁇ m) are plated and filled according to different methods.
  • the test results are shown in Table 1.
  • the method of the present invention has a shorter plating time and a higher filling effect of the through holes than the prior art.
  • This embodiment is based on the first embodiment, and cooperates with the control of the jet flow device during the electroplating process.
  • a method of plating a through hole comprising the steps of:
  • an electroplating apparatus is used.
  • the electroplating apparatus includes a plating tank 1, a plating solution 2, a power source 3, an anode 4, and a jetting device 5.
  • the plating tank 1 is provided with a plating solution 2, a jetting device 5 and plating.
  • the tank 1 is connected, the nozzle device 5 is provided with a nozzle 51 located in the plating tank 1, the anode 4 is connected to the anode of the power source 5, and the anode 4 is placed in the plating solution 2 of the plating tank 1;
  • the jet flow device 5 sucks the plating solution 2 in the plating tank 1 and ejects it from the nozzle 51 into the plating tank 1 to drive the plating solution 2 to flow in the plating tank 1, so that the plating solution 2 is more uniform.
  • control conditions are:
  • the current density J1 of the member to be plated 6 is 2-3 ASD
  • the nozzle flow rate q1 is 1.5-2 L/min
  • the current density J2 of the member to be plated 6 is 0.5-1.5 ASD
  • the nozzle flow rate q2 is 3-5 L L/min, 20% ⁇ T1/T ⁇ 40%
  • the current density J3 of the member to be plated 6 is 1.0-2.0 ASD
  • the nozzle flow rate q3 is 2-3 L/min
  • T3 T-T1-T2
  • the nozzle flow rate refers to the flow rate of the nozzle in unit time, and the unit is L/min.
  • the side jet means that the spray direction of the nozzle is perpendicular to the plate surface of the member to be plated, that is, the hole axis which is balanced with the through hole of the member to be plated.
  • the method is based on the first embodiment, in combination with the operation of controlling the jet flow device during the electroplating process, using different nozzle flow rates in the three electroplating stages, and the effect of the method is tested in the effect of the first embodiment method. On the basis of this, there is further improvement.
  • the through holes of the same size (pore size 80 ⁇ m, hole depth 100 ⁇ m) were electroplated and filled according to the method of the present invention, and the test results are shown in Table 2.

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Printing Elements For Providing Electric Connections Between Printed Circuits (AREA)
  • Electroplating Methods And Accessories (AREA)

Abstract

A method for filling a through hole by electroplating. The method comprises the following steps: 1) using an electroplating device; 2) connecting a to-be-electroplated piece that has a through hole to the negative electrode of a power source, and placing the piece into an electroplating solution in an electroplating bath; 3) controlling the power source to work according to a control condition, and continuously electroplating the piece for T time, wherein T>0, the control condition is that: within an initial stage T1 period, a current density J1 of the to-be-electroplated piece ranges from 2 ASD to 3 ASD, and 30%≤T1/T≤50%; in a mid-term stage T2 period, a current density J2 of the to-be-electroplated piece ranges from 0.5 ASD to 1.5 ASD, and 20%≤T2/T≤40%; and in a terminal stage T3 period, a current density J3 of the to-be-electroplated piece ranges from 1.0 ASD to 2.0 ASD, T3=T-T1-T2,and J1>J3>J2. The method can relatively reduce time used for filling a through hole and helps to improve the production efficiency.

Description

一种电镀填通孔的方法Method for plating through holes 技术领域Technical field
本发明涉及电镀技术,特别是涉及一种电镀填通孔的方法。This invention relates to electroplating techniques, and more particularly to a method of electroplating filled vias.
背景技术Background technique
印制线路板的制造过程中,需要对印制线路板上的通孔进行填充;目前来说,多是采用电镀填通孔技术进行填充通孔。In the manufacturing process of printed circuit boards, it is necessary to fill the through holes on the printed circuit board; at present, the through holes are usually filled by the plating through hole technology.
通常,电镀装置包括电镀槽、电镀溶液、电源、阳极,电镀槽中装有电镀溶液,阳极连接电源的正极,阳极置于电镀槽的电镀溶液中。电镀装置通常也设有与电镀槽连接的喷流装置,喷流装置设有喷管,喷管上设有喷嘴。喷流装置将电镀槽中的电镀溶液吸入再由喷嘴喷出到电镀槽中,以驱使电镀溶液在电镀槽中流动。Generally, the electroplating apparatus comprises a plating tank, a plating solution, a power source, an anode, a plating solution is arranged in the plating tank, an anode is connected to the anode of the power source, and the anode is placed in the plating solution of the plating tank. The electroplating apparatus is usually also provided with a jetting device connected to the plating tank, and the jetting device is provided with a nozzle, and the nozzle is provided with a nozzle. The jetting device draws in the plating solution in the plating bath and ejects it from the nozzle into the plating bath to drive the plating solution to flow in the plating bath.
目前,使用上述电镀装置进行电镀填通孔时,将带有通孔的待镀件作为阴极,连接到电源的负极,然后将带有通孔的待镀件置入电镀槽的电镀溶液中,然后控制电源给阳极和阴极供电,并以恒定的电流密度、恒定时间进行电镀,完成填充通孔。例如,对于孔径为80-100μm、孔深为100-150μm的通孔,在达到一定的填充效果(孔口凹陷值为16-22μm)的前提下,按目前的电镀填通孔方法进行填充通孔,电镀时间都要在70-80min。At present, when the plating device is used to fill the through hole, the member to be plated with the through hole is used as a cathode, connected to the negative electrode of the power source, and then the member to be plated with the through hole is placed in the plating solution of the plating bath. The power supply is then controlled to supply power to the anode and cathode, and electroplating is performed at a constant current density for a constant time to complete the fill via. For example, for a via hole having a hole diameter of 80-100 μm and a hole depth of 100-150 μm, under the premise of achieving a certain filling effect (the hole recess value is 16-22 μm), the filling method is performed according to the current plating filling hole method. Hole, plating time should be 70-80min.
但目前的电镀填通孔方法所需的电镀时间相对较长,导致降低生产效率。However, the current plating fill-through method requires a relatively long plating time, resulting in reduced production efficiency.
发明内容Summary of the invention
基于此,有必要针对目前电镀填通孔的时间较长的问题,提供一种电镀填通孔的方法,能相对降低通孔的填充时间,利于提高生产效率。Based on this, it is necessary to provide a method for plating the through-holes for the problem of long time for plating the through-holes, which can relatively reduce the filling time of the through-holes, and is advantageous for improving production efficiency.
一种电镀填通孔的方法,包括以下步骤:A method of plating a through hole, comprising the steps of:
1)采用电镀装置,电镀装置包括电镀槽、电镀溶液、电源、阳极,电镀槽中装有电镀溶液,阳极连接电源的正极,阳极置于电镀槽的电镀溶液中;1) using an electroplating device, the electroplating device comprises a plating tank, a plating solution, a power source, an anode, a plating solution is arranged in the plating tank, an anode is connected to the anode of the power source, and the anode is placed in the plating solution of the plating tank;
2)将带有通孔的待镀件与所述电源的负极连接,并置于电镀槽的电镀溶液 中;2) connecting the member to be plated with the through hole to the negative electrode of the power source, and placing the plating solution in the plating bath in;
3)按控制条件控制电源工作,进行T时间的连续电镀,T>0;所述控制条件为:3) Control the power supply according to the control conditions, and perform continuous plating at T time, T>0; the control conditions are:
在初始阶段T1时间内,待镀件的电流密度J1为2-3ASD,30%≤T1/T≤50%,In the initial stage T1, the current density J1 of the member to be plated is 2-3 ASD, 30% ≤ T1/T ≤ 50%,
在中期阶段T2时间内,待镀件的电流密度J2为0.5-1.5ASD,20%≤T1/T≤40%,In the mid-stage T2, the current density J2 of the parts to be plated is 0.5-1.5 ASD, 20% ≤ T1/T ≤ 40%,
在末期阶段T3时间内,待镀件的电流密度J3为1.0-2.0ASD,T3=T-T1-T2,J1>J3>J2。In the final stage T3, the current density J3 of the member to be plated is 1.0-2.0 ASD, T3=T-T1-T2, and J1>J3>J2.
在其中一个实施例中,步骤1)中的电镀装置还包括与电镀槽连接的喷流装置,喷流装置设有位于电镀槽内的喷嘴;In one embodiment, the electroplating apparatus in step 1) further comprises a jetting device connected to the electroplating tank, the jetting device being provided with a nozzle located in the electroplating tank;
步骤3)具体是,按控制条件控制电源工作和控制喷流装置进行侧面喷流,进行T时间的连续电镀;所述控制条件为:Step 3) Specifically, controlling the power supply operation according to the control condition and controlling the jet flow device to perform the side jet flow, and performing continuous plating for T time; the control condition is:
在初始阶段T1时间内,待镀件的电流密度J1为2-3ASD,喷嘴流量q1为1.5-2L/min,30%≤T1/T≤50%;In the initial stage T1, the current density J1 of the material to be plated is 2-3 ASD, the nozzle flow rate q1 is 1.5-2 L/min, 30% ≤ T1/T ≤ 50%;
在中期阶段T2时间内,待镀件的电流密度J2为0.5-1.5ASD,喷嘴流量q2为3-5L/min,20%≤T1/T≤40%;In the intermediate period T2, the current density J2 of the material to be plated is 0.5-1.5 ASD, the nozzle flow rate q2 is 3-5 L/min, 20% ≤ T1/T ≤ 40%;
在末期阶段T3时间内,待镀件的电流密度J3为1.0-2.0ASD,喷嘴流量q3为2-3L/min,T3=T-T1-T2,J1>J3>J2,q2>q3>q1。In the final stage T3, the current density J3 of the parts to be plated is 1.0-2.0 ASD, the nozzle flow rate q3 is 2-3 L/min, T3=T-T1-T2, J1>J3>J2, q2>q3>q1.
本发明的方法在电镀过程的先后三个阶段中对应地按待镀件的电流密度大小中来控制电源工作以进行电镀,经测试,本发明的方法相对于现有方法具有以下好的效果:达到相同的通孔填充效果,电镀的时间少;电镀的时间相同,通孔填充效果好。因此,本发明能相对降低通孔的填充时间,利于提高生产效率。The method of the present invention controls the power supply operation to perform electroplating correspondingly in the three stages of the electroplating process in accordance with the current density of the material to be plated. After testing, the method of the present invention has the following good effects compared to the existing method: The same through-hole filling effect is achieved, and the plating time is small; the plating time is the same, and the through-hole filling effect is good. Therefore, the present invention can relatively reduce the filling time of the through holes, which is advantageous for improving production efficiency.
本发明的方法在控制电源工作的情况下结合控制喷流装置的工作进行配合,使得通孔填充效果进一步的提高。The method of the present invention cooperates with the operation of controlling the jet flow device in the case of controlling the operation of the power source, so that the through hole filling effect is further improved.
附图说明DRAWINGS
图1为用于实现本发明方法的电镀装置的一种结构示意图。 BRIEF DESCRIPTION OF THE DRAWINGS Figure 1 is a schematic view showing the structure of a plating apparatus for carrying out the method of the present invention.
具体实施方式detailed description
实施例一Embodiment 1
一种电镀填通孔的方法,包括以下步骤:A method of plating a through hole, comprising the steps of:
1)如图1所示,采用电镀装置,电镀装置包括电镀槽1、电镀溶液2、电源3、阳极4,电镀槽1中装有电镀溶液2,阳极4连接电源5的正极,阳极4置于电镀槽1的电镀溶液2中;1) As shown in FIG. 1 , an electroplating apparatus is used. The electroplating apparatus includes a plating tank 1, a plating solution 2, a power source 3, and an anode 4. The plating tank 1 is provided with a plating solution 2, the anode 4 is connected to the anode of the power source 5, and the anode 4 is placed. In the plating solution 2 of the plating bath 1;
2)将带有通孔61的待镀件6与所述电源5的负极连接,并置于电镀槽1的电镀溶液2中;2) connecting the member to be plated 6 with the through hole 61 to the negative electrode of the power source 5, and placing it in the plating solution 2 of the plating tank 1;
在此步骤中,将带有通孔61的待镀件6作为阴极连接到电源5上,在电镀溶液的作用下,待镀件6与电源5、阳极4构成一回路。In this step, the member to be plated 6 with the through hole 61 is connected as a cathode to the power source 5, and the plate to be plated 6 forms a circuit with the power source 5 and the anode 4 under the action of the plating solution.
3)按控制条件控制电源3工作,进行T时间的连续电镀,T>0;所述控制条件为:3) Control the power supply 3 according to the control conditions, and perform continuous plating at T time, T>0; the control conditions are:
在初始阶段T1时间内,待镀件6的电流密度J1为2-3ASD,30%≤T1/T≤50%,During the initial period T1, the current density J1 of the member to be plated 6 is 2-3 ASD, 30% ≤ T1/T ≤ 50%,
在中期阶段T2时间内,待镀件6的电流密度J2为0.5-1.5ASD,20%≤T1/T≤40%,In the intermediate period T2, the current density J2 of the member to be plated 6 is 0.5-1.5 ASD, 20% ≤ T1/T ≤ 40%,
在末期阶段T3时间内,待镀件6的电流密度J3为1.0-2.0ASD,T3=T-T1-T2,J1>J3>J2。In the final stage T3, the current density J3 of the member to be plated 6 is 1.0-2.0 ASD, T3=T-T1-T2, and J1>J3>J2.
在步骤3)中,待镀件6的电流密度大小的调整,是通过控制电源的输出值来实现。In step 3), the adjustment of the current density of the member to be plated 6 is achieved by controlling the output value of the power source.
对于不同的待镀件(在本申请中主要强调通孔的尺寸不同),要到达一定的通孔填充效果,在相同条件下进行电镀所需的时间是不同的;对于同一待镀件,要到达不同的通孔填充效果,在相同条件下进行电镀所需的时间也是不同的。本方法中的连续电镀的时间T的大小,需要考虑最终所需的通孔填充效果来决定。本方法的技术核心是在电镀过程的先后三个阶段中对应地按待镀件6的电流密度大小中来控制电源3工作以进行电镀,经测试,本方法相对于现有方法具有以下好的效果:达到相同的通孔填充效果,电镀的时间少;电镀的时间相 同,通孔填充效果好。For different parts to be plated (in this application, the size of the through holes is mainly emphasized), to achieve a certain through hole filling effect, the time required for electroplating under the same conditions is different; for the same piece to be plated, Different via fill effects are reached, and the time required to perform the plating under the same conditions is also different. The size of the time T of continuous plating in the method needs to be determined in consideration of the final required through-hole filling effect. The technical core of the method is to control the power supply 3 to perform electroplating according to the current density of the material to be plated 6 in three successive stages of the electroplating process. After testing, the method has the following advantages compared with the existing method. Effect: achieve the same through hole filling effect, less plating time; plating time phase Similarly, the through hole filling effect is good.
以同一尺寸(孔径为80μm,孔深为100μm)的通孔按本不同方法进行电镀填充,测试结果见表一。The through holes of the same size (the aperture is 80 μm and the hole depth is 100 μm) are plated and filled according to different methods. The test results are shown in Table 1.
表一测试结果Table 1 test results
Figure PCTCN2015094365-appb-000001
Figure PCTCN2015094365-appb-000001
由表一可知,本发明方法相对现有方法,进行电镀的时间较短,通孔的填充效果仍然提高。As can be seen from Table 1, the method of the present invention has a shorter plating time and a higher filling effect of the through holes than the prior art.
实施例二 Embodiment 2
本实施例在实施例一的基础上,在电镀的过程中结合控制喷流装置的工作进行配合。This embodiment is based on the first embodiment, and cooperates with the control of the jet flow device during the electroplating process.
一种电镀填通孔的方法,包括以下步骤:A method of plating a through hole, comprising the steps of:
1)如图1所示,采用电镀装置,电镀装置包括电镀槽1、电镀溶液2、电源3、阳极4、喷流装置5,电镀槽1中装有电镀溶液2,喷流装置5与电镀槽1连接,喷流装置5设有位于电镀槽1内的喷嘴51,阳极4连接电源5的正极,阳极4置于电镀槽1的电镀溶液2中;1) As shown in FIG. 1 , an electroplating apparatus is used. The electroplating apparatus includes a plating tank 1, a plating solution 2, a power source 3, an anode 4, and a jetting device 5. The plating tank 1 is provided with a plating solution 2, a jetting device 5 and plating. The tank 1 is connected, the nozzle device 5 is provided with a nozzle 51 located in the plating tank 1, the anode 4 is connected to the anode of the power source 5, and the anode 4 is placed in the plating solution 2 of the plating tank 1;
喷流装置5将电镀槽1中的电镀溶液2吸入再由喷嘴51喷出到电镀槽1中,以驱使电镀溶液2在电镀槽1中流动,从而电镀溶液2更为均匀。The jet flow device 5 sucks the plating solution 2 in the plating tank 1 and ejects it from the nozzle 51 into the plating tank 1 to drive the plating solution 2 to flow in the plating tank 1, so that the plating solution 2 is more uniform.
2)将带有通孔61的待镀件6与所述电源5的负极连接,并置于电镀槽1的电镀溶液2中; 2) connecting the member to be plated 6 with the through hole 61 to the negative electrode of the power source 5, and placing it in the plating solution 2 of the plating tank 1;
3)按控制条件控制电源3工作和控制喷流装置5进行侧面喷流,进行T时间的连续电镀;所述控制条件为:3) Control the power supply 3 according to the control conditions and control the jet flow device 5 to perform side jet flow, and perform continuous plating for T time; the control conditions are:
在初始阶段T1时间内,待镀件6的电流密度J1为2-3ASD,喷嘴流量q1为1.5-2L/min,30%≤T1/T≤50%;During the initial period T1, the current density J1 of the member to be plated 6 is 2-3 ASD, the nozzle flow rate q1 is 1.5-2 L/min, and 30% ≤ T1/T ≤ 50%;
在中期阶段T2时间内,待镀件6的电流密度J2为0.5-1.5ASD,喷嘴流量q2为3-5L L/min,20%≤T1/T≤40%;In the intermediate period T2, the current density J2 of the member to be plated 6 is 0.5-1.5 ASD, the nozzle flow rate q2 is 3-5 L L/min, 20% ≤ T1/T ≤ 40%;
在末期阶段T3时间内,待镀件6的电流密度J3为1.0-2.0ASD,喷嘴流量q3为2-3L/min,T3=T-T1-T2,J1>J3>J2,q2>q3>q1。In the final stage T3, the current density J3 of the member to be plated 6 is 1.0-2.0 ASD, the nozzle flow rate q3 is 2-3 L/min, T3=T-T1-T2, J1>J3>J2, q2>q3>q1 .
喷嘴流量指喷嘴在单位时间内的流量,单位是L/min。侧面喷流是指喷嘴的喷射方向与待镀件的板面垂直,即平衡于待镀件的通孔的孔轴。The nozzle flow rate refers to the flow rate of the nozzle in unit time, and the unit is L/min. The side jet means that the spray direction of the nozzle is perpendicular to the plate surface of the member to be plated, that is, the hole axis which is balanced with the through hole of the member to be plated.
本方法在实施例一的基础上,在电镀的过程中结合控制喷流装置的工作进行配合,在三个电镀阶段使用不同喷嘴流量,经测试,本方法的效果在实施例一方法的效果的基础上,有进一步的提高。The method is based on the first embodiment, in combination with the operation of controlling the jet flow device during the electroplating process, using different nozzle flow rates in the three electroplating stages, and the effect of the method is tested in the effect of the first embodiment method. On the basis of this, there is further improvement.
以同一尺寸(孔径为80μm,孔深为100μm)的通孔按本发明方法进行电镀填充,测试结果见表二。The through holes of the same size (pore size 80 μm, hole depth 100 μm) were electroplated and filled according to the method of the present invention, and the test results are shown in Table 2.
表二测试结果Table 2 test results
Figure PCTCN2015094365-appb-000002
Figure PCTCN2015094365-appb-000002
由表一和表二对比可知,本实施例的本发明方法相对实施例一的本发明方法,在进行相同时间的电镀情况下,通孔的填充效果有进一步的提高。 It can be seen from the comparison between Table 1 and Table 2 that the method of the present invention of the present embodiment is further improved in the filling effect of the through holes in the case of the method of the present invention in the first embodiment.
以上所述实施例仅表达了本发明的几种实施方式,其描述较为具体和详细,但并不能因此而理解为对本发明专利范围的限制。应当指出的是,对于本领域的普通技术人员来说,在不脱离本发明构思的前提下,还可以做出若干变形和改进,这些都属于本发明的保护范围。因此,本发明专利的保护范围应以所附权利要求为准。 The above-mentioned embodiments are merely illustrative of several embodiments of the present invention, and the description thereof is more specific and detailed, but is not to be construed as limiting the scope of the invention. It should be noted that a number of variations and modifications may be made by those skilled in the art without departing from the spirit and scope of the invention. Therefore, the scope of the invention should be determined by the appended claims.

Claims (2)

  1. 一种电镀填通孔的方法,其特征在于,包括以下步骤:A method of plating a through hole, comprising the steps of:
    1)采用电镀装置,电镀装置包括电镀槽、电镀溶液、电源、阳极,电镀槽中装有电镀溶液,阳极连接电源的正极,阳极置于电镀槽的电镀溶液中;1) using an electroplating device, the electroplating device comprises a plating tank, a plating solution, a power source, an anode, a plating solution is arranged in the plating tank, an anode is connected to the anode of the power source, and the anode is placed in the plating solution of the plating tank;
    2)将带有通孔的待镀件与所述电源的负极连接,并置于电镀槽的电镀溶液中;2) connecting the member to be plated with the through hole to the negative electrode of the power source, and placing it in the plating solution of the plating tank;
    3)按控制条件控制电源工作,进行T时间的连续电镀,T>0;所述控制条件为:3) Control the power supply according to the control conditions, and perform continuous plating at T time, T>0; the control conditions are:
    在初始阶段T1时间内,待镀件的电流密度J1为2-3ASD,30%≤T1/T≤50%,In the initial stage T1, the current density J1 of the member to be plated is 2-3 ASD, 30% ≤ T1/T ≤ 50%,
    在中期阶段T2时间内,待镀件的电流密度J2为0.5-1.5ASD,20%≤T1/T≤40%,In the mid-stage T2, the current density J2 of the parts to be plated is 0.5-1.5 ASD, 20% ≤ T1/T ≤ 40%,
    在末期阶段T3时间内,待镀件的电流密度J3为1.0-2.0ASD,T3=T-T1-T2,J1>J3>J2。In the final stage T3, the current density J3 of the member to be plated is 1.0-2.0 ASD, T3=T-T1-T2, and J1>J3>J2.
  2. 如权利要求1所述的一种电镀填通孔的方法,其特征在于,A method of plating a via hole according to claim 1, wherein
    步骤1)中的电镀装置还包括与电镀槽连接的喷流装置,喷流装置设有位于电镀槽内的喷嘴;The electroplating apparatus in the step 1) further includes a jetting device connected to the plating tank, and the jetting device is provided with a nozzle located in the plating tank;
    步骤3)具体是,按控制条件控制电源工作和控制喷流装置进行侧面喷流,进行T时间的连续电镀;所述控制条件为:Step 3) Specifically, controlling the power supply operation according to the control condition and controlling the jet flow device to perform the side jet flow, and performing continuous plating for T time; the control condition is:
    在初始阶段T1时间内,待镀件的电流密度J1为2-3ASD,喷嘴流量q1为1.5-2L/min,30%≤T1/T≤50%;In the initial stage T1, the current density J1 of the material to be plated is 2-3 ASD, the nozzle flow rate q1 is 1.5-2 L/min, 30% ≤ T1/T ≤ 50%;
    在中期阶段T2时间内,待镀件的电流密度J2为0.5-1.5ASD,喷嘴流量q2为3-5L/min,20%≤T1/T≤40%;In the intermediate period T2, the current density J2 of the material to be plated is 0.5-1.5 ASD, the nozzle flow rate q2 is 3-5 L/min, 20% ≤ T1/T ≤ 40%;
    在末期阶段T3时间内,待镀件的电流密度J3为1.0-2.0ASD,喷嘴流量q3为2-3L/min,T3=T-T1-T2,J1>J3>J2,q2>q3>q1。 In the final stage T3, the current density J3 of the parts to be plated is 1.0-2.0 ASD, the nozzle flow rate q3 is 2-3 L/min, T3=T-T1-T2, J1>J3>J2, q2>q3>q1.
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