WO2015057178A1 - Procédé de préparation de composition à fumer sans tabac pour narguilé - Google Patents

Procédé de préparation de composition à fumer sans tabac pour narguilé Download PDF

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Publication number
WO2015057178A1
WO2015057178A1 PCT/UA2013/000154 UA2013000154W WO2015057178A1 WO 2015057178 A1 WO2015057178 A1 WO 2015057178A1 UA 2013000154 W UA2013000154 W UA 2013000154W WO 2015057178 A1 WO2015057178 A1 WO 2015057178A1
Authority
WO
WIPO (PCT)
Prior art keywords
hookah
tobacco
main organic
smoking
preparing
Prior art date
Application number
PCT/UA2013/000154
Other languages
English (en)
Russian (ru)
Inventor
Евгений Владимирович БАЛЮРА
Дмитрий ЧУРАКОВ
Original Assignee
Шишафрутс Лтд.
Евгений Владимирович БАЛЮРА
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Шишафрутс Лтд., Евгений Владимирович БАЛЮРА filed Critical Шишафрутс Лтд.
Priority to EP13873139.3A priority Critical patent/EP2923587A4/fr
Priority to CN201380019642.XA priority patent/CN105592726A/zh
Priority to US14/389,848 priority patent/US20160255875A1/en
Priority to EA201400802A priority patent/EA027156B1/ru
Publication of WO2015057178A1 publication Critical patent/WO2015057178A1/fr
Priority to US15/099,424 priority patent/US20160324210A1/en

Links

Classifications

    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
    • A24B15/303—Plant extracts other than tobacco
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B13/00—Tobacco for pipes, for cigars, e.g. cigar inserts, or for cigarettes; Chewing tobacco; Snuff
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F1/00—Tobacco pipes
    • A24F1/30—Hookahs

Definitions

  • the invention relates to tobacco substitutes, in particular to smoking compositions without tobacco, and is intended primarily for smoking using a hookah.
  • smoking is used in smoking mixtures prepared in a certain way and containing tobacco as the main gum-forming material, as well as various fillers in the form of various flavoring and aromatic additives, from which smoking articles, mainly cigarettes, are prepared.
  • Nicotine contained in smoke causes and maintains tobacco dependence.
  • Dependence is also accompanied by the habit of inhaling aromatic substances contained in tobacco smoke, such as gums, eugenol, pyrazine, licorice, sugar, honey, menthol and others.
  • Cigarette smoking is a pyrolysis process: decomposition, decomposition or conversion of compounds or substances as a result of heating to high temperatures of 850 - 900 ° ⁇ . Recently, smoking through a hookah has become widespread, in which smoke is passed through water and partially cleared of harmful components.
  • the process of smoking a hookah mixture occurs at relatively low temperatures of 180-200 ° C, is characterized by evaporation and distillation of volatile components of carbohydrate-containing substances, in which sublimation of low-boiling compounds occurs under the influence of heat from smoldering coal, so the hookah mixture does not burn, but dries, while the mass decreases reaches 30%.
  • Glycerin propylene glycol or a similar substance, which is part of the hookah smoking composition, when heated forms a thick vapor, similar to tobacco smoke.
  • Smoking through a hookah has become widespread due to the fact that smoke in a hookah passes through water and is partially cleared of harmful components.
  • the role of the filter is played by a hookah mine, on the cold walls of which various impurities condense, and a vessel with a liquid in which up to 38% of the substances contained in the smoke are deposited.
  • a smoking cup with a pipe is inserted into the vessel, the end of which goes under water. Above the water level, a pipe leaves the vessel through which smoke is inhaled.
  • tobacco is used as a smoke-generating component, which is very dangerous for human health.
  • the known method is intended mainly for the production of cigarettes.
  • the content of inorganic filler is from May 30 to 90%, and the content of fruit material is from May 10 to 30. % in terms of dry matter.
  • the disadvantage of this method is that the powdered dried fruits, due to the high dispersion, lose most of the taste and aromatic properties, and therefore, the resulting smoking material is used primarily for cigarettes, but not for hookah.
  • tea leaves are used as the main filling component, which are ground to obtain particles of 0.5-10 mm in size and dried to a moisture content of 12-20%.
  • the smoking filler material obtained in this way does not contain nicotine and does not have a harmful effect on the smoker's body, while it contains a small amount of alkaloids: caffeine (from 1 to 4 percent), as well as theobromine, theophylline, adeine, guanine, while allowing to obtain a tonic effect and feel the “smoke blowing effect”.
  • the disadvantages of this method is that the resulting filling material quickly burns out, has a high consumption and low smoke quality, will not allow replacing tobacco smoking and overcoming the habit of smoking tobacco, and also limits the range of taste and aromatic properties.
  • the closest to the intended purpose and the technical result achieved is a method of preparing a smoking composition without tobacco for hookah, including the preliminary preparation of the main organic filling material and impregnating it with a binder [“Smoking mixture without tobacco” RU2388387, A24B15 / 16, 05/10/2010] [5] .
  • the tobacco-free smoking mixture obtained in this way contains tea raw materials as the main organic filler material, and glycerin as the binder.
  • tea raw materials are washed with hot water (80-90 ° C) for 8 hours, dried and cut.
  • Rinsing with hot water allows you to remove theobromine, theophylline, anthocyanin glycosides and tannin - catechin mixtures from tea raw materials, which can suppress the organoleptic properties of the flavor and can also cause allergic reactions.
  • the disadvantage of this method is that the resulting smoking composition quickly burns out, has a high consumption per refueling a cup of hookah and not a high quality smoke.
  • the objective of the invention is the creation of such a method of preparing a smoking composition without tobacco for hookah, which would reduce the rate of combustion and consumption of the smoking composition by one filling, and also would improve the quality of the smoke.
  • the problem is solved in that in the method of preparing a smoking composition without tobacco for hookah, comprising pre-preparing the main organic filler material and impregnating it with a binder, according to the invention, at least one kind of fruit is used as the main organic filler material, and as a binder use a mixture of propylene glycol and food glycerin in the ratio (1: 4) - (4: 1), and the preliminary preparation of the main organic filling material carried out by lyophilization, during which the fruit is crushed to a fraction of 3-12 mm, frozen in liquid nitrogen at a temperature of (-) 40 - (-) 60 ° C, kept under vacuum for 30-40 minutes to obtain a filler material, with residual moisture 1-6%, and impregnation with its binder is performed in the following ratio of components in the composition, May. %:
  • the main organic filling material is 10-55;
  • Preliminary preparation of the main organic filling material by lyophilization during which at least one kind of fruit is ground to a fraction of 3-12 mm, then frozen in liquid nitrogen at a temperature of (-) 40 - (-) 60 ° ⁇ , kept under vacuum 30-40 minutes to obtain a filling material with a residual moisture content of 1-6%, ensures the preservation of natural properties in dried fruits, structural integrity and biological activity.
  • the residual moisture content of the filler material is higher than 6%, the effectiveness of moistening it with a binder is reduced, which leads to a decrease in the quality of the smoking composition.
  • the resulting smoking composition becomes liquid, which makes it possible to flow through the holes in the hookah bowl, which in turn shortens the life of one gas station and contaminates the hookah shaft
  • the inventive method of preparing a smoking composition without tobacco for hookah can reduce the rate of combustion and reduce the consumption of the smoking composition for one gas station, and also improves its quality.
  • Impregnation under pressure up to 1 MPa, or under vacuum up to (-) 1 MPa. improves the quality of impregnation of fruits, especially those that are poorly absorbing liquid, which reduces the cost of the production process, since it does not require the use of additional equipment for air purification and supply of liquid to the impregnation chamber.
  • vanilla extract and / or food flavorings in the amount of 2-5% of the composition as flavoring additives provides an expansion of the assortment of taste and aromatic combinations.
  • the main organic filling material which is used as at least one kind of fruit, is pre-prepared and impregnated with a binder.
  • binder use a mixture of propylene glycol and food glycerin in the ratio (1: 4) - (4: 1),
  • Preliminary preparation of the main organic filler material is carried out by lyophilization, in the process by which the fruit is crushed to a fraction of 3-12 mm., Then quickly frozen at a temperature of (-) 40 - (-) 60 ° C and kept under vacuum for 30-40 minutes until obtaining freeze-dried fruits with a residual moisture content of 1-6%,
  • Binder impregnation is carried out immediately before packaging in a retail container, for which the organic filling material is removed from the packaging and placed in a mixing container, where the binder is impregnated in the following ratio of components in May. %:
  • the main organic filling material is 10-55;
  • At least one of the fruits is used as the main organic filling material: apple, pear, plum, peach, quince, apricot, grape, lemon, watermelon, lychee, mango, banana, kiwi, orange, cherry, strawberry, melon, pineapple, raspberries, as well as mixtures thereof.
  • the impregnation is carried out in a mixing container at atmospheric pressure, or under high pressure up to 1 MPa, or under vacuum up to (-) 1 MPa, while the residence time of the mixture under pressure varies depending on the type of fruit;
  • vanilla extract and / or food flavorings are used in an amount of 2-5% to the composition, which are added to the binder during the impregnation process.
  • the invention is further illustrated by examples.
  • Lemon was used as the main organic filling material.
  • a binder used a mixture of propylene glycol and food glycerin in a ratio of 1: 4. with the addition of 3% natural lemon flavor.
  • the lemon was washed with water and crushed to a fraction of 3-6 mm and quickly frozen in liquid nitrogen at a temperature of -45 ° C, then kept under vacuum for 40 minutes to obtain a filling material with a residual moisture content of 6%,
  • the dried lemon slices were placed in an airtight package made of a foil-based polymeric material, which excludes the access of oxygen inside.
  • Binder impregnation was performed before packaging in retail containers in a mixing container, in the following ratio of components in the composition, in May. %:
  • the smoking composition obtained in this way is characterized by low concentration steam, softness, easy to inhale, has a pleasant lemon taste with a slight tart and sweet taste.
  • Grapes were used as the main organic filling material.
  • the grapes were crushed to a fraction of 3-6 mm and quickly frozen in liquid nitrogen at a temperature of -50 ° C, then kept under vacuum for 30 minutes until a filler material with a residual moisture content of 4% was obtained,
  • the filler material was impregnated with a binder in a mixing container under vacuum to -0.75MPa for 10 seconds with the following ratio of components in the composition, May. %:
  • binder - a mixture of propylene glycol and food glycerol - the rest.
  • the smoking composition obtained in this way is characterized by light and soft steam, tastes like grapes with a tart sweetish flavor.
  • Example 3 Apples were used as the main organic filling material.
  • binder a mixture of propylene glycol and food glycerin in a ratio of 1: 1.
  • the apples were washed and crushed to a fraction of 3-5 mm, quickly frozen in liquid nitrogen at a temperature of -60 ° C, then kept under vacuum for 40 minutes to obtain a filler material with a residual moisture content of 3%,
  • Binder impregnation was performed in a mixing container, with the following ratio of components in May. %:
  • binder - a mixture of propylene glycol and food glycerin
  • smoking composition is characterized by soft steam, has a pleasant taste and aroma of apples.
  • Pears were used as the main organic filling material, and a mixture of propylene glycol and food glycerin in a ratio of 1: 4 was used as a binder.
  • Pears were crushed to a fraction of 3-12 mm, frozen in liquid nitrogen at a temperature of -45 ° C, then kept under vacuum for 30 minutes to obtain a filler material with a residual moisture content of 4%.
  • the resulting filler material was placed in a sealed package.
  • Impregnation with a binder with flavorings which were used coconut oil and food flavorings of TAIGA International NV, in an amount of 2-5% of the total volume of the liquid mixture, was carried out in a mixing container in the following ratio of components in the composition, May. %:
  • the vapor When smoking the resulting smoking composition, the vapor is characterized by softness and ease of inhalation, has a pleasant taste and aroma of a pear with a weak tart, moderately sweetish taste and a slight smell .
  • the use of the proposed method for preparing a smoking composition allows to reduce the combustion rate and consumption per refueling, improve the quality of the smoke and expand the range of taste and aromatic properties.
  • the temperature of the hookah mixture at the time of consumption was 180 ⁇ 10 ° ⁇ .
  • the pieces of the filling material made of fruits are conveniently sized to fit into a cup of hookah by hand.
  • the size of the pieces of fruit is less than 3 mm, then they will turn into porridge, which in turn will lead to leakage of the mixture through the holes of the hookah cup, which reduces the service life of one filling and increases the consumption of the smoking composition.
  • the size of the pieces of fruit is more than 12 mm, then they will not be evenly located in a cup of hookah and will create problems with the compactness of the package.
  • the inventive method allows to expand the range of the smoking composition and reduce the consumption of the smoking composition when using it.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Botany (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

L'invention concerne des substituts de tabac, notamment des compositions à fumer sans tabac, et est essentiellement destinée à être utilisée avec un narguilé. Le procédé de préparation de composition à fumer sans tabac pour narguilé consiste à préparer au préalable un matériau organique principal, et on utilise en qualité matériau organique principal de charge au moins un type de fruits, tandis que le liant consiste en un mélange de propylène glycol et de glycérine alimentaire dans une proportion de (1 :4) -(4:1); la préparation préalable du matériau organique principal de charge se fait par lyophilisation au cours de laquelle les fruits sont broyés en fraction de 3 à 12 mm, puis congelés dans de l'azote liquide à une température de -40 à -60°C, après quoi on observe un vide pendant 30-40 minutes jusqu'à obtenir le matériau de charge avec une humidité résiduelle de 1-6%; on l'imprègne ensuite du liant selon les proportions suivantes des composants en % en poids dans la composition : 10-55 de matériau organique principal de charge; le reste se composant du liant. Le résultat technique consiste en un procédé de préparation de composition à fumer sans tabac pour narguilé qui permet de ralentir la vitesse de combustion et de réduire les dépenses pour une recharge et d'améliorer sa qualité.
PCT/UA2013/000154 2013-10-14 2013-12-30 Procédé de préparation de composition à fumer sans tabac pour narguilé WO2015057178A1 (fr)

Priority Applications (5)

Application Number Priority Date Filing Date Title
EP13873139.3A EP2923587A4 (fr) 2013-10-14 2013-12-30 Procédé de préparation de composition à fumer sans tabac pour narguilé
CN201380019642.XA CN105592726A (zh) 2013-10-14 2013-12-30 水烟用无烟草烟气混合物的制备方法
US14/389,848 US20160255875A1 (en) 2013-10-14 2013-12-30 Method of preparation the smoking composition without tobacco for the hookah
EA201400802A EA027156B1 (ru) 2013-10-14 2013-12-30 Способ приготовления курительной композиции без табака для кальяна
US15/099,424 US20160324210A1 (en) 2013-10-14 2016-04-14 Method of preparing tobacco-free smoking composition for hookah

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
UAA201312059A UA108692C2 (uk) 2013-10-14 2013-10-14 Спосіб приготування курильної композиції без тютюну для кальяну
UAA201312059 2013-10-14

Related Child Applications (1)

Application Number Title Priority Date Filing Date
US15/099,424 Continuation US20160324210A1 (en) 2013-10-14 2016-04-14 Method of preparing tobacco-free smoking composition for hookah

Publications (1)

Publication Number Publication Date
WO2015057178A1 true WO2015057178A1 (fr) 2015-04-23

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PCT/UA2013/000154 WO2015057178A1 (fr) 2013-10-14 2013-12-30 Procédé de préparation de composition à fumer sans tabac pour narguilé

Country Status (6)

Country Link
US (2) US20160255875A1 (fr)
EP (1) EP2923587A4 (fr)
CN (1) CN105592726A (fr)
EA (1) EA027156B1 (fr)
UA (1) UA108692C2 (fr)
WO (1) WO2015057178A1 (fr)

Cited By (2)

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Publication number Priority date Publication date Assignee Title
US11330834B2 (en) 2016-04-22 2022-05-17 Japan Tobacco Inc. Flavor source manufacturing method
WO2022108474A1 (fr) * 2020-11-19 2022-05-27 Общество С Ограниченной Ответственностью "Спейс Смоук" Mélange pour narguilé à base minérale

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US20180199617A1 (en) 2017-01-18 2018-07-19 Bianca Iodice Tobacco Free Hookah Smoking Gel
CN109832654A (zh) * 2019-01-10 2019-06-04 广东中烟工业有限责任公司 一种片烟低温复烤方法及其制备的复烤片烟
CN109875095A (zh) * 2019-02-01 2019-06-14 湖北中烟工业有限责任公司 可用于卷烟产品加香加料的孜然超微粉的超低温制备方法
CN112369644A (zh) * 2020-10-22 2021-02-19 湖北中烟工业有限责任公司 烟草原料的制备方法及具有该烟草原料的加热不燃烧卷烟
AU2022443169A1 (en) * 2022-02-26 2024-09-12 Admish, Inc. Smoking product and methods of manufacture

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RU2403832C1 (ru) 2009-08-10 2010-11-20 Общество с ограниченной ответственностью Торгово-Промышленное Предприятие "Столичное" Способ производства курительной композиции для кальяна

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11330834B2 (en) 2016-04-22 2022-05-17 Japan Tobacco Inc. Flavor source manufacturing method
WO2022108474A1 (fr) * 2020-11-19 2022-05-27 Общество С Ограниченной Ответственностью "Спейс Смоук" Mélange pour narguilé à base minérale

Also Published As

Publication number Publication date
UA108692C2 (uk) 2015-05-25
EP2923587A1 (fr) 2015-09-30
US20160324210A1 (en) 2016-11-10
US20160255875A1 (en) 2016-09-08
CN105592726A (zh) 2016-05-18
EA201400802A1 (ru) 2016-08-31
EP2923587A4 (fr) 2016-08-24
EA027156B1 (ru) 2017-06-30

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