WO2015010351A1 - 一种多层金属网与金属粉末复合过滤管、滤芯的生产方法 - Google Patents
一种多层金属网与金属粉末复合过滤管、滤芯的生产方法 Download PDFInfo
- Publication number
- WO2015010351A1 WO2015010351A1 PCT/CN2013/081742 CN2013081742W WO2015010351A1 WO 2015010351 A1 WO2015010351 A1 WO 2015010351A1 CN 2013081742 W CN2013081742 W CN 2013081742W WO 2015010351 A1 WO2015010351 A1 WO 2015010351A1
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- WIPO (PCT)
- Prior art keywords
- layer
- metal
- filter
- mesh
- composite
- Prior art date
Links
- 229910052751 metal Inorganic materials 0.000 title claims abstract description 117
- 239000002184 metal Substances 0.000 title claims abstract description 111
- 239000000843 powder Substances 0.000 title claims abstract description 62
- 239000002131 composite material Substances 0.000 title claims abstract description 56
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 17
- 238000000034 method Methods 0.000 title claims abstract description 15
- 238000001914 filtration Methods 0.000 claims abstract description 24
- 238000005245 sintering Methods 0.000 claims abstract description 15
- 238000003466 welding Methods 0.000 claims abstract description 10
- 238000003475 lamination Methods 0.000 claims abstract description 5
- 239000002905 metal composite material Substances 0.000 claims abstract 2
- 238000005096 rolling process Methods 0.000 claims abstract 2
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 12
- 229910052759 nickel Inorganic materials 0.000 claims description 7
- 238000005507 spraying Methods 0.000 claims description 7
- 229910045601 alloy Inorganic materials 0.000 claims description 6
- 239000000956 alloy Substances 0.000 claims description 6
- 229910052782 aluminium Inorganic materials 0.000 claims description 6
- 229910052786 argon Inorganic materials 0.000 claims description 6
- 229910052802 copper Inorganic materials 0.000 claims description 6
- 229910052742 iron Inorganic materials 0.000 claims description 6
- 229910052758 niobium Inorganic materials 0.000 claims description 6
- 229910052715 tantalum Inorganic materials 0.000 claims description 6
- 229910052718 tin Inorganic materials 0.000 claims description 6
- 229910052719 titanium Inorganic materials 0.000 claims description 6
- 229910052721 tungsten Inorganic materials 0.000 claims description 6
- 229910052725 zinc Inorganic materials 0.000 claims description 6
- 229910052726 zirconium Inorganic materials 0.000 claims description 6
- 229910052804 chromium Inorganic materials 0.000 claims description 5
- 229910052750 molybdenum Inorganic materials 0.000 claims description 5
- 238000005266 casting Methods 0.000 claims description 3
- 238000007750 plasma spraying Methods 0.000 claims description 3
- 238000007590 electrostatic spraying Methods 0.000 claims description 2
- 230000004907 flux Effects 0.000 abstract description 5
- 238000009940 knitting Methods 0.000 abstract 1
- 239000003208 petroleum Substances 0.000 abstract 1
- 238000007493 shaping process Methods 0.000 abstract 1
- 238000002156 mixing Methods 0.000 description 11
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 8
- 238000000465 moulding Methods 0.000 description 7
- 238000001816 cooling Methods 0.000 description 5
- 239000010935 stainless steel Substances 0.000 description 4
- 229910001220 stainless steel Inorganic materials 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000010344 co-firing Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000010285 flame spraying Methods 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/11—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with bag, cage, hose, tube, sleeve or like filtering elements
- B01D29/111—Making filtering elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F3/00—Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
- B22F3/10—Sintering only
- B22F3/11—Making porous workpieces or articles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D39/00—Filtering material for liquid or gaseous fluids
- B01D39/10—Filter screens essentially made of metal
- B01D39/12—Filter screens essentially made of metal of wire gauze; of knitted wire; of expanded metal
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D39/00—Filtering material for liquid or gaseous fluids
- B01D39/14—Other self-supporting filtering material ; Other filtering material
- B01D39/20—Other self-supporting filtering material ; Other filtering material of inorganic material, e.g. asbestos paper, metallic filtering material of non-woven wires
- B01D39/2027—Metallic material
- B01D39/2031—Metallic material the material being particulate
- B01D39/2034—Metallic material the material being particulate sintered or bonded by inorganic agents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F3/00—Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
- B22F3/10—Sintering only
- B22F3/1017—Multiple heating or additional steps
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F5/00—Manufacture of workpieces or articles from metallic powder characterised by the special shape of the product
- B22F5/10—Manufacture of workpieces or articles from metallic powder characterised by the special shape of the product of articles with cavities or holes, not otherwise provided for in the preceding subgroups
- B22F5/106—Tube or ring forms
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F7/00—Manufacture of composite layers, workpieces, or articles, comprising metallic powder, by sintering the powder, with or without compacting wherein at least one part is obtained by sintering or compression
- B22F7/02—Manufacture of composite layers, workpieces, or articles, comprising metallic powder, by sintering the powder, with or without compacting wherein at least one part is obtained by sintering or compression of composite layers
- B22F7/04—Manufacture of composite layers, workpieces, or articles, comprising metallic powder, by sintering the powder, with or without compacting wherein at least one part is obtained by sintering or compression of composite layers with one or more layers not made from powder, e.g. made from solid metal
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F7/00—Manufacture of composite layers, workpieces, or articles, comprising metallic powder, by sintering the powder, with or without compacting wherein at least one part is obtained by sintering or compression
- B22F7/06—Manufacture of composite layers, workpieces, or articles, comprising metallic powder, by sintering the powder, with or without compacting wherein at least one part is obtained by sintering or compression of composite workpieces or articles from parts, e.g. to form tipped tools
- B22F7/08—Manufacture of composite layers, workpieces, or articles, comprising metallic powder, by sintering the powder, with or without compacting wherein at least one part is obtained by sintering or compression of composite workpieces or articles from parts, e.g. to form tipped tools with one or more parts not made from powder
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K10/00—Welding or cutting by means of a plasma
- B23K10/02—Plasma welding
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K9/00—Arc welding or cutting
- B23K9/02—Seam welding; Backing means; Inserts
- B23K9/025—Seam welding; Backing means; Inserts for rectilinear seams
- B23K9/0253—Seam welding; Backing means; Inserts for rectilinear seams for the longitudinal seam of tubes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2239/00—Aspects relating to filtering material for liquid or gaseous fluids
- B01D2239/06—Filter cloth, e.g. knitted, woven non-woven; self-supported material
- B01D2239/065—More than one layer present in the filtering material
- B01D2239/0672—The layers being joined by welding
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T29/00—Metal working
- Y10T29/49—Method of mechanical manufacture
- Y10T29/49826—Assembling or joining
- Y10T29/4989—Assembling or joining with spreading of cable strands
Definitions
- the invention belongs to the technical field of refinery filtration equipment production, and relates to a supporting application in the S-Zorb device 101, 102, 103, 104, 105, 110, 111, 108 device of the China Petrochemical Co., Ltd., the raw material oil filter device 104 and A method for producing a multi-layer metal mesh and metal powder composite filter tube and a filter element for hydrogen treatment of a F100-B device.
- the existing metal filter used in the S-Zorb device of China Petrochemical Co., Ltd. has a large working pressure difference, generally 2.5 to <6, ie a, using such a metal filter, the filtration flow rate is low, As a result, the capacity of the entire device is low.
- the present invention provides a method for producing a multi-layer metal mesh and a metal powder composite filter tube and a filter element which have the characteristics of low filtration resistance, large filtration flux and high pressure resistance.
- a method for producing a multi-layer metal mesh and a metal powder composite filter tube and a filter element the process steps are as follows:
- the wire is woven to obtain wire mesh of different meshes, and then the wire mesh of different meshes is laminated to obtain a laminated structure.
- the principle of lamination is continuous from one side to the other side.
- the number of the laminates is 1 to 5 layers;
- the laminated structure is placed in a vacuum furnace, and sintered at 900 to 1500 ° C for 10 to 30 hours to obtain a multilayer support layer;
- the support layer is taken out after cooling, using electrostatic spraying or ordinary spraying
- the casting method is performed at 900 to 1500 ° C, and is cooled, and the thickness of the composite layer is 0. l ⁇ 0. 5mm, and then sintered at 900 to 1500 ° C, and cooling is performed on the side of the high mesh layer of the support layer.
- a multi-layer metal mesh and metal powder composite filter sheet and tube having a multi-layer metal mesh as a structural support layer and a metal powder sintered structure as a filter layer are obtained, and then the composite filter sheet and the tube are rolled into a tubular shape by a molding machine.
- the filter core is then welded with a argon arc welder or a plasma welder to form a multi-layer metal mesh and metal powder composite filter tube and filter product.
- the structure of the support layer is a composite structure of a multilayer wire mesh.
- the structural support layer has a thickness of l ⁇ 19 mm, and is formed by superposing and sintering a multi-layer metal mesh having a filtration precision of 1 to 1000.
- the support layer and the filter layer formed by the wire are formed into a double-layer composite structure for co-sintering treatment, or the support layer formed of the wire is formed into a composite structure with the metal powder sheet.
- the filter layer is adhered to the support layer by low-temperature spraying and then sintering by using a metal powder of 100 to 1000 mesh, and the filter layer is prepared by plasma spraying or conventional spraying, and then sintered together with the support layer.
- the metal powder used in the filter layer is an elemental metal powder of Fe, Co, Ni, W, Mo, Cr, Cu, Al, Ti, Zn, Sn, Ta, Nb, Zr, or a plurality of these metal elements
- the alloy powder is composed.
- the metal mesh of the support layer is a single metal wire of Fe, Co, Ni, W, Mo, Cr, Cu, Al, Ti, Zn, Sn, Ta, Nb, Zr, or among these metal elements
- a variety of alloy wires are prepared by preparation.
- the multi-layer metal mesh and the metal powder composite filter sheet and the tube are processed into a non-symmetrical structure powder sintered filter tube having a composite structure by a coiling tube and a welding process.
- the invention has the advantages that: the composite structure using the multi-layer metal mesh as the support layer and the sintered metal powder layer as the filter layer has the characteristics of low filtration resistance, large filtration flux and strong pressure resistance, and is mainly used in China Petrochemical Co., Ltd.
- Company S-Zorb devices 101, 102, 103, 104, 105, 110, 111, 108 devices, feedstock oil filter 104 devices and hydrotreating F100-B devices can be improved while other components in the device are unchanged
- the filtration flow rate is 10% to 50%, which greatly increases the overall output.
- DRAWINGS BRIEF DESCRIPTION OF THE DRAWINGS Fig. 1 is a schematic view showing the comparison of the test throughput of the present invention with the existing domestic and foreign similar products under the condition of a filtration precision of 1 ⁇ 10 ⁇ . detailed description
- the invention discloses a method for producing a multi-layer metal mesh and a metal powder composite filter tube and a filter element, and the process steps are as follows:
- the wire is woven to obtain wire mesh of different meshes, and then the wire mesh of different meshes is laminated to obtain a laminated structure.
- the principle of lamination is continuous from one side to the other side.
- the number of laminations is 1 ⁇ -5 layers;
- the laminated structure is placed in a vacuum furnace, and sintered at 900 ⁇ 1500 °C for 10 ⁇ 30 hours to obtain a multi-layer support layer; 1 ⁇ 0.
- the thickness of the composite layer is 0. l ⁇ 0.
- the thickness of the composite layer is 0. l ⁇ 0.
- the structure of the support layer is a composite structure of a multi-layered metal mesh; the thickness of the structural support layer is 1 ⁇ 10 mm, which is formed by superposing and sintering a multi-layer metal mesh with a filtration precision of 20 ⁇ 1000;
- the support layer and the filter layer of the wire are formed into a double-layer composite structure for co-firing treatment, or the support layer formed of the wire is formed into a composite structure with the metal powder piece;
- the metal mesh of the support layer is made of metal A simple metal wire of Fe, Co, Ni, W, Mo, Cr, Cu, Al, Ti, Zn, Sn, Ta, Nb, Zr, or an alloy wire composed of a plurality of these metal elements is prepared.
- the multi-layer metal mesh and metal powder composite filter plate and tube have a multi-layer metal mesh as a structural support layer and a metal powder sintered structure as a filter layer; the filter layer is sprayed with a metal powder of 100-1000 mesh by low temperature spraying, and then sintered.
- the method is attached to the support layer, or the filter layer is prepared by flame or plasma spraying, and then co-sintered with the support layer; the metal powder used in the filter layer is Fe, Co, Ni, W, Mo, An elemental metal powder of Cr, Cu, Al, Ti, Zn, Sn, Ta, Nb, Zr, or an alloy powder composed of a plurality of these metal elements.
- the multi-layer metal mesh and the metal powder composite filter sheet and the tube are processed into a non-symmetrical structure powder sintered filter tube having a composite structure by a coiling tube and a welding process.
- a composite powder sintered filter sheet and a tube having a double-layer or a three-layer structure are produced by the present invention, and the composite powder sintered filter sheet and tube have the advantages of high filtration precision, low filtration resistance and high strength. Compared with the prior art, the invention has substantial and significant progress.
- Example 1 Take 100 sheets of 1000 inches long and 500 inches wide, 2 sheets of 40 mesh, 2 sheets of 12 mesh, 100 mesh, 40 mesh, 40 mesh, 12 mesh, 12 mesh from top to bottom, The five layers of the screen are arranged in a neat manner, and then subjected to boundary welding, welded, placed in a vacuum furnace, sintered at 900-1500 ° C, sintered for 10 hours to obtain a support layer; after the support layer is cooled and taken out, Take 1 ⁇ 2 kg of stainless steel 316L, 304, 310S powder with a particle size of 100 ⁇ 200 mesh, add 0.1%_20% of molding agent, and take it out in mixing equipment for 1-3 hours.
- the mixing equipment is V type.
- the machine or plasma welder welds the middle seam of the filter core, and installs the prepared filter core product in the S-Zorb device 101, 102, 103, 104, 105, 110, 1 11, 108 of China Petrochemical Co., Ltd.
- the oil filter 104 unit and the hydrotreated F100-B unit are used.
- Example 2 Take 500 sheets of 1000 mm long and 500 mm wide, 2 sheets of 40 mesh, 2 sheets of 12 * 64 mesh, and 500 mesh, 40 mesh, 40 mesh, 12 64 mesh, and 12 64 mesh in order from top to bottom. , the five layers of the screen are arranged neatly and then subjected to boundary welding. After welding, it is placed in a vacuum furnace, sintered at 900-1500 ° C, and sintered for 15 hours to obtain a support layer; the support layer is cooled and taken out, and then 1-2 kg of stainless steel having a particle size of 50 to 600 mesh is taken. 316 304, 310S powder, adding 0.1% ⁇ 20% of the molding agent, in the mixing The equipment is taken out after mixing for 1-3 hours.
- the mixing equipment is a V-type mixing equipment, a double-cone mixer or a ball mill, and then the mixed stainless steel powder is cast on the re-sintered 5-layer mesh support layer, and the thickness is L-5mm, then the composite structure is placed in a vacuum furnace, sintered at 1000 1600 ° ⁇ for secondary sintering treatment, cooled and taken out to obtain a multi-layer metal mesh and metal powder composite filter, tube, and then filter
- the tube is formed by a molding machine, and the filter sheet and the tube are rolled into a tubular filter core. Finally, the middle seam of the filter core is welded by a argon arc welder or a plasma welder, and the prepared filter core product is installed in China Petrochemical Co., Ltd.
- Example 3 Take a metal nickel mesh with a length of 1000 mm and a width of 500 mm, wherein one of 100 meshes, one of 40 meshes, and two of ten meshes are 100 mesh, 40 mesh, 10 mesh, and 10 mesh from top to bottom.
- the four layers of wire mesh are arranged neatly and then welded to the boundary. After welding, they are placed in a vacuum furnace, sintered at 9000 1500 ° C, and sintered for 20 hours to obtain a support layer. After the support layer is cooled, it is taken out and then taken.
- the mixing equipment is a V-mixing device, double cone Mixer or ball mill, and then cast the mixed metal nickel powder on the re-sintered 4-layer mesh support layer to a thickness of 15 mm. Then, the composite structure is placed in a vacuum furnace and sintered at 1000 1600 ° C. After the secondary sintering treatment, after cooling and taking out, a multi-layer metal mesh and metal powder composite filter sheet and tube are obtained, and then the filter sheet and the tube are molded by a molding machine, the filter sheet and the tube are rolled into a tubular filter core, and finally the argon arc is used.
- the welder or plasma welder will be in the middle of the filter Welded, to products prepared of the filter element is mounted in China Petrochemical Co., Ltd.
Abstract
Description
Claims
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US14/758,616 US10092865B2 (en) | 2013-07-22 | 2013-08-19 | Method for producing composite filter tube and filter element made of multilayer metal mesh and metal powders |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310308196.6 | 2013-07-22 | ||
CN2013103081966A CN103357881A (zh) | 2013-07-22 | 2013-07-22 | 一种多层金属网与金属粉末复合过滤管、滤芯的生产方法 |
Publications (1)
Publication Number | Publication Date |
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WO2015010351A1 true WO2015010351A1 (zh) | 2015-01-29 |
Family
ID=49360616
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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PCT/CN2013/081742 WO2015010351A1 (zh) | 2013-07-22 | 2013-08-19 | 一种多层金属网与金属粉末复合过滤管、滤芯的生产方法 |
Country Status (3)
Country | Link |
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US (1) | US10092865B2 (zh) |
CN (1) | CN103357881A (zh) |
WO (1) | WO2015010351A1 (zh) |
Cited By (1)
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US10525384B2 (en) * | 2014-01-15 | 2020-01-07 | Fuji Filter Manufacturing Co., Ltd. | Filter element and filtering apparatus |
JP6203145B2 (ja) * | 2014-08-01 | 2017-09-27 | 株式会社東芝 | 濾過用フィルター |
CN104524870A (zh) * | 2015-01-07 | 2015-04-22 | 江苏云才材料有限公司 | 一种镍铜合金烧结丝网管的制备方法 |
CN104857775A (zh) * | 2015-06-05 | 2015-08-26 | 徐小平 | 一种金属粉末和金属烧结网复合滤芯及其生产方法 |
CN105536356A (zh) * | 2016-01-22 | 2016-05-04 | 韶关市贝瑞过滤科技有限公司 | 一种S-Zorb装置用高强度、抗断裂的滤芯 |
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