WO2014192062A1 - マイクロ波プラズマ発生装置の空洞共振器 - Google Patents
マイクロ波プラズマ発生装置の空洞共振器 Download PDFInfo
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- WO2014192062A1 WO2014192062A1 PCT/JP2013/064641 JP2013064641W WO2014192062A1 WO 2014192062 A1 WO2014192062 A1 WO 2014192062A1 JP 2013064641 W JP2013064641 W JP 2013064641W WO 2014192062 A1 WO2014192062 A1 WO 2014192062A1
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/32—Gas-filled discharge tubes
- H01J37/32009—Arrangements for generation of plasma specially adapted for examination or treatment of objects, e.g. plasma sources
- H01J37/32192—Microwave generated discharge
- H01J37/32211—Means for coupling power to the plasma
- H01J37/32247—Resonators
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- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05H—PLASMA TECHNIQUE; PRODUCTION OF ACCELERATED ELECTRICALLY-CHARGED PARTICLES OR OF NEUTRONS; PRODUCTION OR ACCELERATION OF NEUTRAL MOLECULAR OR ATOMIC BEAMS
- H05H1/00—Generating plasma; Handling plasma
- H05H1/24—Generating plasma
- H05H1/46—Generating plasma using applied electromagnetic fields, e.g. high frequency or microwave energy
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/32—Gas-filled discharge tubes
- H01J37/32009—Arrangements for generation of plasma specially adapted for examination or treatment of objects, e.g. plasma sources
- H01J37/32192—Microwave generated discharge
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/32—Gas-filled discharge tubes
- H01J37/32009—Arrangements for generation of plasma specially adapted for examination or treatment of objects, e.g. plasma sources
- H01J37/32192—Microwave generated discharge
- H01J37/32211—Means for coupling power to the plasma
- H01J37/32229—Waveguides
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/32—Gas-filled discharge tubes
- H01J37/32009—Arrangements for generation of plasma specially adapted for examination or treatment of objects, e.g. plasma sources
- H01J37/32192—Microwave generated discharge
- H01J37/32211—Means for coupling power to the plasma
- H01J37/32238—Windows
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05H—PLASMA TECHNIQUE; PRODUCTION OF ACCELERATED ELECTRICALLY-CHARGED PARTICLES OR OF NEUTRONS; PRODUCTION OR ACCELERATION OF NEUTRAL MOLECULAR OR ATOMIC BEAMS
- H05H1/00—Generating plasma; Handling plasma
- H05H1/24—Generating plasma
- H05H1/46—Generating plasma using applied electromagnetic fields, e.g. high frequency or microwave energy
- H05H1/461—Microwave discharges
- H05H1/4622—Microwave discharges using waveguides
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01P—WAVEGUIDES; RESONATORS, LINES, OR OTHER DEVICES OF THE WAVEGUIDE TYPE
- H01P7/00—Resonators of the waveguide type
- H01P7/06—Cavity resonators
Definitions
- the present invention relates to a cavity resonator provided in a microwave plasma generator that generates plasma using microwaves.
- the manufacturing process of a semiconductor integrated circuit includes a film forming process for forming an insulating film such as a silicon oxide film or a silicon nitride film on a semiconductor wafer.
- a plasma CVD (PECVD) method is widely used for the film forming process.
- PECVD plasma CVD
- solid deposits mainly composed of film-forming components accumulate in the processing container of the semiconductor manufacturing apparatus. If this is left as it is, the accumulated solid deposits peel off from the surface of the processing container. There is a risk of depositing on a semiconductor wafer and causing film formation abnormalities and device defects. For this reason, it is necessary to clean the inside of the processing container according to the frequency of film forming processing.
- a dry cleaning method in which a solid deposit is chemically changed to gaseous silicon tetrafluoride (SiF 4 ) by active fluorine atoms and exhausted and removed is widely used. Then, to generate active fluorine atom, a gas having a fluorine atom is used in the molecule, usually, a method of plasma hexafluoride ethane (C 2 F 6) or nitrogen trifluoride (NF 3) Is used.
- SiF 4 gaseous silicon tetrafluoride
- NF 3 nitrogen trifluoride
- in-situ plasma in which a processing container of a semiconductor manufacturing apparatus also serves as a plasma generation chamber
- remote plasma in which the plasma generation chamber is disposed outside the processing container of the semiconductor manufacturing apparatus.
- remote plasma has advantages such as less damage to the processing vessel of semiconductor manufacturing equipment, better gas decomposition efficiency, and shorter cleaning time. It is suitable for a semiconductor manufacturing apparatus designed for film formation (see, for example, Patent Document 1).
- a microwave plasma generating apparatus that forms plasma using microwave discharge is known.
- a microwave plasma generator for example, a microwave generated by a high-frequency power supply is supplied to a waveguide extending in the microwave cavity, and the microwave cavity is penetrated and extends across the waveguide axis.
- a type in which gas is supplied into a gas carrier tube and the gas is converted into plasma by a discharge generated in the gas carrier tube is known in the prior art (see, for example, Patent Document 2).
- impedance matching is performed so that the power of the microwave is maximized at the position of the gas carrier tube in the microwave cavity, thereby maintaining a standing wave (resonant state) in the waveguide.
- the initial setting of the microwave plasma apparatus is performed. This initial setting is made so that the resonance frequency matches the frequency of the microwave (usually 2.45 GHz, which is one of the frequency bands defined as the ISM band) supplied from the high frequency power source into the waveguide.
- the resonance frequency is affected by the physical characteristics of the gas carrier tube (relative permittivity, diameter, thickness, etc.) and the change in the relative dielectric constant of the plasma due to variations in the plasma density formed in the gas carrier tube.
- the change in the relative permittivity of the gas carrier tube is caused by the erosion of the inner wall surface of the gas carrier tube by plasma ions or radicals. It fluctuates in the size of several tens of MHz under the influence of
- JP 2007-16315 A JP-T-2002-541672
- an object of the present invention is to provide a cavity resonator that can reduce the cost of the apparatus without correcting the fluctuation of the resonance frequency during operation in the microwave plasma generator.
- a microwave plasma generator for generating plasma using microwaves which is a convex polygonal rectangular tube having a line-symmetric cross section, Or a cylindrical side wall, and an upper wall and a lower wall that close the upper end opening and the lower end opening of the side wall, respectively, and a resonator body made of a conductor having a cavity therein, and the side wall of the resonator body includes A microwave supply port is provided, and a reaction tube mounting port is provided in each of the upper wall and the lower wall, and a normal line at a center point of the microwave supply port extends along the symmetry axis of the cross section of the side wall, Further, a waveguide connected to the microwave supply port of the resonator body through an inductive window, and attached to the reaction tube mounting port of the resonator body, penetrating up and down the cavity, The axis of the waveguide and And a dielectric reaction tube extending between the upper wall
- a square cylinder or a cylinder, and the square cylinder or the cylinder has a cross-sectional shape similar to the cross-sectional shape of the cavity, and is disposed coaxially with the resonator body.
- the side surface has a lattice pattern of nonmagnetic metal, and corresponds to the microwave supply port at a position on the side surface between the reaction tube and the microwave supply port and facing the microwave supply port.
- An opening, and the upper end edge and the lower end edge of the rectangular cylinder or the cylinder are joined to the upper wall and the lower wall, respectively, so that the gas flows in the reaction tube.
- Cavity resonator characterized in that it is intended to be plasma by microwave supplied from the microwave supplying port is provided.
- the rectangular cylinder or the cylinder is formed of a lattice or mesh made of nonmagnetic metal.
- the rectangular cylinder or the cylindrical body is formed by covering a surface of a rectangular cylinder or a cylindrical dielectric with a nonmagnetic metal layer in a lattice pattern. It has become.
- a square tube having a convex polygon that is provided in a microwave plasma generator for generating plasma using microwaves and has a line-symmetric cross section.
- a resonator body made of a conductor having a cavity inside, and a microwave on the side wall of the resonator body.
- a supply port is provided, and a reaction tube mounting port is provided in each of the upper wall and the lower wall, a normal line at a center point of the microwave supply port extends along the symmetry axis of the cross section of the side wall, and A waveguide connected to the microwave supply port of the resonator body through an inductive window, and attached to the reaction tube mounting port of the resonator body, vertically passing through the cavity, and Intersects the axis of the tube
- a plurality of partition plates comprising: a dielectric reaction tube extending; and a plurality of partition plates extending between the upper wall and the lower wall and partitioning a space between the reaction tube and an inner surface of the side wall in the cavity.
- the partition plate is nonmagnetic on the entire side surface thereof. It has a metal lattice pattern, the upper edge and the lower edge of the partition plate are joined to the upper wall and the lower wall, respectively, so as to have conductivity, and the gas flowing through the reaction tube supplies the microwave
- a cavity resonator is characterized in that it is turned into plasma by microwaves supplied from the mouth.
- a square tube of a convex polygon having a line-symmetric cross section is provided in a microwave plasma generator for generating plasma using microwaves.
- a resonator body made of a conductor having a cavity inside, and a microwave on the side wall of the resonator body.
- a supply port is provided, and a reaction tube attachment port is provided in each of the upper wall and the lower wall, and a normal line at a center point of the microwave supply port extends along a symmetry axis of a cross section of the side wall, and the resonance A waveguide connected to the microwave supply port of the resonator body through an inductive window, and attached to the reaction tube mounting port of the resonator body, vertically passing through the cavity, Extend across the axis An electric reaction tube, and one or a plurality of partition plates extending between the upper wall and the lower wall and partitioning a space between the reaction tube and the inner surface of the side wall in the cavity, The partition plates are spaced apart from each other in the direction of the symmetry axis and extend perpendicular to the symmetry axes, respectively, and the partition plate has a lattice pattern of nonmagnetic metal on the entire side surface thereof, The upper and lower edges of the partition plate are joined to the upper wall and the lower wall so as to have conductivity, respectively, and
- the partition plate is formed of a lattice or mesh made of nonmagnetic metal.
- the gap between the outermost partition plate and the inner surface of the side wall, and the gap between the partition plates adjacent to each other, A dielectric having a shape corresponding to the gap is disposed.
- the partition plate comprises a plate-like dielectric surface coated with a nonmagnetic metal layer in a lattice pattern.
- the space between the inner surface of the side wall of the resonator body and the reaction tube in the cavity of the resonator body having an axisymmetric convex polygon or circular cross section extends in the axial direction of the resonator body, and the side surface.
- a cavity resonator is provided with a stagger function by partitioning into a plurality of portions coaxially and in a nested manner in the resonator body by at least one rectangular tube or tube having a non-magnetic metal lattice pattern on the cavity resonator.
- the resonance frequency can be widened.
- the space between the inner surface of the side wall of the resonator body and the reaction tube in the cavity of the resonator body having a line-symmetric convex polygonal cross section extends in the axial direction of the resonator body, and is not formed on the side surface.
- the cavity resonator has a stagger function by dividing it into a plurality of parts in a direction perpendicular to the symmetry axis of the cross section of the resonator body by one or more partition plates having a lattice pattern of magnetic metal, and cavity resonance.
- the resonance frequency of the device can be widened.
- the space between the inner wall of the resonator main body and the reaction tube in the cavity of the resonator main body having a cross section of a line-symmetric convex polygonal cross section extends in the axial direction of the resonator main body to the side surface.
- a cavity resonator is provided with a stagger function by partitioning into a plurality of parts in a direction parallel to the symmetry axis of the transverse cross section of the resonator body by one or more partition plates having a lattice pattern of non-magnetic metal.
- the resonance frequency of the resonator can be widened.
- the TE 101 mode electromagnetic field can be maintained in the cavity resonator, and as a result, a high-power microwave is applied to the cavity resonator. As a result, the remote plasma can be generated more efficiently.
- the resonance frequency of the cavity resonator can be widened only by making a relatively simple structural change to the conventional cavity resonator. This eliminates the need for a mechanism for correcting fluctuations in the resonance frequency, thereby reducing the cost of the apparatus.
- FIG. 2 is an enlarged photograph of a nonmagnetic metal mesh used for the rectangular tube of the cavity resonator of FIG. 1. It is a graph which shows the resonant frequency characteristic at the time of removing a square cylinder from the cavity resonator of FIG.
- FIG. 3 is a view similar to FIG. 1B showing a cavity resonator according to another embodiment of the present invention.
- FIG. 6 is a view similar to FIG. 1B showing a cavity resonator according to yet another embodiment of the present invention.
- FIG. 1 illustrates a cavity resonator of a microwave plasma generation apparatus according to an embodiment of the present invention.
- FIG. 1A is a longitudinal sectional view of the cavity resonator, and FIG. It is a cross-sectional view of the cavity resonator along the central axis.
- FIG. 2 is a perspective view illustrating a rectangular tube disposed in the cavity resonator of FIG.
- the cavity resonator according to the present invention includes a rectangular tube-shaped side wall 2 having a rectangular cross section, and an upper wall 3 and a lower wall 4 that close an upper end opening and a lower end opening of the side wall 2, respectively.
- a resonator body 1 made of a conductor having a cavity 5 inside is provided.
- a rectangular microwave supply port 6 is provided on the side wall 2 of the resonator body 1, that is, one of the four rectangular side wall portions 2 a to 2 d constituting the side wall 2.
- the normal line at the center point of the microwave supply port 6 extends along the symmetry axis of the cross section of the side wall 2.
- reaction tube attachment ports 3a and 4a are provided in the upper wall 3 and the lower wall 4 of the resonator body 1, respectively.
- the reaction tube attachment ports 3a and 4a are preferably provided at positions slightly closer to the plasma supply port 6 side than the centers of the upper wall 3 and the lower wall 4, respectively. Thereby, plasma is generated uniformly along the central axis of the reaction tube 8 (described later).
- a waveguide 7 is connected to the microwave supply port 6 via an inductive window (also referred to as “inductive iris”) 13.
- the inductive window 13 includes a pair of diaphragm plates that are provided on both the left and right sides of the microwave supply port 6 and are slidable in a direction perpendicular to the axis of the resonator body 1. And the magnitude
- a dielectric reaction tube 8 (in this embodiment, a quartz tube) is attached to the reaction tube attachment ports 3a and 4a via an annular fixing member 9 so as to penetrate the cavity 5 up and down. , Extending across the axis of the waveguide 7.
- the resonator body 1 also extends between the upper wall 3 and the lower wall 4, and is provided with three rectangular cylinders 10 a arranged in a nested manner at positions spaced from the inner surface of the side wall 2 and the reaction tube 8 in the cavity 5. To 10c.
- FIG. 2A shows one rectangular tube 10a as a representative example of the three rectangular tubes 10a to 10c.
- the rectangular tube body 10a is formed of a non-magnetic metal mesh, and has a cross-sectional shape similar to the cross-sectional shape of the cavity 5 (in this embodiment, a rectangle).
- the mesh has a mesh size smaller than ⁇ / 4 ( ⁇ is the wavelength of the microwave supplied to the resonator body 1), and the mesh opening ratio (ratio of the opening area in the total area of the mesh). It is preferable to have a configuration that is as large as possible.
- the rectangular tube 10a is disposed coaxially with the resonator body 1 and has an opening 11a at a position facing the microwave supply port 6 between the reaction tube 8 and the microwave supply port 6 on the side surface of the rectangular tube 10a. ing.
- the three rectangular cylinders 10a to 10c having different cross-sectional sizes are placed in the cavity 5 of the resonator body 1 coaxially with the resonator body 1, and the respective openings 11a are formed in the microwave supply port 6 (inductive property).
- the upper and lower edges of each of the rectangular cylinders 10a to 10c are electrically conductive to the upper wall 3 and the lower wall 4 of the resonator body 1, respectively. Joined to have.
- the configuration of the rectangular tube bodies 10a to 10c is not limited to this embodiment, and has a cross-sectional shape similar to the cross-sectional shape of the cavity 5, is disposed coaxially with the resonator body 1, and has the entire side surface thereof. As long as it has a lattice pattern made of a non-magnetic metal and has an opening corresponding to the microwave supply port 6 on the side surface, any configuration may be used.
- the entire surface of the rectangular tube 12a made of a highly heat-resistant nonmetallic plate is nonmagnetic.
- What stuck metal piece 12b in the shape of a lattice can also be used.
- the long side of the inner opening of the grating is shorter than ⁇ / 4 ( ⁇ is the wavelength of the microwave supplied to the resonator body 1), and the aperture ratio (the ratio of the opening area in the total area of the grating) is It is preferable that it be as large as possible.
- the rectangular tube may be made of a nonmagnetic metal lattice or punch plate.
- the inner opening of the grating or the punch hole of the punch plate has a long side or diameter size smaller than ⁇ / 4 ( ⁇ is the wavelength of the microwave supplied to the resonator body 1) and an aperture ratio ( It is preferable that the ratio of the open area in the total area of the lattice or punch plate is as large as possible.
- the rectangular tube may be formed by coating the surface of a rectangular tube-shaped dielectric with a nonmagnetic metal layer with a lattice pattern.
- the dimension of each part of the resonator main body 1 is determined as follows.
- the waveguide 7 is a rectangular waveguide, and is usually designed so that the ratio of the length of the long side to the short side of the rectangular cross section is 2: 1.
- the waveguide 7 is connected to the microwave supply port 6 of the resonator body 1 through the inductive window 13 with the short side being parallel to the axis of the resonator body 1. .
- the length of the long side of the waveguide 7 is d
- the wavelength of the microwave in the vacuum is ⁇ 0
- the in-tube wavelength ⁇ g of the waveguide 7 is expressed by a relational expression: Determined by.
- the cavity 5 of the resonator body 1 has a width a along the direction perpendicular to the axis of the waveguide 7, a height b, and a depth c along the axial direction of the waveguide 7.
- the frequency of the microwave supplied to the main body 1 is f 0
- the electromagnetic field mode to be generated in the resonator main body 1 is TE mns
- v 0 is the light velocity
- the size (width a, height b, depth c) of the cavity 5 of the resonator body 1 set by the equation (2) is a numerical value when the reaction tube 8 is not attached. Since the reaction tube 8 is made of a dielectric, when the reaction tube 8 is attached to the resonator body 1, the wavelength of the electromagnetic field in the cavity 5 is shortened from the initial setting value. As a result, the resonance frequency of the resonator body 1 set according to the equation (2) fluctuates, and this fluctuation must be corrected (similar to the case of the above prior art).
- the resonance frequency of the cavity resonator set according to the equation (2) fluctuates, and this fluctuation must be corrected (as in the case of the prior art).
- each of the three rectangular cylinders 10a to 10c partitioning the cavity 5 of the resonator body 1 has a width and a depth as in the resonator body 1 (inner wall inner surface). And having a resonance frequency determined according to equation (2).
- the four resonance frequencies are as follows. In other words, the resonator body 1 has a resonance frequency with a bandwidth of f 4 -f 1 .
- FIG. 3 shows an equivalent circuit of the cavity resonator of FIG.
- the same reference numerals as those in FIG. 1 are assigned to circuit elements corresponding to the components shown in FIG.
- numeral 14 indicates a high-frequency power supply for supplying microwaves.
- the resonator body 1 is magnetically coupled to the waveguide 7 through the inductive window 13. And by optimizing the inductive window 13, the resonator body 1 and the waveguide 7 can be brought into a critically coupled state.
- FIG. 6 is a graph showing the measurement results.
- the vertical axis represents the value of SWR
- the horizontal axis represents the frequency (GHz). Since the numerical range of the horizontal axis of this graph is 2 GHz to 2.5 GHz, one scale on the horizontal axis is 50 MHz.
- FIG. 5 is a graph showing the measurement results.
- the vertical axis represents the value of SWR
- the horizontal axis represents the frequency (GHz). Since the numerical range of the horizontal axis of this graph is 2 to 3 GHz, one scale on the horizontal axis is 100 MHz.
- the SWR curve C1 has a minimum value at the point P0, but in this case, a very narrow peak is formed.
- the SWR curve C2 takes the minimum value at four points (points P1 to P4).
- the point P1, the point P2, the point P3, and the point P4 are respectively the inner surface of the side wall 2 of the resonator body 1, the first rectangular tube 10a, the second rectangular tube 10b, and the third rectangular tube 10c. It was obtained by.
- FIG. 7 is a side view showing an example of the configuration of a microwave plasma generator provided with the cavity resonator of FIG. Since the resonator main body 1 of the present invention has a wide-band resonance frequency as described above, the microwave plasma generator is a waveguide 7 connected to the resonator main body 1 as shown in FIG. Is connected to the high frequency power source 14 and the incident wave power / reflected wave power measuring instrument 15 is arranged in the middle of the waveguide 7.
- reference numerals 16a to 16c denote observation windows for visually confirming whether or not plasma is uniformly generated in the reaction tube 8.
- the inductive window 13 of the cavity resonator is adjusted while observing the measured value by the incident wave power / reflected wave power measuring device 15 before operating the device to generate plasma.
- the size of the opening of the inductive window 13 is set so that the critical coupling state of the resonator body 1 is achieved.
- a microwave is supplied from the high frequency power source 14 to the cavity resonator, and a gas is supplied into the reaction tube 8.
- the TE 101 mode electromagnetic field is maintained in the cavity resonator, and plasma can be generated stably and efficiently in the reaction tube 8.
- the TE 101 mode electromagnetic field can always be maintained in the cavity resonator. It becomes possible to supply a high-power microwave to the resonator and generate remote plasma more efficiently.
- the resonance frequency of the cavity resonator can be widened only by making a relatively simple structural change to the conventional cavity resonator. Since a mechanism for correcting the fluctuation of the resonance frequency that occurs at the time of attachment and plasma generation becomes unnecessary, the configuration of the microwave plasma generator does not become complicated and expensive.
- the resonator body has a rectangular tube-shaped side wall having a rectangular cross section, but as shown in FIG. 9A, the resonator body may have a tube-shaped side wall.
- the resonator body may have a tube-shaped side wall.
- Good Referring to FIG. 9A, when side wall 2 ′ of resonator body 1 ′ has a cylindrical shape, it is spaced from the inner surface of side wall 2 ′ and reaction tube 8 in cavity 5 ′ of resonator body 1 ′. At least one cylindrical body 19a to 19c is arranged coaxially with the resonator body 1 and nested in place of the rectangular cylinder.
- the cylinders 19a to 19c have a cross-sectional shape similar to the cross-sectional shape of the cavity 5 ′, like the rectangular cylinders 10a to 10c shown in FIG. 1, and are arranged coaxially with the resonator body 1 ′. Any configuration may be used as long as it has a lattice pattern made of non-magnetic metal on the entire side surface and has an opening corresponding to the microwave supply port 6 ′ on the side surface.
- the cylinders 19a to 19c extend between the upper and lower walls of the resonator body 1 ', and the upper and lower edges of the cylinders 19a to 19c are electrically conductive to the upper and lower walls of the resonator body 1', respectively. It has joined so that it may have.
- the radius r and the height l of the cavity 5 of the resonator body 1 set the frequency of the microwave supplied to the resonator body 1 to f 0
- the electromagnetic field mode to be generated in the resonator body 1 is TM mns (usually TM 010 mode), and v 0 is the speed of light. Is set to satisfy.
- the outermost rectangular cylinder 10a or the gap between the cylindrical body 19a and the inner surfaces of the side walls 2 and 2 ′, and the adjacent rectangular cylinders 10a and 10b. ; 10b, 10c or cylinders 19a, 19b; 19b, 19c, a dielectric having a shape corresponding to the gap may be disposed in each gap.
- the resonator body 1 has a line-symmetric convex polygonal cross section, as shown in FIGS. 8A and 8B, the resonator body 1 is replaced with the rectangular tubes 10a to 10c.
- the space between the reaction tube 8 and the inner surface of the side wall 2 in the cavity 5 can also be partitioned by one or more partition plates extending in the axial direction.
- the plurality of partition plates 17a to 17c are spaced apart from each other in a direction perpendicular to the symmetry axis of the transverse section of the resonator body 1, and extend parallel to the symmetry axis.
- the partition plates 17a to 17c have a non-magnetic metal lattice pattern on the entire side surfaces thereof, and the upper and lower edges of the partition plates 17a to 17c are electrically connected to the upper wall and the lower wall of the resonator body 1, respectively. It joins so that it may have property.
- both side edges of the partition plates 17a to 17c are located at a distance from the inner surface of the side wall 2.
- partition plates 18a to 18c are spaced apart from each other in the direction of the symmetry axis of the cross section of the resonator body 1 and perpendicular to the symmetry axis. It is Partition plates 18a to 18c have a non-magnetic metal lattice pattern on the entire side surface, and the upper and lower edges of partition plates 18a to 18c are electrically conductive to the upper and lower walls of resonator body 1, respectively. Joined to have. Note that both side edges of the partition plates 18a to 18c are located at a distance from the inner surface of the side wall 2. In this case, the partition plate located between the reaction tube 8 and the microwave supply port 6 is provided with an opening corresponding to the microwave supply port 6 at a position facing the microwave supply port 6.
- the outermost cylinder or square cylinder located in the cavity of the cavity and the gap between the inner surface of the side wall of the cavity and the cylinders adjacent to each other
- dielectrics having shapes corresponding to the gaps are arranged in the gaps between the rectangular cylinders.
- the side wall 2 of the resonator body 1 has a rectangular tube shape with a rectangular cross section.
- the cross section of the rectangular tube side wall 2 is not limited to a rectangular shape, and It can be an arbitrary line-symmetric convex polygon including a polygon.
- FIG. 9B is a view similar to FIG. 1B, showing an example of a configuration in which the cross section of the rectangular tubular side wall is an isosceles trapezoid.
- the axis of symmetry of the cross section of the side wall 2 ′′ is a straight line passing through the midpoints of the upper and lower bases of the isosceles trapezoid, and the side wall 2 ′′ of the resonator body 1 ′′.
- a microwave supply port 6 ′′ is formed on the wall surface forming the bottom of the cross section.
- a pair of partition plates 20a, 20b having a lattice pattern of nonmagnetic metal on the entire side surface are symmetrically arranged with respect to the symmetry axis on both sides in a direction perpendicular to the symmetry axis with the reaction tube 8 interposed therebetween. Yes.
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Abstract
Description
成膜処理においては、半導体製造装置の処理容器内に、膜形成成分を主とする固体状堆積物が蓄積し、これを放置すると、蓄積された固体状堆積物が処理容器表面から剥がれ落ちて半導体ウエハー上に堆積し、成膜異常やデバイスの欠陥を生じさせるおそれがあり、そのため、成膜処理の頻度に応じて処理容器内をクリーニングする必要があった。
マイクロ波プラズマ発生装置としては、例えば、マイクロ波キャビティ内にのびる導波管に、高周波電源で発生させたマイクロ波を供給するとともに、マイクロ波キャビティを貫通し、導波管の軸を横切ってのびるガス搬送管内にガスを供給し、ガス搬送管内に生じさせた放電によってガスをプラズマ化するタイプのものが従来技術において知られている(例えば、特許文献2参照)。
この共振周波数の変動を補正する方法として、例えば、マイクロ波を供給する高周波電源の周波数を可変にすることが考えられる。しかし、この方法によれば、マイクロ波の出力電力を大きくしようとすると、電源装置が複雑で大掛かりなものになって、電源装置の製造コストが増大し、また、高周波電源の周波数を、2.45GHzの上下に数100MHz変動させることは、法律で定められたISMバンドを逸脱することになって好ましくない。
こうして、従来の空洞共振器を備えたマイクロ波プラズマ発生装置において共振周波数の変動を補正しようとすると、マイクロ波プラズマ発生装置が複雑化し、製造コストが増大するという問題があった。
第1発明の別の好ましい実施例によれば、最外側に位置する前記角筒体または前記筒体と前記側壁の内面との間の間隙、および互いに隣接する前記角筒体または前記筒体間の間隙には、それぞれ、当該間隙に対応する形状を有する誘電体が配置されている。
第1発明のさらに別の好ましい実施例によれば、前記角筒体または前記筒体は、角筒状または筒状の誘電体の表面に、非磁性金属層を格子状パターンで被覆したものからなっている。
第2および第3発明の別の好ましい実施例によれば、最外側に位置する前記仕切板と前記側壁の内面との間の間隙、および互いに隣接する前記仕切板間の間隙には、それぞれ、当該間隙に対応する形状を有する誘電体が配置されている。
第2および第3発明のさらに別の好ましい実施例によれば、前記仕切板は、板状の誘電体の表面に、非磁性金属層を格子状パターンで被覆したものからなっている。
また、共振器本体1の上壁3および下壁4にはそれぞれ反応管取付口3a、4aが設けられている。この場合、反応管取付口3a、4aは、それぞれ、上壁3および下壁4の中心よりも少しプラズマ供給口6側に寄った位置に設けられることが好ましい。それによって、反応管8(後述する)の中心軸に沿って均一にプラズマが発生するようになる。
また、反応管取付口3a、4aには、誘電体製の反応管8(この実施例では、石英管)が、環状の固定部材9を介して取り付けられて、空洞5を上下に貫通するとともに、導波管7の軸と交差してのびている。
この場合、メッシュは、メッシュサイズがλ/4(λは共振器本体1に供給されるマイクロ波の波長)よりも小さく、かつメッシュの開口率(メッシュの全面積に占める開口領域の割合)ができるだけ大きくなるような構成を有していることが好ましい。
こうして、横断面のサイズが異なる3つの角筒体10a~10cが、共振器本体1の空洞5内に、共振器本体1と同軸に、それぞれの開口部11aがマイクロ波供給口6(誘導性窓13の開口部)に重なり合うようにして入れ子状に配置され、そして、各角筒体10a~10cの上端縁および下端縁がそれぞれ共振器本体1の上壁3および下壁4に導電性を有するように接合される。
あるいは、例えば、角筒体は、角筒状の誘電体の表面に、非磁性金属層を格子状パターンで被覆したものからなっていてもよい。
導波管7は方形導波管からなっており、通常、その矩形断面の長辺と短辺の長さの比が2:1になるように設計されている。そして、この実施例では、導波管7は、短辺が共振器本体1の軸に平行となる配置で、誘導性窓13を介して共振器本体1のマイクロ波供給口6に接続される。
このとき、導波管7の長辺の長さをd、真空中のマイクロ波の波長をλ0として、導波管7の管内波長λgが、関係式、
関係式
本発明では、共振器本体1内にTE101モードの電磁界が生じるように設定がなされるので、(2)式において、m=1、n=0、s=1に設定される。
反応管8は誘電体製であるため、反応管8が共振器本体1に装着されると、空洞5内の電磁界の波長が初期設定値よりも短縮される。その結果、(2)式に従って設定された共振器本体1の共振周波数が変動し、そして、この変動が補正されなければならない(上記従来技術の場合と同様)。
その結果、共振器本体1内に反応管8を配置しない状態でTE101モードの電磁界が維持されるとしたとき、共振器本体1は、
(1)f1=共振器本体1の側壁2の内面によって得られる共振周波数(最低値)
(2)f2=第1の角筒体10aによって得られる共振周波数
(3)f3=第2の角筒体10bによって得られる共振周波数
(4)f4=第3の角筒体10cによって得られる共振周波数(最高値)
の4つの共振周波数を有している。言い換えれば、共振器本体1はf4-f1の帯域幅の共振周波数を有している。
まず、図1に示したものと同じ構造の空洞共振器を作製した。そして、3つの角筒体10a~10cは、図4に示すような非磁性金属製のメッシュから作製した。
製作製した空洞共振器の各部の寸法は以下のとおりである。
導波管7の長辺の長さ=109.2mm
導波管7の短辺の長さ=54.6mm
共振器本体1の空洞5の幅a0=90mm
共振器本体1の空洞5の高さb0=163.8mm
共振器本体1の空洞5の奥行c0=80mm
第1の角筒体10aの内部空間の幅a1=85mm
第1の角筒体10aの内部空間の奥行c1=75mm
第2の角筒体10bの内部空間の幅a2=79mm
第2の角筒体10bの内部空間の奥行c2=69mm
第3の角筒体10cの内部空間の幅a3=73mm
第3の角筒体10cの内部空間の奥行c3=63mm
誘導性窓13の開口部の大きさ=42mm
反応管(石英管)8の内径=50mm、厚さ=5mm
図6は測定結果を示すグラフである。図6のグラフ中、縦軸はSWRの値を表し、横軸は周波数(GHz)を表している。なお、このグラフの横軸の数値範囲は2GHz~2.5GHzであるので、横軸の1目盛は50MHzである。
図9Aを参照して、共振器本体1’の側壁2’が筒状を有している場合には、共振器本体1’の空洞5’内における側壁2’の内面および反応管8から間隔をあけた位置に、角筒体の代わりに、少なくとも1つの筒体19a~19cが共振器本体1と同軸にかつ入れ子状に配置される。
また、筒体19a~19cは共振器本体1’の上壁および下壁間にのび、筒体19a~19cの上端縁および下端縁はそれぞれ共振器本体1’の上壁および下壁に導電性を有するように接合されている。
この場合、反応管8およびマイクロ波供給口6間に位置する仕切板には、マイクロ波供給口6に対向する位置にマイクロ波供給口6に対応する開口部が設けられる。
図9Bを参照して、この実施例では、側壁2”の断面の対称軸は、等脚台形の上底および下底の各中点を通る直線であり、共振器本体1”の側壁2”断面の下底を形成する壁面にマイクロ波供給口6”が形成されている。そして、側面の全体に非磁性金属の格子状パターンを有する一対の仕切板20a、20bが、反応管8を挟んで上記対称軸に直交する方向の両側に、対称軸に関して対称的に配置されている。
2、2’、2” 側壁
2a、2b 第1の側壁部分
2c、2d 第2の側壁部分
3 上壁
3a 反応管取付口
4 下壁
4a 反応管取付口
5、5’、5” 空洞
6、6’、6” マイクロ波供給口
7 導波管
8 反応管
9 固定部材
10a~10c 角筒体
10a’ 角筒体
11a 開口部
12a~12c 筒体
13 誘導性窓
14 高周波電源
15 入射波電力/反射波電力測定器
16a~16c 観測窓
17a~17c 仕切板
18a~18c 仕切板
19a~19c 筒体
20a、20b 仕切板
Claims (9)
- マイクロ波を利用してプラズマを生成するマイクロ波プラズマ発生装置に備えられるものであって、
断面が線対称な凸多角形の角筒状、または筒状の側壁と、前記側壁の上端開口および下端開口をそれぞれ閉じる上壁および下壁とからなり、内部に空洞を有する導体製の共振器本体を備え、
前記共振器本体の前記側壁にはマイクロ波供給口が設けられ、前記上壁および前記下壁にはそれぞれ反応管取付口が設けられ、前記マイクロ波供給口の中心点における法線が前記側壁の断面の対称軸に沿ってのび、さらに、
前記共振器本体の前記マイクロ波供給口に誘導性窓を介して接続された導波管と、
前記共振器本体の前記反応管取付口に取り付けられ、前記空洞を上下に貫通し、前記導波管の軸と交差してのびる誘電体製の反応管と、
前記上壁および前記下壁間にのび、前記空洞内における前記側壁の内面および前記反応管から間隔をあけた位置に入れ子状に配置された少なくとも1つの角筒体または筒体と、を備え、
前記角筒体または前記筒体は、前記空洞の横断面形状と相似な横断面形状を有していて、前記共振器本体に同軸に配置され、さらに、その側面の全体に非磁性金属の格子状パターンを有するとともに、当該側面における、前記反応管および前記マイクロ波供給口間にあって前記マイクロ波供給口に対向する位置に前記マイクロ波供給口に対応する開口部を有し、前記角筒体または前記筒体の上端縁および下端縁がそれぞれ前記上壁および前記下壁に導電性を有するように接合されており、
前記反応管内を流れるガスが前記マイクロ波供給口から供給されるマイクロ波によってプラズマ化されるものであることを特徴とする空洞共振器。 - 前記角筒体または前記筒体は、非磁性金属製の格子またはメッシュから形成されていることを特徴とする請求項1に記載の空洞共振器。
- 最外側に位置する前記角筒体または前記筒体と前記側壁の内面との間の間隙、および互いに隣接する前記角筒体または前記筒体間の間隙には、それぞれ、当該間隙に対応する形状を有する誘電体が配置されていることを特徴とする請求項1または請求項2に記載の空洞共振器。
- 前記角筒体または前記筒体は、角筒状または筒状の誘電体の表面に、非磁性金属層を格子状パターンで被覆したものからなっていることを特徴とする請求項1に記載の空洞共振器。
- マイクロ波を利用してプラズマを生成するマイクロ波プラズマ発生装置に備えられるものであって、
断面が線対称な凸多角形の角筒状の側壁と、前記側壁の上端開口および下端開口をそれぞれ閉じる上壁および下壁とからなり、内部に空洞を有する導体製の共振器本体を備え、
前記共振器本体の前記側壁にはマイクロ波供給口が設けられ、前記上壁および前記下壁にはそれぞれ反応管取付口が設けられ、前記マイクロ波供給口の中心点における法線が前記側壁の断面の対称軸に沿ってのび、さらに、
前記共振器本体の前記マイクロ波供給口に誘導性窓を介して接続された導波管と、
前記共振器本体の前記反応管取付口に取り付けられ、前記空洞を上下に貫通し、前記導波管の軸と交差してのびる誘電体製の反応管と、
前記上壁および前記下壁間にのび、前記空洞における前記反応管および前記側壁の内面間の空間を仕切る複数の仕切板と、を備え、
前記複数の仕切板は、前記対称軸に直交する方向に互いに間隔をあけて、それぞれ前記対称軸に平行にのびるとともに、前記対称軸に関して対称的に配置され、さらに、前記仕切板は、その側面の全体に非磁性金属の格子状パターンを有し、前記仕切板の上端縁および下端縁がそれぞれ前記上壁および前記下壁に導電性を有するように接合されており、
前記反応管内を流れるガスが前記マイクロ波供給口から供給されるマイクロ波によってプラズマ化されるものであることを特徴とする空洞共振器。 - マイクロ波を利用してプラズマを生成するマイクロ波プラズマ発生装置に備えられるものであって、
断面が線対称な凸多角形断面の角筒状の側壁と、前記側壁の上端開口および下端開口をそれぞれ閉じる上壁および下壁とからなり、内部に空洞を有する導体製の共振器本体を備え、
前記共振器本体の前記側壁にはマイクロ波供給口が設けられ、前記上壁および前記下壁にはそれぞれ反応管取付口が設けられ、前記マイクロ波供給口の中心点における法線が前記側壁の断面の対称軸に沿ってのび、さらに、
前記共振器本体の前記マイクロ波供給口に誘導性窓を介して接続された導波管と、
前記共振器本体の前記反応管取付口に取り付けられ、前記空洞を上下に貫通し、前記導波管の軸と交差してのびる誘電体製の反応管と、
前記上壁および前記下壁間にのび、前記空洞における前記反応管および前記側壁の内面間の空間を仕切る1つまたは複数の仕切板と、を備え、
前記複数の仕切板は、前記対称軸の方向に互いに間隔をあけて、それぞれ前記対称軸に直交してのび、さらに、前記仕切板は、その側面の全体に非磁性金属の格子状パターンを有し、前記仕切板の上端縁および下端縁がそれぞれ前記上壁および前記下壁に導電性を有するように接合されており、さらに、前記反応管および前記マイクロ波供給口間に位置する前記仕切板には、前記マイクロ波供給口に対向する位置に前記マイクロ波供給口に対応する開口部が設けられており、
前記反応管内を流れるガスが前記マイクロ波供給口から供給されるマイクロ波によってプラズマ化されるものであることを特徴とする空洞共振器。 - 前記仕切板は、非磁性金属製の格子またはメッシュから形成されていることを特徴とする請求項5または請求項6に記載の空洞共振器。
- 最外側に位置する前記仕切板と前記側壁の内面との間の間隙、および互いに隣接する前記仕切板間の間隙には、それぞれ、当該間隙に対応する形状を有する誘電体が配置されていることを特徴とする請求項5または請求項6に記載の空洞共振器。
- 前記仕切板は、板状の誘電体の表面に、非磁性金属層を格子状パターンで被覆したものからなっていることを特徴とする請求項5または請求項6に記載の空洞共振器。
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- 2013-05-27 WO PCT/JP2013/064641 patent/WO2014192062A1/ja active Application Filing
- 2013-05-27 US US14/397,516 patent/US9526160B2/en active Active
- 2013-05-27 KR KR1020147027318A patent/KR101614028B1/ko active IP Right Grant
- 2013-05-27 JP JP2013548674A patent/JP5458427B1/ja not_active Expired - Fee Related
- 2013-11-22 TW TW102142616A patent/TWI528870B/zh not_active IP Right Cessation
Patent Citations (2)
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JPH01309972A (ja) * | 1988-06-07 | 1989-12-14 | Fujitsu Ltd | 薄膜形成装置 |
JPH0262650U (ja) * | 1988-10-31 | 1990-05-10 |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2017205034A2 (en) | 2016-05-27 | 2017-11-30 | Mks Instruments, Inc. | Compact microwave plasma applicator utilizing conjoining electric fields |
KR20190002529A (ko) * | 2016-05-27 | 2019-01-08 | 엠케이에스 인스트루먼츠, 인코포레이티드 | 결합 전기장을 이용한 소형 마이크로파 플라즈마 어플리케이터 |
JP2019517707A (ja) * | 2016-05-27 | 2019-06-24 | エム ケー エス インストルメンツ インコーポレーテッドMks Instruments,Incorporated | 電場結合を用いる小型マイクロ波プラズマ照射装置 |
EP3465728A4 (en) * | 2016-05-27 | 2020-01-01 | MKS Instruments, Inc. | COMPACT MICROWAVE PLASPLICATOR WITH CONNECTING ELECTRICAL FIELDS |
KR102378924B1 (ko) | 2016-05-27 | 2022-03-28 | 엠케이에스 인스트루먼츠, 인코포레이티드 | 결합 전기장을 이용한 소형 마이크로파 플라즈마 어플리케이터 |
JP2021072221A (ja) * | 2019-10-31 | 2021-05-06 | 日本無線株式会社 | マイクロ波加熱装置 |
JP7253481B2 (ja) | 2019-10-31 | 2023-04-06 | 日本無線株式会社 | マイクロ波加熱装置 |
Also Published As
Publication number | Publication date |
---|---|
TWI528870B (zh) | 2016-04-01 |
US20160157330A1 (en) | 2016-06-02 |
KR101614028B1 (ko) | 2016-04-20 |
JPWO2014192062A1 (ja) | 2017-02-23 |
US9526160B2 (en) | 2016-12-20 |
JP5458427B1 (ja) | 2014-04-02 |
KR20150013437A (ko) | 2015-02-05 |
TW201446080A (zh) | 2014-12-01 |
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