WO2014119955A1

WO2014119955A1 - Batch deposition apparatus

Info

Publication number: WO2014119955A1
Application number: PCT/KR2014/000900
Authority: WO
Inventors: 연세훈; 이유진; 이재학
Original assignee: 주식회사 티지오테크
Priority date: 2013-02-01
Filing date: 2014-02-03
Publication date: 2014-08-07

Abstract

The present invention relates to a batch deposition apparatus. According to an embodiment of the present invention, which includes: a chamber for providing a space for depositing a layer on a plurality of substrates; a heater arranged on the outside of the chamber for heating the plurality of substrates; a substrate support arranged on the inside of the chamber for supporting the plurality of substrates; a process gas supply part arranged on the inside of the chamber through the center of the substrate support for supplying a process gas to the plurality of substrates; an exhaust gas part for discharging the process gas; and a process gas generation part arranged on the inside of the chamber for providing the process gas supply part with a first process gas generated by reacting a metal of a metal source with a gas containing a halogen.

Description

Batch Deposition Layer Forming Device

The present invention relates to a batch deposition layer forming apparatus. More specifically, the present invention relates to a batch deposition layer forming apparatus capable of stably supplying a metal halide gas.

Light Emitting Diodes (LEDs) are semiconductor light emitting devices that convert current into light and have been widely used as light sources for display images of electronic devices including information and communication devices. In particular, unlike conventional lighting such as incandescent lamps, fluorescent lamps, it is known that the efficiency of converting electrical energy into light energy can be saved up to 90%, and it is widely used as a device that can replace fluorescent lamps or incandescent bulbs. I am getting it.

The manufacturing process of such an LED device can be largely classified into an epi process, a chip process, and a package process. The epitaxial process refers to a process for epitaxial growth of a compound semiconductor on a substrate, and the chip process refers to a process of manufacturing an epi chip by forming electrodes on each part of the epitaxially grown substrate. It refers to a process of connecting leads to the manufactured epi chip and packaging so that light is emitted to the outside as much as possible.

Among these processes, the epi process is the most important process for determining the luminous efficiency of the LED device. This is because when the compound semiconductor is not epitaxially grown on the substrate, defects occur in the crystal and these defects act as nonradiative centers, thereby lowering the luminous efficiency of the LED device.

In such an epitaxial process, that is, a process of forming an epitaxial layer on a substrate, a liquid phase epitaxy (LPE), a vapor phase epitaxy (VPE), a molecular beam epitaxy (MBE), and a chemical vapor deposition (CVD) method are used. Among them, metal-organic chemical vapor deposition (MOCVD) or hydride vapor phase epitaxy (HVPE) is mainly used.

For this process, a process gas supply for supplying the process gas necessary for causing a reaction to form an epitaxial layer on the substrate is included in the apparatus for forming the epitaxial layer, wherein the process gas supply includes the process gas. It is most important to supply stably. In order to form the epitaxial layer, GaCl gas is supplied through the process gas supply unit as one of the process gases, and GaCl has a property of liquefying or condensing at 600 ° C or lower. Therefore, the temperature of the process gas supply unit for supplying GaCl should be maintained at a high temperature exceeding 600 ° C. In the conventional epitaxial layer forming apparatus, since the process gas supply unit is disposed outside the chamber, the temperature of the process gas supply unit is maintained at a high temperature. There was a difficulty in maintaining. Therefore, GaCl is liquefied or condensed in the process gas supply part, so that GaCl gas is not stably supplied into the chamber.

The present invention has been made to solve the above-mentioned problems of the prior art, and an object thereof is to provide a process gas reaction apparatus capable of stably supplying a supply gas and a batch epitaxial layer forming apparatus including the same.

In order to achieve the above object, a batch deposition layer forming apparatus according to an embodiment of the present invention, a batch deposition layer forming apparatus for forming a deposition layer on a plurality of substrates, the space in which the deposition layer is formed A chamber providing a; A heater disposed outside the chamber to apply heat to a plurality of substrates; A substrate support disposed inside the chamber and in which the plurality of substrates are seated; A process gas supply unit arranged to penetrate a center of the substrate support inside the chamber and supply process gas to the plurality of substrates; A process gas exhaust unit configured to exhaust the process gas; And a process gas generating unit disposed inside the chamber and generating a first process gas by reacting a metal in the metal source with a halogen-containing gas, and supplying the first process gas to the process gas supply unit. .

According to the present invention, it is possible to form an epitaxial layer uniformly on a plurality of substrates.

1 is a view showing the configuration of a batch deposition layer forming apparatus according to an embodiment of the present invention.

2 is a cross-sectional view illustrating a structure of a process gas supply unit according to an exemplary embodiment of the present invention.

3 is a cross-sectional view illustrating a structure of a process gas generating unit according to an embodiment of the present invention.

DETAILED DESCRIPTION The following detailed description of the invention refers to the accompanying drawings that show, by way of illustration, specific embodiments in which the invention may be practiced. These embodiments are described in sufficient detail to enable those skilled in the art to practice the invention. It should be understood that the various embodiments of the present invention are different but need not be mutually exclusive. For example, certain shapes, structures, and characteristics described herein may be embodied in other embodiments without departing from the spirit and scope of the invention with respect to one embodiment. In addition, it is to be understood that the location or arrangement of individual components within each disclosed embodiment may be changed without departing from the spirit and scope of the invention. The following detailed description, therefore, is not to be taken in a limiting sense, and the scope of the present invention is defined only by the appended claims, along with the full range of equivalents to which such claims are entitled. Like reference numerals in the drawings refer to the same or similar functions throughout the several aspects.

[Preferred Embodiments of the Invention]

Hereinafter, the configuration of the present invention will be described in detail with reference to the accompanying drawings.

First, the material of the substrate 10 loaded in the batch deposition layer forming apparatus is not particularly limited, and the substrate 10 may be loaded with various materials, such as glass, plastic, polymer, silicon wafer, stainless steel, and sapphire. Hereinafter, a circular sapphire substrate 10 used in the light emitting diode field will be described.

Referring to FIG. 1, a batch deposition layer forming apparatus according to an embodiment of the present invention includes a chamber 110. The chamber 110 may be configured to substantially seal the internal space during the process to provide a space for forming a deposition layer (epitaxial layer) on the plurality of substrates 10. The chamber 110 is configured to maintain optimal process conditions, and the shape may be manufactured in a square or circular shape. The material of the chamber 110 is preferably quartz, but is not necessarily limited thereto.

Referring to FIG. 1, the batch deposition layer forming apparatus according to an embodiment of the present invention may include a heater 120. The heater 120 may be installed outside the chamber 110 to perform a function of applying heat required in an epitaxial process to the plurality of substrates 10. In order to achieve smooth epitaxial growth on the substrate 10, the heater 120 may heat the substrate 10 to a temperature of about 1,200 ° C. or more.

In the present invention, a heating method using a halogen lamp or a resistive heating element may be used to heat the substrate 10, but preferably an induction heating method may be used. Induction heating refers to a method of heating a conductive object such as a metal by using electromagnetic induction. In order to use the induction heating method, the heater 120 includes a coil-type heater 120 capable of induction heating the inside of the chamber 110, and the susceptor 133 installed on the substrate support 131 includes a conductive material. Can be configured. The heating of the substrate 10 using the coil heater 120 is based on the principle that the susceptor 133 including a conductive material is heated as a high frequency alternating current is applied from the coil heater 120 into the chamber 110. Can be implemented.

When the substrate 10 is heated using the induction heating method as described above, components of the batch deposition layer forming apparatus except for the susceptor 133 may be formed of non-conductors (eg, quartz). Accordingly, only the susceptor 133 is heated by the coil heater 120, thereby minimizing deposition of deposition material on the remaining components inside the chamber 110.

Referring to FIG. 1, the batch deposition layer forming apparatus according to an embodiment of the present invention may include a lower support 130. The lower supporter 130 may be installed inside the chamber 110 to support a plurality of substrates 10 during the epitaxial process.

The lower support 130 may be configured to be rotatable in the chamber 110. In order to enable rotation of the lower support 130, various known rotation driving means may be employed in the lower support 130. As the lower support 130 is rotated in the chamber 110, the substrate support 131, which is a component of the lower support 130, also rotates, so that the process gas is supplied in an unbiased position to the substrate 10. Can be prevented. As a result, the process gas can be more uniformly supplied on the plurality of substrates 10.

Referring to FIG. 1, the lower supporter 130 may include a substrate support 131 on which the substrate 10 is mounted. As shown, the substrate support 131 is preferably configured in the form of a disc for smooth rotation of the lower support 130, but is not necessarily limited thereto.

Referring to FIG. 1, the substrate support 131 may be installed to be arranged in a plurality of layers. In this case, the substrate support 131 of the plurality of layers may be connected and fixed to each other by the connection member 132. Although the substrate support 131 is illustrated as having six layers in FIG. 1, the substrate support 131 is not necessarily limited thereto. The number of layers of the substrate support 131 may be variously changed according to the purpose of the present invention. The material of the substrate support 131 is preferably quartz, but is not necessarily limited thereto.

As described later, in the present invention, the process gas supply unit 140 supplies the process gas in a state where the process gas supply unit 140 penetrates the center of the substrate support 131 of the lower support unit 130. In this case, as the process gas is supplied from the center of the substrate support 131, a problem may occur in that more process gas is supplied to a position on the substrate 10 close to the center of the substrate support 131. In order to solve this problem, the plurality of substrates 10 mounted on the substrate support 131 may be independently rotated. In other words, while the epitaxial process is performed, each substrate 10 may be rotated in a horizontal direction with respect to the substrate support 131, but may be rotated at different rotational speeds or different rotational directions. This independent rotation of the substrate 10 may be made by the rotation of the susceptor 133 on which the substrate 10 is seated. As the substrate 10 rotates independently, the process gas can be uniformly supplied onto the plurality of substrates 10.

Referring to FIG. 1, each of the substrate supports 131 may be provided with a plurality of susceptors 133. The susceptor 133 may support the substrate 10 during the epitaxial process to prevent deformation of the substrate 10. The number of susceptors 133 installed on each substrate support 131 may be the same as the number of substrates 10 disposed on each substrate support 131.

In addition to the function of preventing deformation of the substrate 10, the susceptor 133 may perform a function of heating the substrate 10 together with the coil type heater 120. To this end, the material of the susceptor 133 may include a conductive material, for example, amorphous carbon, diamondlike carbon, glasslike carbon, or the like, preferably graphite. (Graphite). Graphite is not only excellent in strength but also excellent in conductivity and may be suitable for heating by induction heating. As such, when the susceptor 133 is made of graphite, the surface of graphite may be coated with silicon carbide (SiC). Since silicon carbide has excellent high temperature strength and hardness and high thermal conductivity, it is possible not only to prevent graphite molecules from dispersing during heating, but also to facilitate heat transfer to the substrate 10.

The susceptor 133 may perform a function of preventing rotation of the substrate 10 and rotating (rotating) the substrate 10 as described above, in addition to preventing deformation of the substrate 10 and heating the substrate 10. To this end, various known rotation drive means may be employed in the susceptor 133. In addition, the susceptor 133 preferably has the shape of a disc for smooth rotation, but is not necessarily limited thereto, and may have various shapes according to the object of the present invention.

Referring to FIG. 1, the batch deposition layer forming apparatus according to an embodiment of the present invention may include a process gas supply unit 140. The process gas supply unit 140 may perform a function of supplying a process gas necessary for forming an epitaxial layer into the chamber 110.

As shown in FIG. 1, in the present invention, the process gas supply unit 140 is disposed to penetrate the center of the substrate support 131. In other words, the process gas supply unit 140 is disposed to penetrate the through hole 135 formed in the center of the substrate support 131, so that the process gas supply unit 140 is supported by the substrate support 131 from the center of the substrate support 131. The supply of the process gas towards the substrate 10 is characterized by its configuration. By adopting such a configuration, in the present invention, the process gas can be uniformly supplied to the plurality of substrates 10, and thus the epitaxial layer having the same quality and standard can be formed on the plurality of substrates 10. FIG.

In addition, the process gas supply unit 140 may be rotated while the epitaxial process is in progress. In order to rotate the process gas supply unit 140, various known rotation driving means may be employed in the process gas supply unit 140. Accordingly, similar to the rotation of the lower support 130, it is possible to prevent the process gas from being supplied unevenly to any position of each substrate 10. As a result, the process gas can be more uniformly supplied on the plurality of substrates 10.

Hereinafter, the structure of the process gas supply unit 140 used in the batch deposition layer forming apparatus 100 according to an embodiment of the present invention will be described in detail.

2 is a cross-sectional view showing the structure of a process gas supply unit 140 according to an embodiment of the present invention.

Referring to FIG. 2, the process gas supply unit 140 may be configured in a multi-pipe structure including a first inner tube 142 and a second inner tube 147 in the exterior 141. In the present exemplary embodiment, the number of the first inner tubes 142 is illustrated as four, but is not limited thereto, and may be variously changed according to the purpose and situation of use. The process gas supply unit 140 may include a plurality of gas injection holes 143 and 145. The plurality of gas injection holes 143 and 145 may perform a function of injecting first and second process gases. Positions of the plurality of gas injection holes 143 and 145 may be formed to correspond to positions of the respective substrate supports 131. The number of gas injection holes is not particularly limited and may be variously changed according to the object of the present invention.

Here, the plurality of gas injection holes 143 and 145 are connected to the plurality of first gas injection holes 143 and the appearance 141 of the process gas supply unit 140 connected to the first inner tube 142 of the process gas supply unit 140. It can be seen as a meaning including a plurality of second gas injection holes 145. In the present exemplary embodiment, the first gas injection hole 143 may inject a process gas into a hole formed at an end of the nozzle in the form of a nozzle formed on an outer wall of the first inner tube 142. The first gas injection hole 143 may penetrate the hole 144 formed in the external appearance 141, and an end portion of the first gas injection hole 143 through which the process gas is injected may be exposed to the outside of the external appearance 141. have. In addition, the second gas injection hole 145 is in the form of a hole formed in the exterior 141, and a space occupied by the first inner tube 142 and the second inner tube 147 of the exterior 141 through the second gas injection hole 145. Process gas supplied to the internal space 146 except for may be injected to the outside. However, the shapes of the first and second gas injection holes 143 and 145 are not limited thereto, and various modifications are possible.

Meanwhile, the process gases supplied on the plurality of substrates 10 may be variously changed according to the type of epitaxial layer to be formed on the substrate 10 or the method of forming the epitaxial layer. For example, in order to form an epitaxial gallium nitride (GaN) layer on the plurality of substrates 10 by using the MOCVD method, trimethylgallium (TMG), triethylgallium (TEG), NH 3 gas, or the like may be used as the process gas. have. In addition, in order to form an epitaxial gallium nitride (GaN) layer on the plurality of substrates 10 using the HVPE method, GaCl, NH 3, H 2 gas, etc., generated by reacting Ga metal with HCl gas, may be used as the process gas. Can be.

The process gas supply unit 140 used in the batch deposition layer forming apparatus according to an exemplary embodiment of the present invention may process process gas injected from the first gas injection hole 143 and process gas injected from the second gas injection hole 145. It is desirable to make them different. For example, in order to form an epitaxial gallium nitride layer on the plurality of substrates 10 using the MOCVD method, the first gas injection port 143 injects a TMG gas or a TEG gas, and the second gas injection port 145. ) Can be injected with NH3 gas. According to the process gas supply part 140 of the present invention, since each of the plurality of process gases is injected through the first gas injection port 143 and the second gas injection port 145, the process gas supply part before the process gas reaches the substrate ( Reaction with each other in the 140 may prevent the deposition material from being deposited on the inner wall of the process gas supply unit 140.

The second inner tube 147 is positioned in the center of the outer shell 141 and is used to provide a halogen-containing gas (eg, HCl) to the process gas generator 160 to be described later.

Referring to FIG. 1, a batch deposition layer forming apparatus according to an exemplary embodiment of the present invention may include a process gas exhaust unit 150. The process gas exhaust unit 150 may perform a function of exhausting the process gas to the outside of the chamber 110. The process gas exhaust unit 150 may be formed in a cylindrical shape surrounding the periphery of the plurality of substrate supports 131. A plurality of exhaust ports 155 for exhausting the process gas may be formed at a height corresponding to each of the substrate supports 131 in the process gas exhaust unit 150. The exhaust port 155 may be formed in a slit shape, but the shape is not limited thereto. In addition, the number of exhaust ports 155 may be variously changed according to the purpose of the present invention is used.

A suction means for sucking the process gas is connected to the outside of the process gas exhaust unit 150 to exhaust the process gas to the outside through the exhaust port 155. The exhaust port 155 is preferably located near the substrate support 131. By employing such a configuration, the flow of the process gas, that is, the process gas injected from the first and second

gas injection ports

143 and 145 is formed to flow directly into the exhaust port 155 without circulating inside the chamber 110. As a result, it is possible to minimize the supply of the process gas in excess of the amount required for the process to the substrate 10. As a result, the process gas can be more uniformly supplied on the plurality of substrates 10. The exhaust ports 155 may be disposed at regular intervals from each other in the horizontal direction for uniform flow of the process gas.

Referring to FIG. 1, a batch deposition layer forming apparatus according to an exemplary embodiment of the present invention may include a process gas generator 160. The process gas generator 160 may be formed in the chamber 110, and may be located at an upper portion of the chamber 110. Therefore, the metal halogen gas generated in the process gas generator 160 may be supplied downward from the top of the process gas supply unit 140. In the process gas generator 160, a metal source (eg, Ga source) and a halogen-containing gas (eg, HCl) react to generate a metal halogen gas (eg, GaCl), which is one of the process gases. . The generated metal halide gas is supplied to the process gas supply unit 140. The specific structure of the process gas generator 160 will be described later.

Referring to FIG. 1, a batch deposition film forming apparatus according to an embodiment of the present invention may include a baffle unit 170. The baffle unit 170 may be positioned below the substrate support 131 to block the heat generated in the chamber 110 from leaking to the outside. In particular, the baffle unit 170 may prevent the heat from flowing out through the lower support 130. You can block.

Referring to FIG. 1, the batch deposition film forming apparatus according to an embodiment of the present invention may be configured such that the rotating unit 180 is positioned. The rotating unit 180 may rotate the process gas supply unit 140 and may be positioned below the process gas supply unit 140.

3 is a cross-sectional view illustrating a structure of a process gas generator 160 according to an embodiment of the present invention.

Referring to FIG. 3, the process gas generating unit 160 includes an inflow passage 161 through which a halogen-containing gas such as HCl supplied from the second inner tube 147 passes and a halogen-containing gas supplied from the inflow passage 161. A metal source containing a metal source 163 reacting with a halogen-containing gas passing through the first communication unit 162a, the second communication unit 162b connected to the first communication unit 162a, and the second communication unit 162b. The storage unit 166 and the discharge path 164 for supplying the metal halogen gas generated by the reaction between the metal source 163 and the halogen-containing gas to the first inner tube 142 may be included.

The halogen-containing gas supplied upward through the second inner tube 147 of the supply gas supply unit 140 may be supplied into the process gas generator 160 through the inlet passage 161. The halogen-containing gas supplied into the process gas generator 160 may be supplied to the metal source 163 through the first communicator 162a and the second communicator 162b. The metal source 163 may be, for example, a Ga source. The supply gas generating unit 160 may have a cylindrical shape, and the first communicating unit 162a and the second communicating unit 162b may be supplied from the inlet passage 161 located in the center of the supply gas generating unit 160. The halogen-containing gas may flow along the outer circumference of the generation unit 160 to reach the metal source 163. By such a configuration, the area and time of the halogen-containing gas in contact with the metal source 163 can be increased, as compared with the case where the halogen-containing gas is in contact with the metal source 163 immediately after the inflow path 161 is introduced. Thus, according to one embodiment of the present invention, the probability that the halogen-containing gas reacts with the metal in the metal source 163 to become a metal halogen gas can be increased. In addition, since the metal source 163 is located inside the chamber 110 maintained at a high temperature by the heater 120, there is no need to use a separate heater to maintain a temperature for the reaction between the halogen-containing gas and the metal and the reaction. Easy temperature control

The halogen-containing gas supplied to the metal source 163 reacts with the metal included in the metal source 163 to generate a metal halogen gas, and the generated metal halogen gas is discharged through the discharge passage 164 to the first inner tube 142. Can be supplied. The halogen-containing gas flowing along the outer circumference of the process gas generator 160 reacts with the metal source 163 to form the first inner tube 142 located at the center side of the supply gas generator 160. A discharge path 164 may be formed in the supply gas generating unit 160 so that the discharge path 164 may flow. Since the discharge path 164 for supplying the metal halogen gas to the process gas supply unit 140 is located inside the chamber 110, the metal halogen gas may be prevented from liquefying or condensing in the discharge path 164. The metal halogen gas supplied to the first inner tube 142 may be injected down the inside of the first inner tube 142 and injected into the plurality of substrates 10 through the first gas injection hole 143.

Meanwhile, in order to form the inflow path 161, the first communication unit 162a, the second communication unit 162b, and the discharge path 164, the block 165 may be disposed in the supply gas generator 160. Can be. That is, the block 165 may be disposed in the supply gas generator 160 so that a gap is formed between the inner surface of the supply gas generator 160 and the block 165, and the gap is introduced according to the formed position. The furnace 161, the first communication unit 162a, the second communication unit 162b, and the discharge path 164 may be provided.

According to the present invention, the metal source 163 for generating the metal halide gas and the discharge passage 164 for supplying the metal halide gas to the process gas supply unit 140 may be located inside the chamber 110. Therefore, unlike the conventional deposition layer forming apparatus in which the element supplying the metal halogen gas is located outside the chamber, it is not necessary to separately include a heater for maintaining the reaction temperature of the metal source 163. It is easy to control the reaction temperature of the 163, it is possible to prevent the phenomenon that the metal halide gas flowing along the discharge path 164 liquefied or condensed by the low temperature. Therefore, the metal halogen gas can be stably supplied to the process gas supply unit 140.

Although the present invention has been shown and described with reference to preferred embodiments as described above, it is not limited to the above embodiments and various modifications made by those skilled in the art without departing from the spirit of the present invention. Modifications and variations are possible. Such modifications and variations are intended to fall within the scope of the invention and the appended claims.

[Description of the code]

110: chamber

120: heater

130: lower support

140: process gas supply

150: process gas exhaust

160: process gas generating unit

Claims

A batch deposition layer forming apparatus for forming a deposition layer on a plurality of substrates,

A chamber providing a space in which the deposition layer is formed;

A heater disposed outside the chamber to apply heat to a plurality of substrates;

A substrate support disposed inside the chamber and in which the plurality of substrates are seated;

A process gas supply unit arranged to penetrate a center of the substrate support inside the chamber and supply process gas to the plurality of substrates;

A process gas exhaust unit configured to exhaust the process gas; And

A process gas generation unit disposed inside the chamber to generate a first process gas by reacting a metal in the metal source with a halogen-containing gas, and supplying the first process gas to the process gas supply unit;

Batch deposition layer forming apparatus comprising a.
The method of claim 1,

The process gas generating unit is a batch deposition layer forming apparatus, characterized in that located on top of the process gas supply.
The method of claim 2,

The process gas supply unit includes a first inner tube and a second inner tube,

The halogen-containing gas to be supplied to the process gas generating unit flows through the second inner tube toward the process gas generating unit, and the first process gas supplied from the process gas generating unit flows through the first inner tube. Batch deposition layer forming apparatus.
The method of claim 3,

The process gas generating unit,

An inflow path for introducing the halogen-containing gas flowing in the second inner tube into the process gas generating unit;

A communication unit for guiding the halogen-containing gas introduced through the inflow path to a metal source;

A metal source storage for storing the metal source; And

A discharge path for discharging the first process gas generated by the reaction of the halogen-containing gas and the metal in the metal source to the first inner tube

Batch deposition layer forming apparatus comprising a.
The method of claim 4, wherein

And the communication unit is formed such that the halogen-containing gas introduced from the inflow passage flows along an outer circumference of the process gas generating unit to reach the metal source.
The method of claim 5,

And a block is disposed in the process gas generating unit to form the inflow passage, the communication portion, and the discharge passage.
The method of claim 3,

The process gas supply unit is supplied through a first gas injection hole for injecting the first process gas supplied through the first inner tube, and a space excluding the space occupied by the first inner tube and the second inner tube in the outer tube. And a second gas injection hole for injecting a second process gas.
The method of claim 7, wherein

And the first gas injection hole passes through a hole formed in the exterior as a nozzle formed on the outer wall of the inner tube, and an end portion of the first gas injection port is exposed to the outside of the exterior.
The method of claim 7, wherein

The second gas injection hole is a batch deposition layer forming apparatus, characterized in that the hole shape formed in the outer appearance.
The method of claim 7, wherein

And the first and second process gases are different from each other.
The method of claim 3,

The first inner tube is a plurality of batch deposition layer forming apparatus, characterized in that.