WO2011074918A3 - 폴리아크릴로니트릴계 중합체 용액，그 제조방법，탄소섬유 전구체 섬유，탄소섬유 전구체 섬유의 제조방법 및 탄소섬유의 제조방법 - Google Patents

폴리아크릴로니트릴계 중합체 용액，그 제조방법，탄소섬유 전구체 섬유，탄소섬유 전구체 섬유의 제조방법 및 탄소섬유의 제조방법 Download PDF

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Publication number
WO2011074918A3
WO2011074918A3 PCT/KR2010/009085 KR2010009085W WO2011074918A3 WO 2011074918 A3 WO2011074918 A3 WO 2011074918A3 KR 2010009085 W KR2010009085 W KR 2010009085W WO 2011074918 A3 WO2011074918 A3 WO 2011074918A3
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WO
WIPO (PCT)
Prior art keywords
carbon fiber
manufacturing
fiber
poly
polymer solution
Prior art date
Application number
PCT/KR2010/009085
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English (en)
French (fr)
Other versions
WO2011074918A2 (ko
Inventor
조은정
윤준영
한인식
Original Assignee
코오롱인더스트리 주식회사
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 코오롱인더스트리 주식회사 filed Critical 코오롱인더스트리 주식회사
Priority to US13/521,081 priority Critical patent/US9212236B2/en
Priority to CN201080063613.XA priority patent/CN102753589B/zh
Publication of WO2011074918A2 publication Critical patent/WO2011074918A2/ko
Publication of WO2011074918A3 publication Critical patent/WO2011074918A3/ko

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F20/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride, ester, amide, imide or nitrile thereof
    • C08F20/02—Monocarboxylic acids having less than ten carbon atoms, Derivatives thereof
    • C08F20/42—Nitriles
    • C08F20/44—Acrylonitrile
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L33/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • C08L33/18—Homopolymers or copolymers of nitriles
    • C08L33/20—Homopolymers or copolymers of acrylonitrile
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
    • D01F6/02—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D01F6/18—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolymers obtained by reactions only involving carbon-to-carbon unsaturated bonds from polymers of unsaturated nitriles, e.g. polyacrylonitrile, polyvinylidene cyanide
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
    • D01F6/28—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from copolymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D01F6/38—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from copolymers obtained by reactions only involving carbon-to-carbon unsaturated bonds comprising unsaturated nitriles as the major constituent
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
    • D01F6/44—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds as major constituent with other polymers or low-molecular-weight compounds
    • D01F6/54—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds as major constituent with other polymers or low-molecular-weight compounds of polymers of unsaturated nitriles
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
    • D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
    • D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
    • D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
    • D01F9/20—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products
    • D01F9/21—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D01F9/22—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from polyacrylonitriles

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Organic Chemistry (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Toxicology (AREA)
  • Inorganic Fibers (AREA)
  • Artificial Filaments (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)

Abstract

본 발명은 용매와 미반응 원료 단량체의 회수율을 높일 수 있어 제조비용을 절감할 수 있는 탄소섬유 전구체 섬유의 제조방법과 이로부터 얻어지는 탄소섬유 전구체, 이를 이용하여 보다 짧은 시간 동안의 내염화 공정을 거쳐 탄소섬유를 제조하는 방법을 개시한다.
PCT/KR2010/009085 2009-12-18 2010-12-17 폴리아크릴로니트릴계 중합체 용액，그 제조방법，탄소섬유 전구체 섬유，탄소섬유 전구체 섬유의 제조방법 및 탄소섬유의 제조방법 WO2011074918A2 (ko)

Priority Applications (2)

Application Number Priority Date Filing Date Title
US13/521,081 US9212236B2 (en) 2009-12-18 2010-12-17 Polyacrylonitrile-based polymer solution, preparing method of the same, carbon fiber precursor, manufacturing method of the same and manufacturing method of carbon fiber using the same
CN201080063613.XA CN102753589B (zh) 2009-12-18 2010-12-17 聚丙烯腈基聚合物溶液及其制备方法、碳纤维母体纤维、碳纤维母体纤维的制备方法以及碳纤维的制备方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR1020090126518A KR101268173B1 (ko) 2009-12-18 2009-12-18 폴리아크릴로니트릴계 중합체 용액，그 제조방법，탄소섬유 전구체 섬유，탄소섬유 전구체 섬유의 제조방법 및 탄소섬유의 제조방법
KR10-2009-0126518 2009-12-18

Publications (2)

Publication Number Publication Date
WO2011074918A2 WO2011074918A2 (ko) 2011-06-23
WO2011074918A3 true WO2011074918A3 (ko) 2011-11-10

Family

ID=44167899

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/KR2010/009085 WO2011074918A2 (ko) 2009-12-18 2010-12-17 폴리아크릴로니트릴계 중합체 용액，그 제조방법，탄소섬유 전구체 섬유，탄소섬유 전구체 섬유의 제조방법 및 탄소섬유의 제조방법

Country Status (4)

Country Link
US (1) US9212236B2 (ko)
KR (1) KR101268173B1 (ko)
CN (1) CN102753589B (ko)
WO (1) WO2011074918A2 (ko)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102596017B1 (ko) * 2015-10-08 2023-10-30 스토라 엔소 오와이제이 전구체 얀의 제조 방법
CN105671692B (zh) * 2016-02-05 2017-10-17 扬州大学 密胺树脂改性的富氮多孔碳纤维电极材料的制备方法
US10676426B2 (en) 2017-06-30 2020-06-09 Novomer, Inc. Acrylonitrile derivatives from epoxide and carbon monoxide reagents

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080152574A1 (en) * 2004-12-27 2008-06-26 Toray Industries, Inc, A Corporation Of Japan Oil Agent for Precursor Fiber of Carbon Fiber, Carbon Fiber and Production Method of the Carbon Fiber
KR20090068370A (ko) * 2006-10-18 2009-06-26 도레이 카부시키가이샤 폴리아크릴로니트릴계 중합체와 그의 제조 방법, 탄소 섬유 전구체 섬유의 제조 방법, 및 탄소 섬유와 그의 제조 방법
JP2009185273A (ja) * 2008-01-09 2009-08-20 Mitsubishi Rayon Co Ltd 炭素繊維前駆体アクリル繊維用重合体粒子及び炭素繊維前駆体アクリル繊維

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4543922B2 (ja) * 2004-12-27 2010-09-15 東レ株式会社 炭素繊維前駆体繊維用シリコーン油剤、炭素繊維前駆体繊維、耐炎化繊維および炭素繊維およびそれらの製造方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080152574A1 (en) * 2004-12-27 2008-06-26 Toray Industries, Inc, A Corporation Of Japan Oil Agent for Precursor Fiber of Carbon Fiber, Carbon Fiber and Production Method of the Carbon Fiber
KR20090068370A (ko) * 2006-10-18 2009-06-26 도레이 카부시키가이샤 폴리아크릴로니트릴계 중합체와 그의 제조 방법, 탄소 섬유 전구체 섬유의 제조 방법, 및 탄소 섬유와 그의 제조 방법
JP2009185273A (ja) * 2008-01-09 2009-08-20 Mitsubishi Rayon Co Ltd 炭素繊維前駆体アクリル繊維用重合体粒子及び炭素繊維前駆体アクリル繊維

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
LIU, J.-J.: "Modification of Polyacrylonitrile Precursors for Carbon Fiber via Copolymerization of Acrylonitrile with Ammonium Itaconate.", J. APPL. POLYM. SCI., vol. 102, 2006, pages 2175 - 2179 *

Also Published As

Publication number Publication date
US20120319315A1 (en) 2012-12-20
CN102753589B (zh) 2015-01-21
US9212236B2 (en) 2015-12-15
KR20110069925A (ko) 2011-06-24
WO2011074918A2 (ko) 2011-06-23
KR101268173B1 (ko) 2013-05-27
CN102753589A (zh) 2012-10-24

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