WO2011069933A3 - Verfahren zur regenerierung eines ruthenium-haltigen geträgerten hydrierkatalysators - Google Patents
Verfahren zur regenerierung eines ruthenium-haltigen geträgerten hydrierkatalysators Download PDFInfo
- Publication number
- WO2011069933A3 WO2011069933A3 PCT/EP2010/068911 EP2010068911W WO2011069933A3 WO 2011069933 A3 WO2011069933 A3 WO 2011069933A3 EP 2010068911 W EP2010068911 W EP 2010068911W WO 2011069933 A3 WO2011069933 A3 WO 2011069933A3
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- containing ruthenium
- catalyst containing
- regenerating
- hydrogenation catalyst
- supported hydrogenation
- Prior art date
Links
- 239000003054 catalyst Substances 0.000 title abstract 5
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 title abstract 3
- 238000005984 hydrogenation reaction Methods 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 3
- 229910052707 ruthenium Inorganic materials 0.000 title abstract 3
- 230000001172 regenerating effect Effects 0.000 title abstract 2
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 abstract 3
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 abstract 1
- 230000008929 regeneration Effects 0.000 abstract 1
- 238000011069 regeneration method Methods 0.000 abstract 1
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/90—Regeneration or reactivation
- B01J23/96—Regeneration or reactivation of catalysts comprising metals, oxides or hydroxides of the noble metals
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J38/00—Regeneration or reactivation of catalysts, in general
- B01J38/04—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
- B01J38/06—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst using steam
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C5/00—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms
- C07C5/02—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by hydrogenation
- C07C5/10—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by hydrogenation of aromatic six-membered rings
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
- B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
- B01J23/46—Ruthenium, rhodium, osmium or iridium
- B01J23/462—Ruthenium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
- B01J35/396—Distribution of the active metal ingredient
- B01J35/397—Egg shell like
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
- B01J35/61—Surface area
- B01J35/615—100-500 m2/g
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
- B01J35/64—Pore diameter
- B01J35/647—2-50 nm
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
- B01J35/64—Pore diameter
- B01J35/651—50-500 nm
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
- B01J35/64—Pore diameter
- B01J35/653—500-1000 nm
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
- B01J35/64—Pore diameter
- B01J35/657—Pore diameter larger than 1000 nm
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
- B01J35/66—Pore distribution
- B01J35/69—Pore distribution bimodal
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2521/00—Catalysts comprising the elements, oxides or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium or hafnium
- C07C2521/02—Boron or aluminium; Oxides or hydroxides thereof
- C07C2521/04—Alumina
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2521/00—Catalysts comprising the elements, oxides or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium or hafnium
- C07C2521/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
- C07C2521/08—Silica
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2523/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group C07C2521/00
- C07C2523/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group C07C2521/00 of noble metals
- C07C2523/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group C07C2521/00 of noble metals of the platinum group metals
- C07C2523/46—Ruthenium, rhodium, osmium or iridium
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/584—Recycling of catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Abstract
Verfahren zur Regenerierung eines Ruthenium-haltigen geträgerten Hydrierkatalysators, wobei der Katalysator mit Wasserdampf behandelt und danach getrocknet wird. Integriertes Verfahren zur Hydrierung von Benzol zu Cyclohexan in Gegenwart eines Ruthenium-haltigen geträgerten Katalysators, umfassend neben dem Hydrierschritt die Katalysator-Regenerierungsschritte.
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP10787119A EP2509712A2 (de) | 2009-12-11 | 2010-12-06 | Verfahren zur regenerierung eines ruthenium-haltigen geträgerten hydrierkatalysators |
CN2010800560855A CN102652037A (zh) | 2009-12-11 | 2010-12-06 | 再生含钌的负载型氢化催化剂的方法 |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP09178939 | 2009-12-11 | ||
EP09178939.6 | 2009-12-11 |
Publications (2)
Publication Number | Publication Date |
---|---|
WO2011069933A2 WO2011069933A2 (de) | 2011-06-16 |
WO2011069933A3 true WO2011069933A3 (de) | 2011-10-13 |
Family
ID=43971286
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/EP2010/068911 WO2011069933A2 (de) | 2009-12-11 | 2010-12-06 | Verfahren zur regenerierung eines ruthenium-haltigen geträgerten hydrierkatalysators |
Country Status (4)
Country | Link |
---|---|
US (1) | US20110144398A1 (de) |
EP (1) | EP2509712A2 (de) |
CN (1) | CN102652037A (de) |
WO (1) | WO2011069933A2 (de) |
Families Citing this family (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR101833077B1 (ko) | 2009-12-15 | 2018-02-27 | 바스프 에스이 | 방향족 화합물의 수소화를 위한 촉매 및 방법 |
US8933262B2 (en) | 2011-05-24 | 2015-01-13 | Basf Se | Process for preparing polyisocyanates from biomass |
WO2013103394A1 (en) | 2012-01-06 | 2013-07-11 | Celanese International Corporation | Processes for making catalysts with metal halide precursors |
WO2013103398A1 (en) | 2012-01-06 | 2013-07-11 | Celanese International Corporation | Modified catalyst supports and process for producing ethanol using the catalyst |
US20130178663A1 (en) | 2012-01-06 | 2013-07-11 | Celanese International Corporation | Cobalt-containing hydrogenation catalysts and processes for making same |
WO2013103396A1 (en) | 2012-01-06 | 2013-07-11 | Celanese International Corporation | Processes for making catalysts with oxalate precursors |
MX2014008252A (es) | 2012-01-06 | 2014-08-08 | Celanese Int Corp | Catalizadores de hidrogenacion. |
WO2013103393A1 (en) | 2012-01-06 | 2013-07-11 | Celanese International Corporation | Processes for making catalysts comprising precious metal and active metal modified support |
WO2013103392A1 (en) | 2012-01-06 | 2013-07-11 | Celanese International Corporation | Hydrogenation catalyst and process for producing ethanol using the catalyst |
CN109382095A (zh) * | 2018-11-13 | 2019-02-26 | 江西理工大学 | 乙苯加氢制备乙基环己烷的催化剂及制备方法、应用 |
US11918989B2 (en) * | 2020-12-18 | 2024-03-05 | Evonik Operations Gmbh | Process for regeneration of hydrogenation catalysts |
EP4015079A1 (de) * | 2020-12-18 | 2022-06-22 | Evonik Operations GmbH | Verfahren zur regenerierung von hydrierkatalysatoren |
CN114522707B (zh) * | 2022-02-22 | 2023-07-21 | 中南大学 | 一种碱土金属碳酸盐负载纳米钌复合材料及其制备方法和应用 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3753926A (en) * | 1971-03-08 | 1973-08-21 | Universal Oil Prod Co | Regeneration of a coke deactivated catalyst comprising a combination of platinum rhenium and halogen with a porous carrier material |
GB1452087A (en) * | 1972-11-13 | 1976-10-06 | Shell Int Research | Process for regenerating a deactivated reforming catalyst |
US5495055A (en) * | 1994-08-12 | 1996-02-27 | Arco Chemical Technology, L.P. | Acetone hydrogenation using a supported ruthenium catalyst |
DE102005029200A1 (de) * | 2005-06-22 | 2006-12-28 | Basf Ag | Katalysator und Verfahren zur Hydrierung von hydrierbare Gruppen enthaltenden organischen Verbindungen |
Family Cites Families (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2757128A (en) * | 1951-04-27 | 1956-07-31 | Exxon Research Engineering Co | Low pressure hydrogenation and hydrogen regeneration of the catalyst |
US3245919A (en) * | 1961-05-22 | 1966-04-12 | Sinclair Refining Co | Boehmite base precursor |
US3851004A (en) * | 1973-09-27 | 1974-11-26 | Union Carbide Corp | Hydrocarbon alkylation process using catalyst regeneration |
US4431750A (en) * | 1982-05-19 | 1984-02-14 | Phillips Petroleum Company | Platinum group metal catalyst on the surface of a support and a process for preparing same |
CA1284982C (en) | 1986-05-02 | 1991-06-18 | Carmo Joseph Pereira | Hydroprocessing catalyst and support having bidisperse pore structure |
DE4128629A1 (de) | 1991-08-29 | 1993-03-04 | Basf Ag | Silberhaltiger traegerkatalysator und verfahren zur katalytischen zersetzung von distickstoffmonoxid |
US5817589A (en) | 1996-04-02 | 1998-10-06 | Intevep, S.A. | Regeneration of catalyst comprising flushing with inert gas followed by flushing with hydrogen |
US6248924B1 (en) | 1996-06-19 | 2001-06-19 | Basf Aktiengesellschaft | Process for reacting an organic compound in the presence of a supported ruthenium catalyst |
DE19917051A1 (de) | 1999-04-15 | 2000-10-19 | Basf Ag | Verfahren zur Hydrierung von unsubstituierten oder alkylsubstituierten Aromaten unter Verwendung eines Makroporen aufweisenden Katalysators |
DE10128205A1 (de) * | 2001-06-11 | 2002-12-12 | Basf Ag | Ruthenium-Katalysatoren |
US7230035B2 (en) * | 2002-12-30 | 2007-06-12 | Conocophillips Company | Catalysts for the conversion of methane to synthesis gas |
DE10361157A1 (de) * | 2003-12-22 | 2005-07-21 | Basf Ag | Ruthenium-Heterogenkatalysator und Verfahren zur Herstellung eines Bisglycidylethers der Formel I |
ES2759627T3 (es) * | 2006-07-31 | 2020-05-11 | Basf Se | Procedimiento integrado consistente en la hidrogenación con catalizadores de rutenio y regeneración de los mismos |
US8889936B2 (en) | 2006-07-31 | 2014-11-18 | Basf Se | Method of regenerating ruthenium catalysts for the hydrogenation of benzene |
JP4754519B2 (ja) | 2007-03-27 | 2011-08-24 | Jx日鉱日石エネルギー株式会社 | 改質触媒の再生方法 |
-
2010
- 2010-12-01 US US12/958,010 patent/US20110144398A1/en not_active Abandoned
- 2010-12-06 CN CN2010800560855A patent/CN102652037A/zh active Pending
- 2010-12-06 WO PCT/EP2010/068911 patent/WO2011069933A2/de active Application Filing
- 2010-12-06 EP EP10787119A patent/EP2509712A2/de not_active Withdrawn
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3753926A (en) * | 1971-03-08 | 1973-08-21 | Universal Oil Prod Co | Regeneration of a coke deactivated catalyst comprising a combination of platinum rhenium and halogen with a porous carrier material |
GB1452087A (en) * | 1972-11-13 | 1976-10-06 | Shell Int Research | Process for regenerating a deactivated reforming catalyst |
US5495055A (en) * | 1994-08-12 | 1996-02-27 | Arco Chemical Technology, L.P. | Acetone hydrogenation using a supported ruthenium catalyst |
DE102005029200A1 (de) * | 2005-06-22 | 2006-12-28 | Basf Ag | Katalysator und Verfahren zur Hydrierung von hydrierbare Gruppen enthaltenden organischen Verbindungen |
Also Published As
Publication number | Publication date |
---|---|
EP2509712A2 (de) | 2012-10-17 |
US20110144398A1 (en) | 2011-06-16 |
WO2011069933A2 (de) | 2011-06-16 |
CN102652037A (zh) | 2012-08-29 |
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