WO2010056077A9 - High-hardness coating powder, and preparation method thereof - Google Patents
High-hardness coating powder, and preparation method thereof Download PDFInfo
- Publication number
- WO2010056077A9 WO2010056077A9 PCT/KR2009/006719 KR2009006719W WO2010056077A9 WO 2010056077 A9 WO2010056077 A9 WO 2010056077A9 KR 2009006719 W KR2009006719 W KR 2009006719W WO 2010056077 A9 WO2010056077 A9 WO 2010056077A9
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- powder
- salt
- base
- coating
- producing
- Prior art date
Links
- 239000000843 powders Substances 0.000 title claims abstract description 121
- 239000011248 coating agents Substances 0.000 title claims abstract description 103
- 238000000576 coating method Methods 0.000 title claims abstract description 103
- 238000002360 preparation methods Methods 0.000 title 1
- 239000000463 materials Substances 0.000 claims abstract description 135
- 150000003839 salts Chemical class 0.000 claims abstract description 90
- 239000011780 sodium chloride Substances 0.000 claims abstract description 89
- 239000010936 titanium Substances 0.000 claims abstract description 52
- 229910052719 titanium Inorganic materials 0.000 claims abstract description 39
- RTAQQCXQSZGOHL-UHFFFAOYSA-N titanium Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims abstract description 38
- 238000006243 chemical reactions Methods 0.000 claims abstract description 37
- 239000002904 solvents Substances 0.000 claims abstract description 13
- 238000010438 heat treatment Methods 0.000 claims abstract description 11
- 239000000460 chlorine Substances 0.000 claims abstract description 7
- 238000001035 drying Methods 0.000 claims abstract description 6
- 238000002156 mixing Methods 0.000 claims abstract description 5
- 229910052801 chlorine Inorganic materials 0.000 claims abstract description 4
- 239000000203 mixtures Substances 0.000 claims abstract description 4
- ZAMOUSCENKQFHK-UHFFFAOYSA-N chlorine atom Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims abstract description 3
- 229910052731 fluorine Inorganic materials 0.000 claims abstract description 3
- 239000011737 fluorine Substances 0.000 claims abstract description 3
- YCKRFDGAMUMZLT-UHFFFAOYSA-N fluorine atom Chemical compound data:image/svg+xml;base64,PD94bWwgdmVyc2lvbj0nMS4wJyBlbmNvZGluZz0naXNvLTg4NTktMSc/Pgo8c3ZnIHZlcnNpb249JzEuMScgYmFzZVByb2ZpbGU9J2Z1bGwnCiAgICAgICAgICAgICAgeG1sbnM9J2h0dHA6Ly93d3cudzMub3JnLzIwMDAvc3ZnJwogICAgICAgICAgICAgICAgICAgICAgeG1sbnM6cmRraXQ9J2h0dHA6Ly93d3cucmRraXQub3JnL3htbCcKICAgICAgICAgICAgICAgICAgICAgIHhtbG5zOnhsaW5rPSdodHRwOi8vd3d3LnczLm9yZy8xOTk5L3hsaW5rJwogICAgICAgICAgICAgICAgICB4bWw6c3BhY2U9J3ByZXNlcnZlJwp3aWR0aD0nMzAwcHgnIGhlaWdodD0nMzAwcHgnIHZpZXdCb3g9JzAgMCAzMDAgMzAwJz4KPCEtLSBFTkQgT0YgSEVBREVSIC0tPgo8cmVjdCBzdHlsZT0nb3BhY2l0eToxLjA7ZmlsbDojRkZGRkZGO3N0cm9rZTpub25lJyB3aWR0aD0nMzAwJyBoZWlnaHQ9JzMwMCcgeD0nMCcgeT0nMCc+IDwvcmVjdD4KPHRleHQgZG9taW5hbnQtYmFzZWxpbmU9ImNlbnRyYWwiIHRleHQtYW5jaG9yPSJlbmQiIHg9JzE2MC42NycgeT0nMTU2JyBzdHlsZT0nZm9udC1zaXplOjQwcHg7Zm9udC1zdHlsZTpub3JtYWw7Zm9udC13ZWlnaHQ6bm9ybWFsO2ZpbGwtb3BhY2l0eToxO3N0cm9rZTpub25lO2ZvbnQtZmFtaWx5OnNhbnMtc2VyaWY7ZmlsbDojNzdEOEVEJyA+PHRzcGFuPkY8L3RzcGFuPjwvdGV4dD4KPHBhdGggZD0nTSAxNTguMTgyLDExMy42MzYgTCAxNTguMTUyLDExMi45MzMgTCAxNTguMDYxLDExMi4yMzUgTCAxNTcuOTExLDExMS41NDcgTCAxNTcuNzAyLDExMC44NzUgTCAxNTcuNDM2LDExMC4yMjMgTCAxNTcuMTE1LDEwOS41OTYgTCAxNTYuNzQxLDEwOSBMIDE1Ni4zMTgsMTA4LjQzNyBMIDE1NS44NDcsMTA3LjkxNCBMIDE1NS4zMzQsMTA3LjQzMiBMIDE1NC43ODEsMTA2Ljk5NiBMIDE1NC4xOTIsMTA2LjYxIEwgMTUzLjU3MywxMDYuMjc2IEwgMTUyLjkyNywxMDUuOTk2IEwgMTUyLjI1OSwxMDUuNzczIEwgMTUxLjU3NSwxMDUuNjA3IEwgMTUwLjg3OSwxMDUuNTAyIEwgMTUwLjE3NiwxMDUuNDU2IEwgMTQ5LjQ3MiwxMDUuNDcyIEwgMTQ4Ljc3MiwxMDUuNTQ3IEwgMTQ4LjA4MSwxMDUuNjgzIEwgMTQ3LjQwNSwxMDUuODc3IEwgMTQ2Ljc0NywxMDYuMTI5IEwgMTQ2LjExNCwxMDYuNDM2IEwgMTQ1LjUwOSwxMDYuNzk3IEwgMTQ0LjkzOCwxMDcuMjA4IEwgMTQ0LjQwNCwxMDcuNjY3IEwgMTQzLjkxMiwxMDguMTcgTCAxNDMuNDY1LDEwOC43MTQgTCAxNDMuMDY2LDEwOS4yOTQgTCAxNDIuNzE4LDEwOS45MDYgTCAxNDIuNDI0LDExMC41NDYgTCAxNDIuMTg3LDExMS4yMDkgTCAxNDIuMDA3LDExMS44ODkgTCAxNDEuODg2LDExMi41ODMgTCAxNDEuODI2LDExMy4yODQgTCAxNDEuODI2LDExMy45ODggTCAxNDEuODg2LDExNC42OSBMIDE0Mi4wMDcsMTE1LjM4MyBMIDE0Mi4xODcsMTE2LjA2NCBMIDE0Mi40MjQsMTE2LjcyNyBMIDE0Mi43MTgsMTE3LjM2NyBMIDE0My4wNjYsMTE3Ljk3OSBMIDE0My40NjUsMTE4LjU1OSBMIDE0My45MTIsMTE5LjEwMiBMIDE0NC40MDQsMTE5LjYwNSBMIDE0NC45MzgsMTIwLjA2NCBMIDE0NS41MDksMTIwLjQ3NiBMIDE0Ni4xMTQsMTIwLjgzNiBMIDE0Ni43NDcsMTIxLjE0NCBMIDE0Ny40MDUsMTIxLjM5NiBMIDE0OC4wODEsMTIxLjU5IEwgMTQ4Ljc3MiwxMjEuNzI2IEwgMTQ5LjQ3MiwxMjEuODAxIEwgMTUwLjE3NiwxMjEuODE2IEwgMTUwLjg3OSwxMjEuNzcxIEwgMTUxLjU3NSwxMjEuNjY1IEwgMTUyLjI1OSwxMjEuNSBMIDE1Mi45MjcsMTIxLjI3NyBMIDE1My41NzMsMTIwLjk5NyBMIDE1NC4xOTIsMTIwLjY2MyBMIDE1NC43ODEsMTIwLjI3NiBMIDE1NS4zMzQsMTE5Ljg0MSBMIDE1NS44NDcsMTE5LjM1OSBMIDE1Ni4zMTgsMTE4LjgzNSBMIDE1Ni43NDEsMTE4LjI3MyBMIDE1Ny4xMTUsMTE3LjY3NiBMIDE1Ny40MzYsMTE3LjA1IEwgMTU3LjcwMiwxMTYuMzk4IEwgMTU3LjkxMSwxMTUuNzI2IEwgMTU4LjA2MSwxMTUuMDM4IEwgMTU4LjE1MiwxMTQuMzQgTCAxNTguMTgyLDExMy42MzYgTCAxNTAsMTEzLjYzNiBaJyBzdHlsZT0nZmlsbDojMDAwMDAwO2ZpbGwtcnVsZTpldmVub2RkO2ZpbGwtb3BhY2l0eT0xO3N0cm9rZTojMDAwMDAwO3N0cm9rZS13aWR0aDoxMHB4O3N0cm9rZS1saW5lY2FwOmJ1dHQ7c3Ryb2tlLWxpbmVqb2luOm1pdGVyO3N0cm9rZS1vcGFjaXR5OjE7JyAvPgo8L3N2Zz4K data:image/svg+xml;base64,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 [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims abstract description 3
- 239000002245 particles Substances 0.000 claims description 46
- 239000010432 diamond Substances 0.000 claims description 29
- 229910003460 diamond Inorganic materials 0.000 claims description 29
- 238000004519 manufacturing process Methods 0.000 claims description 28
- 229910052582 BN Inorganic materials 0.000 claims description 25
- PZNSFCLAULLKQX-UHFFFAOYSA-N N#B Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 claims description 25
- 229910021393 carbon nanotubes Inorganic materials 0.000 claims description 17
- 229910010346 TiF Inorganic materials 0.000 claims description 13
- 239000002041 carbon nanotubes Substances 0.000 claims description 11
- 239000007789 gases Substances 0.000 claims description 9
- WDIHJSXYQDMJHN-UHFFFAOYSA-L Barium chloride Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 [Cl-].[Cl-].[Ba+2] WDIHJSXYQDMJHN-UHFFFAOYSA-L 0.000 claims description 8
- 229910000574 NaK Inorganic materials 0.000 claims description 8
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M potassium chloride Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 8
- 229910001390 sodium chloride Inorganic materials 0.000 claims description 8
- FAPWRFPIFSIZLT-UHFFFAOYSA-M sodium chloride Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 8
- 239000001103 potassium chloride Substances 0.000 claims description 7
- 229910001481 potassium chloride Inorganic materials 0.000 claims description 7
- 239000007815 EtOH Substances 0.000 claims description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N ethanol Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 239000012153 distilled water Substances 0.000 claims description 5
- 239000011775 sodium fluoride Substances 0.000 claims description 5
- 235000013024 sodium fluoride Nutrition 0.000 claims description 5
- 229910001526 sodium fluoride Inorganic materials 0.000 claims description 5
- 239000001257 hydrogen Substances 0.000 claims description 4
- 229910052739 hydrogen Inorganic materials 0.000 claims description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N hydrogen Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N HCl Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 3
- 239000001104 hydrochloric acid Substances 0.000 claims description 3
- 238000002425 crystallisation Methods 0.000 claims description 2
- 238000007710 freezing Methods 0.000 claims 1
- 238000009210 therapy by ultrasound Methods 0.000 claims 1
- 239000010953 base metals Substances 0.000 description 28
- 239000011812 mixed powders Substances 0.000 description 18
- 239000000243 solutions Substances 0.000 description 18
- 238000005520 cutting process Methods 0.000 description 13
- 238000000034 methods Methods 0.000 description 13
- 239000011247 coating layers Substances 0.000 description 12
- 238000010586 diagrams Methods 0.000 description 11
- 238000002844 melting Methods 0.000 description 10
- 230000005540 biological transmission Effects 0.000 description 6
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N boron Chemical compound data:image/svg+xml;base64,PD94bWwgdmVyc2lvbj0nMS4wJyBlbmNvZGluZz0naXNvLTg4NTktMSc/Pgo8c3ZnIHZlcnNpb249JzEuMScgYmFzZVByb2ZpbGU9J2Z1bGwnCiAgICAgICAgICAgICAgeG1sbnM9J2h0dHA6Ly93d3cudzMub3JnLzIwMDAvc3ZnJwogICAgICAgICAgICAgICAgICAgICAgeG1sbnM6cmRraXQ9J2h0dHA6Ly93d3cucmRraXQub3JnL3htbCcKICAgICAgICAgICAgICAgICAgICAgIHhtbG5zOnhsaW5rPSdodHRwOi8vd3d3LnczLm9yZy8xOTk5L3hsaW5rJwogICAgICAgICAgICAgICAgICB4bWw6c3BhY2U9J3ByZXNlcnZlJwp3aWR0aD0nMzAwcHgnIGhlaWdodD0nMzAwcHgnIHZpZXdCb3g9JzAgMCAzMDAgMzAwJz4KPCEtLSBFTkQgT0YgSEVBREVSIC0tPgo8cmVjdCBzdHlsZT0nb3BhY2l0eToxLjA7ZmlsbDojRkZGRkZGO3N0cm9rZTpub25lJyB3aWR0aD0nMzAwJyBoZWlnaHQ9JzMwMCcgeD0nMCcgeT0nMCc+IDwvcmVjdD4KPHRleHQgZG9taW5hbnQtYmFzZWxpbmU9ImNlbnRyYWwiIHRleHQtYW5jaG9yPSJzdGFydCIgeD0nMTM3Ljk4NicgeT0nMTU2JyBzdHlsZT0nZm9udC1zaXplOjQwcHg7Zm9udC1zdHlsZTpub3JtYWw7Zm9udC13ZWlnaHQ6bm9ybWFsO2ZpbGwtb3BhY2l0eToxO3N0cm9rZTpub25lO2ZvbnQtZmFtaWx5OnNhbnMtc2VyaWY7ZmlsbDojM0I0MTQzJyA+PHRzcGFuPkI8L3RzcGFuPjwvdGV4dD4KPHBhdGggZD0nTSAxMDUuNjgyLDExMy42MzYgTCAxMDUuNjUyLDExMi45MzMgTCAxMDUuNTYxLDExMi4yMzUgTCAxMDUuNDExLDExMS41NDcgTCAxMDUuMjAyLDExMC44NzUgTCAxMDQuOTM2LDExMC4yMjMgTCAxMDQuNjE1LDEwOS41OTYgTCAxMDQuMjQxLDEwOSBMIDEwMy44MTgsMTA4LjQzNyBMIDEwMy4zNDcsMTA3LjkxNCBMIDEwMi44MzQsMTA3LjQzMiBMIDEwMi4yODEsMTA2Ljk5NiBMIDEwMS42OTIsMTA2LjYxIEwgMTAxLjA3MywxMDYuMjc2IEwgMTAwLjQyNywxMDUuOTk2IEwgOTkuNzU5LDEwNS43NzMgTCA5OS4wNzQ2LDEwNS42MDcgTCA5OC4zNzg2LDEwNS41MDIgTCA5Ny42NzYsMTA1LjQ1NiBMIDk2Ljk3MjIsMTA1LjQ3MiBMIDk2LjI3MjMsMTA1LjU0NyBMIDk1LjU4MTQsMTA1LjY4MyBMIDk0LjkwNDgsMTA1Ljg3NyBMIDk0LjI0NzQsMTA2LjEyOSBMIDkzLjYxNCwxMDYuNDM2IEwgOTMuMDA5NSwxMDYuNzk3IEwgOTIuNDM4MSwxMDcuMjA4IEwgOTEuOTA0MywxMDcuNjY3IEwgOTEuNDExOSwxMDguMTcgTCA5MC45NjQ1LDEwOC43MTQgTCA5MC41NjU2LDEwOS4yOTQgTCA5MC4yMTgsMTA5LjkwNiBMIDg5LjkyNDMsMTEwLjU0NiBMIDg5LjY4NjYsMTExLjIwOSBMIDg5LjUwNjksMTExLjg4OSBMIDg5LjM4NjMsMTEyLjU4MyBMIDg5LjMyNTgsMTEzLjI4NCBMIDg5LjMyNTgsMTEzLjk4OCBMIDg5LjM4NjMsMTE0LjY5IEwgODkuNTA2OSwxMTUuMzgzIEwgODkuNjg2NiwxMTYuMDY0IEwgODkuOTI0MywxMTYuNzI3IEwgOTAuMjE4LDExNy4zNjcgTCA5MC41NjU2LDExNy45NzkgTCA5MC45NjQ1LDExOC41NTkgTCA5MS40MTE5LDExOS4xMDIgTCA5MS45MDQzLDExOS42MDUgTCA5Mi40MzgxLDEyMC4wNjQgTCA5My4wMDk1LDEyMC40NzYgTCA5My42MTQsMTIwLjgzNiBMIDk0LjI0NzQsMTIxLjE0NCBMIDk0LjkwNDgsMTIxLjM5NiBMIDk1LjU4MTQsMTIxLjU5IEwgOTYuMjcyMywxMjEuNzI2IEwgOTYuOTcyMiwxMjEuODAxIEwgOTcuNjc2LDEyMS44MTYgTCA5OC4zNzg2LDEyMS43NzEgTCA5OS4wNzQ2LDEyMS42NjUgTCA5OS43NTksMTIxLjUgTCAxMDAuNDI3LDEyMS4yNzcgTCAxMDEuMDczLDEyMC45OTcgTCAxMDEuNjkyLDEyMC42NjMgTCAxMDIuMjgxLDEyMC4yNzYgTCAxMDIuODM0LDExOS44NDEgTCAxMDMuMzQ3LDExOS4zNTkgTCAxMDMuODE4LDExOC44MzUgTCAxMDQuMjQxLDExOC4yNzMgTCAxMDQuNjE1LDExNy42NzYgTCAxMDQuOTM2LDExNy4wNSBMIDEwNS4yMDIsMTE2LjM5OCBMIDEwNS40MTEsMTE1LjcyNiBMIDEwNS41NjEsMTE1LjAzOCBMIDEwNS42NTIsMTE0LjM0IEwgMTA1LjY4MiwxMTMuNjM2IEwgOTcuNSwxMTMuNjM2IFonIHN0eWxlPSdmaWxsOiMwMDAwMDA7ZmlsbC1ydWxlOmV2ZW5vZGQ7ZmlsbC1vcGFjaXR5PTE7c3Ryb2tlOiMwMDAwMDA7c3Ryb2tlLXdpZHRoOjEwcHg7c3Ryb2tlLWxpbmVjYXA6YnV0dDtzdHJva2UtbGluZWpvaW46bWl0ZXI7c3Ryb2tlLW9wYWNpdHk6MTsnIC8+CjxwYXRoIGQ9J00gMjEwLjY4MiwxMTMuNjM2IEwgMjEwLjY1MiwxMTIuOTMzIEwgMjEwLjU2MSwxMTIuMjM1IEwgMjEwLjQxMSwxMTEuNTQ3IEwgMjEwLjIwMiwxMTAuODc1IEwgMjA5LjkzNiwxMTAuMjIzIEwgMjA5LjYxNSwxMDkuNTk2IEwgMjA5LjI0MSwxMDkgTCAyMDguODE4LDEwOC40MzcgTCAyMDguMzQ3LDEwNy45MTQgTCAyMDcuODM0LDEwNy40MzIgTCAyMDcuMjgxLDEwNi45OTYgTCAyMDYuNjkyLDEwNi42MSBMIDIwNi4wNzMsMTA2LjI3NiBMIDIwNS40MjcsMTA1Ljk5NiBMIDIwNC43NTksMTA1Ljc3MyBMIDIwNC4wNzUsMTA1LjYwNyBMIDIwMy4zNzksMTA1LjUwMiBMIDIwMi42NzYsMTA1LjQ1NiBMIDIwMS45NzIsMTA1LjQ3MiBMIDIwMS4yNzIsMTA1LjU0NyBMIDIwMC41ODEsMTA1LjY4MyBMIDE5OS45MDUsMTA1Ljg3NyBMIDE5OS4yNDcsMTA2LjEyOSBMIDE5OC42MTQsMTA2LjQzNiBMIDE5OC4wMDksMTA2Ljc5NyBMIDE5Ny40MzgsMTA3LjIwOCBMIDE5Ni45MDQsMTA3LjY2NyBMIDE5Ni40MTIsMTA4LjE3IEwgMTk1Ljk2NSwxMDguNzE0IEwgMTk1LjU2NiwxMDkuMjk0IEwgMTk1LjIxOCwxMDkuOTA2IEwgMTk0LjkyNCwxMTAuNTQ2IEwgMTk0LjY4NywxMTEuMjA5IEwgMTk0LjUwNywxMTEuODg5IEwgMTk0LjM4NiwxMTIuNTgzIEwgMTk0LjMyNiwxMTMuMjg0IEwgMTk0LjMyNiwxMTMuOTg4IEwgMTk0LjM4NiwxMTQuNjkgTCAxOTQuNTA3LDExNS4zODMgTCAxOTQuNjg3LDExNi4wNjQgTCAxOTQuOTI0LDExNi43MjcgTCAxOTUuMjE4LDExNy4zNjcgTCAxOTUuNTY2LDExNy45NzkgTCAxOTUuOTY1LDExOC41NTkgTCAxOTYuNDEyLDExOS4xMDIgTCAxOTYuOTA0LDExOS42MDUgTCAxOTcuNDM4LDEyMC4wNjQgTCAxOTguMDA5LDEyMC40NzYgTCAxOTguNjE0LDEyMC44MzYgTCAxOTkuMjQ3LDEyMS4xNDQgTCAxOTkuOTA1LDEyMS4zOTYgTCAyMDAuNTgxLDEyMS41OSBMIDIwMS4yNzIsMTIxLjcyNiBMIDIwMS45NzIsMTIxLjgwMSBMIDIwMi42NzYsMTIxLjgxNiBMIDIwMy4zNzksMTIxLjc3MSBMIDIwNC4wNzUsMTIxLjY2NSBMIDIwNC43NTksMTIxLjUgTCAyMDUuNDI3LDEyMS4yNzcgTCAyMDYuMDczLDEyMC45OTcgTCAyMDYuNjkyLDEyMC42NjMgTCAyMDcuMjgxLDEyMC4yNzYgTCAyMDcuODM0LDExOS44NDEgTCAyMDguMzQ3LDExOS4zNTkgTCAyMDguODE4LDExOC44MzUgTCAyMDkuMjQxLDExOC4yNzMgTCAyMDkuNjE1LDExNy42NzYgTCAyMDkuOTM2LDExNy4wNSBMIDIxMC4yMDIsMTE2LjM5OCBMIDIxMC40MTEsMTE1LjcyNiBMIDIxMC41NjEsMTE1LjAzOCBMIDIxMC42NTIsMTE0LjM0IEwgMjEwLjY4MiwxMTMuNjM2IEwgMjAyLjUsMTEzLjYzNiBaJyBzdHlsZT0nZmlsbDojMDAwMDAwO2ZpbGwtcnVsZTpldmVub2RkO2ZpbGwtb3BhY2l0eT0xO3N0cm9rZTojMDAwMDAwO3N0cm9rZS13aWR0aDoxMHB4O3N0cm9rZS1saW5lY2FwOmJ1dHQ7c3Ryb2tlLWxpbmVqb2luOm1pdGVyO3N0cm9rZS1vcGFjaXR5OjE7JyAvPgo8cGF0aCBkPSdNIDE1OC4xODIsMTEzLjYzNiBMIDE1OC4xNTIsMTEyLjkzMyBMIDE1OC4wNjEsMTEyLjIzNSBMIDE1Ny45MTEsMTExLjU0NyBMIDE1Ny43MDIsMTEwLjg3NSBMIDE1Ny40MzYsMTEwLjIyMyBMIDE1Ny4xMTUsMTA5LjU5NiBMIDE1Ni43NDEsMTA5IEwgMTU2LjMxOCwxMDguNDM3IEwgMTU1Ljg0NywxMDcuOTE0IEwgMTU1LjMzNCwxMDcuNDMyIEwgMTU0Ljc4MSwxMDYuOTk2IEwgMTU0LjE5MiwxMDYuNjEgTCAxNTMuNTczLDEwNi4yNzYgTCAxNTIuOTI3LDEwNS45OTYgTCAxNTIuMjU5LDEwNS43NzMgTCAxNTEuNTc1LDEwNS42MDcgTCAxNTAuODc5LDEwNS41MDIgTCAxNTAuMTc2LDEwNS40NTYgTCAxNDkuNDcyLDEwNS40NzIgTCAxNDguNzcyLDEwNS41NDcgTCAxNDguMDgxLDEwNS42ODMgTCAxNDcuNDA1LDEwNS44NzcgTCAxNDYuNzQ3LDEwNi4xMjkgTCAxNDYuMTE0LDEwNi40MzYgTCAxNDUuNTA5LDEwNi43OTcgTCAxNDQuOTM4LDEwNy4yMDggTCAxNDQuNDA0LDEwNy42NjcgTCAxNDMuOTEyLDEwOC4xNyBMIDE0My40NjUsMTA4LjcxNCBMIDE0My4wNjYsMTA5LjI5NCBMIDE0Mi43MTgsMTA5LjkwNiBMIDE0Mi40MjQsMTEwLjU0NiBMIDE0Mi4xODcsMTExLjIwOSBMIDE0Mi4wMDcsMTExLjg4OSBMIDE0MS44ODYsMTEyLjU4MyBMIDE0MS44MjYsMTEzLjI4NCBMIDE0MS44MjYsMTEzLjk4OCBMIDE0MS44ODYsMTE0LjY5IEwgMTQyLjAwNywxMTUuMzgzIEwgMTQyLjE4NywxMTYuMDY0IEwgMTQyLjQyNCwxMTYuNzI3IEwgMTQyLjcxOCwxMTcuMzY3IEwgMTQzLjA2NiwxMTcuOTc5IEwgMTQzLjQ2NSwxMTguNTU5IEwgMTQzLjkxMiwxMTkuMTAyIEwgMTQ0LjQwNCwxMTkuNjA1IEwgMTQ0LjkzOCwxMjAuMDY0IEwgMTQ1LjUwOSwxMjAuNDc2IEwgMTQ2LjExNCwxMjAuODM2IEwgMTQ2Ljc0NywxMjEuMTQ0IEwgMTQ3LjQwNSwxMjEuMzk2IEwgMTQ4LjA4MSwxMjEuNTkgTCAxNDguNzcyLDEyMS43MjYgTCAxNDkuNDcyLDEyMS44MDEgTCAxNTAuMTc2LDEyMS44MTYgTCAxNTAuODc5LDEyMS43NzEgTCAxNTEuNTc1LDEyMS42NjUgTCAxNTIuMjU5LDEyMS41IEwgMTUyLjkyNywxMjEuMjc3IEwgMTUzLjU3MywxMjAuOTk3IEwgMTU0LjE5MiwxMjAuNjYzIEwgMTU0Ljc4MSwxMjAuMjc2IEwgMTU1LjMzNCwxMTkuODQxIEwgMTU1Ljg0NywxMTkuMzU5IEwgMTU2LjMxOCwxMTguODM1IEwgMTU2Ljc0MSwxMTguMjczIEwgMTU3LjExNSwxMTcuNjc2IEwgMTU3LjQzNiwxMTcuMDUgTCAxNTcuNzAyLDExNi4zOTggTCAxNTcuOTExLDExNS43MjYgTCAxNTguMDYxLDExNS4wMzggTCAxNTguMTUyLDExNC4zNCBMIDE1OC4xODIsMTEzLjYzNiBMIDE1MCwxMTMuNjM2IFonIHN0eWxlPSdmaWxsOiMwMDAwMDA7ZmlsbC1ydWxlOmV2ZW5vZGQ7ZmlsbC1vcGFjaXR5PTE7c3Ryb2tlOiMwMDAwMDA7c3Ryb2tlLXdpZHRoOjEwcHg7c3Ryb2tlLWxpbmVjYXA6YnV0dDtzdHJva2UtbGluZWpvaW46bWl0ZXI7c3Ryb2tlLW9wYWNpdHk6MTsnIC8+Cjwvc3ZnPgo= data:image/svg+xml;base64,PD94bWwgdmVyc2lvbj0nMS4wJyBlbmNvZGluZz0naXNvLTg4NTktMSc/Pgo8c3ZnIHZlcnNpb249JzEuMScgYmFzZVByb2ZpbGU9J2Z1bGwnCiAgICAgICAgICAgICAgeG1sbnM9J2h0dHA6Ly93d3cudzMub3JnLzIwMDAvc3ZnJwogICAgICAgICAgICAgICAgICAgICAgeG1sbnM6cmRraXQ9J2h0dHA6Ly93d3cucmRraXQub3JnL3htbCcKICAgICAgICAgICAgICAgICAgICAgIHhtbG5zOnhsaW5rPSdodHRwOi8vd3d3LnczLm9yZy8xOTk5L3hsaW5rJwogICAgICAgICAgICAgICAgICB4bWw6c3BhY2U9J3ByZXNlcnZlJwp3aWR0aD0nODVweCcgaGVpZ2h0PSc4NXB4JyB2aWV3Qm94PScwIDAgODUgODUnPgo8IS0tIEVORCBPRiBIRUFERVIgLS0+CjxyZWN0IHN0eWxlPSdvcGFjaXR5OjEuMDtmaWxsOiNGRkZGRkY7c3Ryb2tlOm5vbmUnIHdpZHRoPSc4NScgaGVpZ2h0PSc4NScgeD0nMCcgeT0nMCc+IDwvcmVjdD4KPHRleHQgZG9taW5hbnQtYmFzZWxpbmU9ImNlbnRyYWwiIHRleHQtYW5jaG9yPSJzdGFydCIgeD0nMzAuMzk1MicgeT0nNDcuNzk1NScgc3R5bGU9J2ZvbnQtc2l6ZTozOHB4O2ZvbnQtc3R5bGU6bm9ybWFsO2ZvbnQtd2VpZ2h0Om5vcm1hbDtmaWxsLW9wYWNpdHk6MTtzdHJva2U6bm9uZTtmb250LWZhbWlseTpzYW5zLXNlcmlmO2ZpbGw6IzNCNDE0MycgPjx0c3Bhbj5CPC90c3Bhbj48L3RleHQ+CjxwYXRoIGQ9J00gMjkuNDQzMiwxOC4wNDU1IEwgMjkuNDM0NiwxNy44NDYyIEwgMjkuNDA4OSwxNy42NDg0IEwgMjkuMzY2MywxNy40NTM1IEwgMjkuMzA3MSwxNy4yNjMgTCAyOS4yMzE4LDE3LjA3ODMgTCAyOS4xNDA5LDE2LjkwMDggTCAyOS4wMzUsMTYuNzMxNyBMIDI4LjkxNSwxNi41NzI0IEwgMjguNzgxNywxNi40MjQgTCAyOC42MzYyLDE2LjI4NzYgTCAyOC40Nzk1LDE2LjE2NDIgTCAyOC4zMTI4LDE2LjA1NDcgTCAyOC4xMzcyLDE1Ljk1OTkgTCAyNy45NTQyLDE1Ljg4MDcgTCAyNy43NjUsMTUuODE3NCBMIDI3LjU3MTEsMTUuNzcwNiBMIDI3LjM3MzksMTUuNzQwNyBMIDI3LjE3NDksMTUuNzI3OCBMIDI2Ljk3NTUsMTUuNzMyMSBMIDI2Ljc3NzEsMTUuNzUzNSBMIDI2LjU4MTQsMTUuNzkxOSBMIDI2LjM4OTcsMTUuODQ3IEwgMjYuMjAzNCwxNS45MTgzIEwgMjYuMDI0LDE2LjAwNTQgTCAyNS44NTI3LDE2LjEwNzYgTCAyNS42OTA4LDE2LjIyNDIgTCAyNS41Mzk2LDE2LjM1NDIgTCAyNS40LDE2LjQ5NjggTCAyNS4yNzMzLDE2LjY1MDggTCAyNS4xNjAyLDE2LjgxNTEgTCAyNS4wNjE4LDE2Ljk4ODYgTCAyNC45Nzg1LDE3LjE2OTkgTCAyNC45MTEyLDE3LjM1NzYgTCAyNC44NjAzLDE3LjU1MDUgTCAyNC44MjYxLDE3Ljc0NyBMIDI0LjgwOSwxNy45NDU3IEwgMjQuODA5LDE4LjE0NTIgTCAyNC44MjYxLDE4LjM0MzkgTCAyNC44NjAzLDE4LjU0MDQgTCAyNC45MTEyLDE4LjczMzMgTCAyNC45Nzg1LDE4LjkyMTEgTCAyNS4wNjE4LDE5LjEwMjMgTCAyNS4xNjAyLDE5LjI3NTggTCAyNS4yNzMzLDE5LjQ0MDEgTCAyNS40LDE5LjU5NDEgTCAyNS41Mzk2LDE5LjczNjcgTCAyNS42OTA4LDE5Ljg2NjcgTCAyNS44NTI3LDE5Ljk4MzMgTCAyNi4wMjQsMjAuMDg1NSBMIDI2LjIwMzQsMjAuMTcyNiBMIDI2LjM4OTcsMjAuMjQzOSBMIDI2LjU4MTQsMjAuMjk5IEwgMjYuNzc3MSwyMC4zMzc0IEwgMjYuOTc1NSwyMC4zNTg4IEwgMjcuMTc0OSwyMC4zNjMxIEwgMjcuMzczOSwyMC4zNTAyIEwgMjcuNTcxMSwyMC4zMjAzIEwgMjcuNzY1LDIwLjI3MzUgTCAyNy45NTQyLDIwLjIxMDMgTCAyOC4xMzcyLDIwLjEzMSBMIDI4LjMxMjgsMjAuMDM2MiBMIDI4LjQ3OTUsMTkuOTI2NyBMIDI4LjYzNjIsMTkuODAzMyBMIDI4Ljc4MTcsMTkuNjY2OSBMIDI4LjkxNSwxOS41MTg1IEwgMjkuMDM1LDE5LjM1OTIgTCAyOS4xNDA5LDE5LjE5MDEgTCAyOS4yMzE4LDE5LjAxMjYgTCAyOS4zMDcxLDE4LjgyNzkgTCAyOS4zNjYzLDE4LjYzNzQgTCAyOS40MDg5LDE4LjQ0MjUgTCAyOS40MzQ2LDE4LjI0NDcgTCAyOS40NDMyLDE4LjA0NTUgTCAyNy4xMjUsMTguMDQ1NSBaJyBzdHlsZT0nZmlsbDojMDAwMDAwO2ZpbGwtcnVsZTpldmVub2RkO2ZpbGwtb3BhY2l0eT0xO3N0cm9rZTojMDAwMDAwO3N0cm9rZS13aWR0aDoycHg7c3Ryb2tlLWxpbmVjYXA6YnV0dDtzdHJva2UtbGluZWpvaW46bWl0ZXI7c3Ryb2tlLW9wYWNpdHk6MTsnIC8+CjxwYXRoIGQ9J00gNTkuMTkzMiwxOC4wNDU1IEwgNTkuMTg0NiwxNy44NDYyIEwgNTkuMTU4OSwxNy42NDg0IEwgNTkuMTE2MywxNy40NTM1IEwgNTkuMDU3MSwxNy4yNjMgTCA1OC45ODE4LDE3LjA3ODMgTCA1OC44OTA5LDE2LjkwMDggTCA1OC43ODUsMTYuNzMxNyBMIDU4LjY2NSwxNi41NzI0IEwgNTguNTMxNywxNi40MjQgTCA1OC4zODYyLDE2LjI4NzYgTCA1OC4yMjk1LDE2LjE2NDIgTCA1OC4wNjI4LDE2LjA1NDcgTCA1Ny44ODcyLDE1Ljk1OTkgTCA1Ny43MDQyLDE1Ljg4MDcgTCA1Ny41MTUsMTUuODE3NCBMIDU3LjMyMTEsMTUuNzcwNiBMIDU3LjEyMzksMTUuNzQwNyBMIDU2LjkyNDksMTUuNzI3OCBMIDU2LjcyNTUsMTUuNzMyMSBMIDU2LjUyNzEsMTUuNzUzNSBMIDU2LjMzMTQsMTUuNzkxOSBMIDU2LjEzOTcsMTUuODQ3IEwgNTUuOTUzNCwxNS45MTgzIEwgNTUuNzc0LDE2LjAwNTQgTCA1NS42MDI3LDE2LjEwNzYgTCA1NS40NDA4LDE2LjIyNDIgTCA1NS4yODk2LDE2LjM1NDIgTCA1NS4xNSwxNi40OTY4IEwgNTUuMDIzMywxNi42NTA4IEwgNTQuOTEwMiwxNi44MTUxIEwgNTQuODExOCwxNi45ODg2IEwgNTQuNzI4NSwxNy4xNjk5IEwgNTQuNjYxMiwxNy4zNTc2IEwgNTQuNjEwMywxNy41NTA1IEwgNTQuNTc2MSwxNy43NDcgTCA1NC41NTksMTcuOTQ1NyBMIDU0LjU1OSwxOC4xNDUyIEwgNTQuNTc2MSwxOC4zNDM5IEwgNTQuNjEwMywxOC41NDA0IEwgNTQuNjYxMiwxOC43MzMzIEwgNTQuNzI4NSwxOC45MjExIEwgNTQuODExOCwxOS4xMDIzIEwgNTQuOTEwMiwxOS4yNzU4IEwgNTUuMDIzMywxOS40NDAxIEwgNTUuMTUsMTkuNTk0MSBMIDU1LjI4OTYsMTkuNzM2NyBMIDU1LjQ0MDgsMTkuODY2NyBMIDU1LjYwMjcsMTkuOTgzMyBMIDU1Ljc3NCwyMC4wODU1IEwgNTUuOTUzNCwyMC4xNzI2IEwgNTYuMTM5NywyMC4yNDM5IEwgNTYuMzMxNCwyMC4yOTkgTCA1Ni41MjcxLDIwLjMzNzQgTCA1Ni43MjU1LDIwLjM1ODggTCA1Ni45MjQ5LDIwLjM2MzEgTCA1Ny4xMjM5LDIwLjM1MDIgTCA1Ny4zMjExLDIwLjMyMDMgTCA1Ny41MTUsMjAuMjczNSBMIDU3LjcwNDIsMjAuMjEwMyBMIDU3Ljg4NzIsMjAuMTMxIEwgNTguMDYyOCwyMC4wMzYyIEwgNTguMjI5NSwxOS45MjY3IEwgNTguMzg2MiwxOS44MDMzIEwgNTguNTMxNywxOS42NjY5IEwgNTguNjY1LDE5LjUxODUgTCA1OC43ODUsMTkuMzU5MiBMIDU4Ljg5MDksMTkuMTkwMSBMIDU4Ljk4MTgsMTkuMDEyNiBMIDU5LjA1NzEsMTguODI3OSBMIDU5LjExNjMsMTguNjM3NCBMIDU5LjE1ODksMTguNDQyNSBMIDU5LjE4NDYsMTguMjQ0NyBMIDU5LjE5MzIsMTguMDQ1NSBMIDU2Ljg3NSwxOC4wNDU1IFonIHN0eWxlPSdmaWxsOiMwMDAwMDA7ZmlsbC1ydWxlOmV2ZW5vZGQ7ZmlsbC1vcGFjaXR5PTE7c3Ryb2tlOiMwMDAwMDA7c3Ryb2tlLXdpZHRoOjJweDtzdHJva2UtbGluZWNhcDpidXR0O3N0cm9rZS1saW5lam9pbjptaXRlcjtzdHJva2Utb3BhY2l0eToxOycgLz4KPHBhdGggZD0nTSA0NC4zMTgyLDE4LjA0NTUgTCA0NC4zMDk2LDE3Ljg0NjIgTCA0NC4yODM5LDE3LjY0ODQgTCA0NC4yNDEzLDE3LjQ1MzUgTCA0NC4xODIxLDE3LjI2MyBMIDQ0LjEwNjgsMTcuMDc4MyBMIDQ0LjAxNTksMTYuOTAwOCBMIDQzLjkxLDE2LjczMTcgTCA0My43OSwxNi41NzI0IEwgNDMuNjU2NywxNi40MjQgTCA0My41MTEyLDE2LjI4NzYgTCA0My4zNTQ1LDE2LjE2NDIgTCA0My4xODc4LDE2LjA1NDcgTCA0My4wMTIyLDE1Ljk1OTkgTCA0Mi44MjkyLDE1Ljg4MDcgTCA0Mi42NCwxNS44MTc0IEwgNDIuNDQ2MSwxNS43NzA2IEwgNDIuMjQ4OSwxNS43NDA3IEwgNDIuMDQ5OSwxNS43Mjc4IEwgNDEuODUwNSwxNS43MzIxIEwgNDEuNjUyMSwxNS43NTM1IEwgNDEuNDU2NCwxNS43OTE5IEwgNDEuMjY0NywxNS44NDcgTCA0MS4wNzg0LDE1LjkxODMgTCA0MC44OTksMTYuMDA1NCBMIDQwLjcyNzcsMTYuMTA3NiBMIDQwLjU2NTgsMTYuMjI0MiBMIDQwLjQxNDYsMTYuMzU0MiBMIDQwLjI3NSwxNi40OTY4IEwgNDAuMTQ4MywxNi42NTA4IEwgNDAuMDM1MiwxNi44MTUxIEwgMzkuOTM2OCwxNi45ODg2IEwgMzkuODUzNSwxNy4xNjk5IEwgMzkuNzg2MiwxNy4zNTc2IEwgMzkuNzM1MywxNy41NTA1IEwgMzkuNzAxMSwxNy43NDcgTCAzOS42ODQsMTcuOTQ1NyBMIDM5LjY4NCwxOC4xNDUyIEwgMzkuNzAxMSwxOC4zNDM5IEwgMzkuNzM1MywxOC41NDA0IEwgMzkuNzg2MiwxOC43MzMzIEwgMzkuODUzNSwxOC45MjExIEwgMzkuOTM2OCwxOS4xMDIzIEwgNDAuMDM1MiwxOS4yNzU4IEwgNDAuMTQ4MywxOS40NDAxIEwgNDAuMjc1LDE5LjU5NDEgTCA0MC40MTQ2LDE5LjczNjcgTCA0MC41NjU4LDE5Ljg2NjcgTCA0MC43Mjc3LDE5Ljk4MzMgTCA0MC44OTksMjAuMDg1NSBMIDQxLjA3ODQsMjAuMTcyNiBMIDQxLjI2NDcsMjAuMjQzOSBMIDQxLjQ1NjQsMjAuMjk5IEwgNDEuNjUyMSwyMC4zMzc0IEwgNDEuODUwNSwyMC4zNTg4IEwgNDIuMDQ5OSwyMC4zNjMxIEwgNDIuMjQ4OSwyMC4zNTAyIEwgNDIuNDQ2MSwyMC4zMjAzIEwgNDIuNjQsMjAuMjczNSBMIDQyLjgyOTIsMjAuMjEwMyBMIDQzLjAxMjIsMjAuMTMxIEwgNDMuMTg3OCwyMC4wMzYyIEwgNDMuMzU0NSwxOS45MjY3IEwgNDMuNTExMiwxOS44MDMzIEwgNDMuNjU2NywxOS42NjY5IEwgNDMuNzksMTkuNTE4NSBMIDQzLjkxLDE5LjM1OTIgTCA0NC4wMTU5LDE5LjE5MDEgTCA0NC4xMDY4LDE5LjAxMjYgTCA0NC4xODIxLDE4LjgyNzkgTCA0NC4yNDEzLDE4LjYzNzQgTCA0NC4yODM5LDE4LjQ0MjUgTCA0NC4zMDk2LDE4LjI0NDcgTCA0NC4zMTgyLDE4LjA0NTUgTCA0MiwxOC4wNDU1IFonIHN0eWxlPSdmaWxsOiMwMDAwMDA7ZmlsbC1ydWxlOmV2ZW5vZGQ7ZmlsbC1vcGFjaXR5PTE7c3Ryb2tlOiMwMDAwMDA7c3Ryb2tlLXdpZHRoOjJweDtzdHJva2UtbGluZWNhcDpidXR0O3N0cm9rZS1saW5lam9pbjptaXRlcjtzdHJva2Utb3BhY2l0eToxOycgLz4KPC9zdmc+Cg== [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 5
- 229910052796 boron Inorganic materials 0.000 description 5
- 229910052751 metals Inorganic materials 0.000 description 5
- 239000002184 metals Substances 0.000 description 5
- TXKRDMUDKYVBLB-UHFFFAOYSA-N methane;titanium Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 C.[Ti] TXKRDMUDKYVBLB-UHFFFAOYSA-N 0.000 description 5
- 238000007254 oxidation reactions Methods 0.000 description 5
- 238000002441 X-ray diffraction Methods 0.000 description 4
- 150000002500 ions Chemical class 0.000 description 4
- 230000003647 oxidation Effects 0.000 description 4
- 238000004220 aggregation Methods 0.000 description 3
- 230000002776 aggregation Effects 0.000 description 3
- 239000006185 dispersions Substances 0.000 description 3
- 239000011521 glasses Substances 0.000 description 3
- 238000010884 ion-beam techniques Methods 0.000 description 3
- 239000010410 layers Substances 0.000 description 3
- 239000000155 melts Substances 0.000 description 3
- 239000011259 mixed solutions Substances 0.000 description 3
- 239000001308 nitrogen Substances 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N nitrogen Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 3
- 238000005245 sintering Methods 0.000 description 3
- -1 titanium ions Chemical class 0.000 description 3
- 229910034327 TiC Inorganic materials 0.000 description 2
- 238000009792 diffusion process Methods 0.000 description 2
- 239000010419 fine particles Substances 0.000 description 2
- 230000004907 flux Effects 0.000 description 2
- 239000007788 liquids Substances 0.000 description 2
- 238000010309 melting process Methods 0.000 description 2
- 239000010932 platinum Substances 0.000 description 2
- NRTOMJZYCJJWKI-UHFFFAOYSA-N titanium nitride Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 [Ti]#N NRTOMJZYCJJWKI-UHFFFAOYSA-N 0.000 description 2
- 229910010055 TiB Inorganic materials 0.000 description 1
- 238000004458 analytical methods Methods 0.000 description 1
- XKRFYHLGVUSROY-UHFFFAOYSA-N argon Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 1
- 239000004199 argon Substances 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- QXUAMGWCVYZOLV-UHFFFAOYSA-N boride(3-) Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 [B-3] QXUAMGWCVYZOLV-UHFFFAOYSA-N 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 125000001309 chloro group Chemical group data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 Cl* 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 238000000113 differential scanning calorimetry Methods 0.000 description 1
- 239000011363 dried mixtures Substances 0.000 description 1
- 101710042769 eIF-6 Proteins 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000011888 foils Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000006011 modification reactions Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N oxygen Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,PD94bWwgdmVyc2lvbj0nMS4wJyBlbmNvZGluZz0naXNvLTg4NTktMSc/Pgo8c3ZnIHZlcnNpb249JzEuMScgYmFzZVByb2ZpbGU9J2Z1bGwnCiAgICAgICAgICAgICAgeG1sbnM9J2h0dHA6Ly93d3cudzMub3JnLzIwMDAvc3ZnJwogICAgICAgICAgICAgICAgICAgICAgeG1sbnM6cmRraXQ9J2h0dHA6Ly93d3cucmRraXQub3JnL3htbCcKICAgICAgICAgICAgICAgICAgICAgIHhtbG5zOnhsaW5rPSdodHRwOi8vd3d3LnczLm9yZy8xOTk5L3hsaW5rJwogICAgICAgICAgICAgICAgICB4bWw6c3BhY2U9J3ByZXNlcnZlJwp3aWR0aD0nODVweCcgaGVpZ2h0PSc4NXB4JyB2aWV3Qm94PScwIDAgODUgODUnPgo8IS0tIEVORCBPRiBIRUFERVIgLS0+CjxyZWN0IHN0eWxlPSdvcGFjaXR5OjEuMDtmaWxsOiNGRkZGRkY7c3Ryb2tlOm5vbmUnIHdpZHRoPSc4NScgaGVpZ2h0PSc4NScgeD0nMCcgeT0nMCc+IDwvcmVjdD4KPHBhdGggY2xhc3M9J2JvbmQtMCcgZD0nTSAyMS43MDkxLDQ3Ljg5MjcgTCA2Mi4yOTA5LDQ3Ljg5MjcnIHN0eWxlPSdmaWxsOm5vbmU7ZmlsbC1ydWxlOmV2ZW5vZGQ7c3Ryb2tlOiNFODQyMzU7c3Ryb2tlLXdpZHRoOjJweDtzdHJva2UtbGluZWNhcDpidXR0O3N0cm9rZS1saW5lam9pbjptaXRlcjtzdHJva2Utb3BhY2l0eToxJyAvPgo8cGF0aCBjbGFzcz0nYm9uZC0wJyBkPSdNIDIxLjcwOTEsMzYuMTA3MyBMIDYyLjI5MDksMzYuMTA3Mycgc3R5bGU9J2ZpbGw6bm9uZTtmaWxsLXJ1bGU6ZXZlbm9kZDtzdHJva2U6I0U4NDIzNTtzdHJva2Utd2lkdGg6MnB4O3N0cm9rZS1saW5lY2FwOmJ1dHQ7c3Ryb2tlLWxpbmVqb2luOm1pdGVyO3N0cm9rZS1vcGFjaXR5OjEnIC8+Cjx0ZXh0IGRvbWluYW50LWJhc2VsaW5lPSJjZW50cmFsIiB0ZXh0LWFuY2hvcj0iZW5kIiB4PScxOS43NDQ5JyB5PSc0NC45NDY0JyBzdHlsZT0nZm9udC1zaXplOjE5cHg7Zm9udC1zdHlsZTpub3JtYWw7Zm9udC13ZWlnaHQ6bm9ybWFsO2ZpbGwtb3BhY2l0eToxO3N0cm9rZTpub25lO2ZvbnQtZmFtaWx5OnNhbnMtc2VyaWY7ZmlsbDojRTg0MjM1JyA+PHRzcGFuPk88L3RzcGFuPjwvdGV4dD4KPHRleHQgZG9taW5hbnQtYmFzZWxpbmU9ImNlbnRyYWwiIHRleHQtYW5jaG9yPSJzdGFydCIgeD0nNjQuMjU1MScgeT0nNDQuOTQ2NCcgc3R5bGU9J2ZvbnQtc2l6ZToxOXB4O2ZvbnQtc3R5bGU6bm9ybWFsO2ZvbnQtd2VpZ2h0Om5vcm1hbDtmaWxsLW9wYWNpdHk6MTtzdHJva2U6bm9uZTtmb250LWZhbWlseTpzYW5zLXNlcmlmO2ZpbGw6I0U4NDIzNScgPjx0c3Bhbj5PPC90c3Bhbj48L3RleHQ+Cjwvc3ZnPgo= O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- 239000008188 pellets Substances 0.000 description 1
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 239000011241 protective layers Substances 0.000 description 1
- 238000006722 reduction reactions Methods 0.000 description 1
- 238000000527 sonication Methods 0.000 description 1
- 238000002525 ultrasonication Methods 0.000 description 1
- 238000009827 uniform distribution Methods 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES; PREPARATION OF CARBON BLACK; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/36—Compounds of titanium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
Abstract
Description
The present invention relates to a high hardness coating powder and a method for producing the same, and more particularly, to a method for easily coating a coating material on the surface of a base material and a powder produced by the method.
The cutting tool wears as the cutting process continues. The cutting tool is therefore formed using a hard material. Typically, a cutting tool is formed by mixing and sintering a base metal such as diamond and a metal.
The bonding force between the base metal and the metal is important for the durability of the cutting tool. In addition, since the sintering temperature is a high temperature, high temperature safety of the base material and prevention of oxidation of the base material surface are important.
To this end, techniques for forming a coating layer on the surface of the base material before mixing and sintering the base metal and metal have been studied. The surface of the base material can be coated to prevent oxidation, to improve the bonding strength with the metal, and to improve the high temperature safety.
However, when the particles of the base material are sub-micrometers, that is, fine particles of several nanometers to several micrometers, the base material agglomerates during the process of coating the coating material on the surface of the base material, and the coating material is unevenly coated on the surface of the base material, thereby coating the high hardness coating powder. There was a limit to getting.
This invention can provide the high hardness coating powder which can coat | cover a coating material on the surface of a base material, and its manufacturing method.
The present invention comprises the steps of (a) dissolving the first salt of chlorine (Cl) series, the second salt of fluorine (F) series in a solvent to form a solution, (b) a coating material containing a base material and titanium in the solution Mixing and drying, (c) placing the mixture obtained in step (b) into a reactor and (d) maintaining the reactor after heating to a predetermined temperature to melt the first salt and the second salt. Disclosed is a method for preparing a high hardness coating powder comprising the step of causing a molten salt reaction to occur.
In the present invention, the first salt may include at least two selected from the group consisting of KCl, NaCl, and BaCl 2.
In the present invention, the second salt may include at least one selected from the group consisting of NaF, K 2 TiF 6 and NaK 2 TiF 6 .
In the present invention, the solvent may include ethanol.
In the present invention, the step (d) may proceed at 800 ℃ to 1000 ℃.
In the present invention, the step (d) may proceed with the reaction while stirring the inside of the reactor in an Ar gas atmosphere.
In the present invention, the step (d) may be followed by the step of sonicating the powder obtained after the molten salt reaction in the reactor in distilled water and reacting with a hydrochloric acid solution.
In the present invention, after the step (d) may further comprise the step of removing the remaining coating material by a wet filling method.
In the present invention, after the step (d) may include the step of proceeding the crystallization by heat treatment in a hydrogen atmosphere.
In the present invention, the base material powder may include one selected from the group consisting of diamond, cubic boron nitride, and carbon nanotubes.
According to another aspect of the present invention there is disclosed a high hardness coating powder produced by the method of any one of the above methods.
The high hardness coating powder and the manufacturing method thereof according to the present invention can uniformly coat the coating material on the surface of the base material including the fine particles to obtain a high hardness coating powder having improved strength, improved surface properties and excellent high temperature safety.
1 is a flowchart sequentially illustrating a method for producing a high hardness coated powder of the present invention.
FIG. 2 is a diagram schematically illustrating an apparatus for describing the manufacturing method of FIG. 1 of FIG. 1.
3 is an enlarged view of a portion A of FIG. 1.
FIG. 4 is a photograph obtained by measuring an electron microscope of a powder formed according to a method of preparing a high hardness coating powder according to an embodiment of the present invention. FIG.
FIG. 5 is a diagram illustrating an X-ray diffraction pattern of the powder of FIG. 4.
FIG. 6 is a diagram of a powder formed according to a method for preparing high hardness coated powder according to another embodiment of the present invention, measured by an electron microscope. FIG.
FIG. 7 is a diagram illustrating an X-ray diffraction pattern of the powder of FIG. 6.
8 is a cross-sectional view of the powder of FIG. 6 using a focused ion beam (FIB).
9 is a cross-sectional view of the powder of FIG. 6 using a transmission electron microscope (TEM).
FIG. 10 is a diagram illustrating a measured component of part B of FIG. 9.
11 is a cross-sectional view of the powder of FIG. 6 after heat treatment using a transmission electron microscope.
FIG. 12 illustrates the limited field of view diffraction pattern of FIG. 11.
It is a figure for demonstrating the glass transition temperature of the powder of FIG.
14 is a view of a powder formed by a transmission electron microscope of a powder formed according to a method for producing a high hardness coated powder according to another embodiment of the present invention.
FIG. 15 is an enlarged view of C of FIG. 14.
FIG. 16 is a diagram illustrating a limited field of view diffraction pattern of the powder of FIG. 14.
<Brief description of symbols for the main parts of the drawings>
200: reactor 210: electric furnace
202: crucible 203: thermocouple
204: stirrer 205: gas inlet
206: gas outlet 310: molten salt
320: base material 330: covering material
Hereinafter, with reference to the embodiments of the present invention shown in the accompanying drawings will be described in detail the configuration and operation of the present invention.
1 is a flow chart sequentially showing a method for producing a high hardness coating powder of the present invention and FIG. 2 is a view schematically showing an apparatus for explaining the manufacturing method of FIG. 1 of FIG.
Referring to FIG. 1, in the method of preparing the high hardness coating powder according to the present embodiment, the first salt and the second salt are dissolved in a solvent to form a solution (101), and the base material and the coating material are mixed in a solution (102). ), Drying (103), placing the dried mixture into the reactor (104), heating and maintaining the reactor (105), removing residual salt (106), removing the residual coating material 107 and heat treating step 108.
Before the process proceeds, the members necessary for the manufacturing method according to the present embodiment are prepared.
The first salt is a chlorine-based salt and includes at least two selected from the group consisting of KCl, NaCl and BaCl 2. In the process of melting the salt as described below, two or more salts are selected to lower the melting temperature and ensure uniform distribution of the molten salt and high temperature safety. That is, the first salt may comprise two or more salts. That is, the first salt may be KCl and NaCl, NaCl and BaCl 2, and KCl and BaCl 2. The first salt may also be KCL and NaCl and BaCl 2.
The second salt comprises at least one selected from the group consisting of NaF, K 2 TiF 6 and NaK 2 TiF 6 .
The base material has particles of several micrometers or less and can be formed by using various materials. The base material includes any one selected from the group consisting of diamond, cubic boron nitride, and carbon nanotubes having excellent hardness.
First, for convenience of description, an embodiment of using diamond as a base material will be described.
The coating includes titanium. Titanium is coated on the surface of the base material particles containing diamond to prevent oxidation of the surface of the base material particles, to ensure safety at high temperatures, and to improve the bonding force between the base powder and the metal powder in forming a cutting tool later. The coating can be prepared in various forms. That is, the coating material may be in the form of powder, foil, pellets. However, the coating material is preferably in the form of a powder so that uniform melting occurs easily in the reactor.
After preparing each material, first, the second salt is dissolved in a solvent to form a solution. At this time, the solvent may be ethanol. The base metal powder containing diamond is then added to the solution and the coating material containing titanium is added to the solution.
This mixed solution is then stirred to make it homogeneous and dried to form a mixed powder.
The particle size of the base metal powder containing diamond is several micrometers or less. Preferably they are 5 nanometers or more and 5 micrometers or less.
If the size of the particles of the base metal powder containing diamond is less than 5 nanometers, due to van der Waals' forces between the base material powder particles, dispersion between the base material powder particles is difficult and aggregation occurs, and the base material powder particles are coated with the coating material. There is a limit. Therefore, the particle size of the base metal powder containing diamond is preferably 5 nanometers or more.
In addition, when the particle size of the base metal powder containing diamond exceeds 5 micrometers, the toughness of the cutting tool is reduced when forming the cutting tool using the base material. Therefore, the particle size of the base metal powder containing diamond is preferably 5 micrometers or less.
Since the particle size of the base material powder is small, the base material particles agglomerate with each other by van der Waals' force in the process of coating the surface of the base material particles with a coating material.
However, in this embodiment, first, the second salt, the base material and the coating material are dissolved by using ethanol to form a solution. This facilitates the dispersion of each particle. In particular, a uniform dispersion of each particle occurs during the process of forming the solution and then stirring it evenly. And it is possible to remove unnecessary solvent components through drying to form a mixed powder of the first salt, the second salt, the base material and the coating material in a uniform state.
Then, a process of melting the mixed powder is performed. 2 schematically illustrates a reactor in which mixed powder is added and a process is performed.
The reactor 200 includes an electric furnace 201, a crucible 202, a thermocouple 203, an agitator 204, a gas inlet 204, and a gas outlet 205. The mixed powder described above is placed in the crucible 202. The mixed powder in the crucible 202 may be melted by supplying heat from the electric furnace 201 surrounding the crucible 202. The electric furnace 201 is a method of supplying heat using electric energy. However, the present invention is not limited thereto, and various types of heat sources may be used as long as the heat necessary for melting the mixed powder of the crucible 202 can be supplied.
The thermocouple 203 may be used to measure the temperature in the process of melting and stirring the mixed powder and to adjust the heat supply amount of the electric furnace 201 for supplying heat to the crucible 202. The mixed powder is melted so that the reaction of melting the first salt and the second salt occurs at 800 ° C to 1000 ° C.
The melting temperature of a 1st salt, a 2nd salt is about 600 degreeC or more. In addition, the reaction rate due to diffusion of titanium atoms when the coating material containing titanium is melted is proportional to the temperature. In the melting temperature atmosphere below 800 ° C, the reaction rate due to diffusion of titanium atoms is reduced, and the uniformity of the coating layer formed after the coating material is coated on the base material is reduced. Therefore, the reaction in which the mixed powder is melted to melt the first salt and the second salt is controlled to occur at 800 ° C. or higher.
In addition, durability is weakened by brittleness of a base material in the atmosphere of temperature exceeding 1000 degreeC. Therefore, the reaction in which the mixed powder is melted to melt the first salt and the second salt is controlled to occur at 1000 ° C. or lower.
The stirrer 204 allows the first salt, the second salt, the base material and the coating material to be evenly stirred when the mixed powder is melted. The stirrer 204 preferably has the form of an impeller.
Argon (Ar) gas is introduced and discharged through the gas inlet 205 and the gas outlet 206. Through this, the melting reaction of the mixed powder in the crucible may proceed in an inert atmosphere.
3 is an enlarged view of A of FIG. 2. Referring to FIG. 3, the base material 320 and the coating material 330 are evenly distributed in the molten salt 310 in which the first salt and the second salt are melted.
In the crucible 202, the mixed powder is melted and maintained for a period of time, and the coating material is oxidized and reduced in a molten salt to coat the coating material on the surface of the base material. Specifically, the following reactions occur sequentially.
(1) Ti-> 2Ti 2+
(2) 2Ti 2+ -> Ti + Ti 4+
(3) C (diamond) + Ti-> TiC
First, the coating material is melted in the molten salt in which the first salt and the second salt are molten to cause a reaction in the above reaction (1). Particularly, when K 2 TiF 6 or NaK 2 TiF 6 is used as the second salt, the reaction of Ti + Ti 4+ -> 2Ti 2 occurs in the molten salt because the second salt forms tetravalent titanium ions.
(2) reaction occurs in the above reaction on the surface of the base metal powder. That is, titanium divalent ions formed in the molten salt are reduced on the surface of the base material. The produced titanium tetravalent ions again promote the oxidation of titanium in the molten salt.
Then, reaction of (3) occurs on the surface of the base material. That is, diamond and titanium react at a high temperature on the surface of the particles of the base metal including diamond to form titanium carbide. That is, the coating powder which coat | covered the coating material is formed on the surface of a base material.
The coated powder recovered from the crucible 202 is in a lump state immediately after the high temperature melting process is finished. In addition, since the remaining salts and coating materials aggregate together with the coating powder without reacting with the base metal in the melting process, a process of separating these is necessary.
First, in order to remove the remaining salt, the coating powder, the remaining salt and the powder containing the remaining coating material are put in distilled water and stirred. Ultrasonication is then performed to remove any remaining salt. At this time, after the sonication, a hydrochloric acid solution may be added to proceed the process quickly and easily.
After removing the remaining salt, it is not reacted with the base material to remove the remaining coating material. The remaining coating material powder can be easily removed through the wet coloring. In other words, the remaining titanium powder and the coating powder are agglomerated in a liquid such as distilled water to fill the liquid powder to remove the remaining titanium powder.
Then use a centrifuge to remove the solution used for wet filling. Distilled water can then be added to dissolve and remove traces of the remaining salt.
The coated powder is then recovered by vacuum filtering. That is, the diamond powder coated with titanium is recovered.
The recovered coating powder is heat-treated after drying in a vacuum atmosphere. The heat treatment is performed in a hydrogen atmosphere at a temperature of 800 ° C. or higher. Through this, titanium carbide formed on the surface of the base material is crystallized, and adhesion between the base material and the coating material is improved and durability is improved.
FIG. 4 is a photograph obtained by measuring an electron microscope of a powder formed according to a method of preparing a high hardness coated powder according to an embodiment of the present invention, and FIG. 5 is an X-ray diffraction pattern of the powder of FIG. 4. Drawing.
Specifically, KCl, NaCl and BaCl 2 were used as the first salt, and NaF and NaK 2 TiF 6 were used as the second salt. KCl, NaCl and BaCl 2 were each prepared with 10 g, and 10 g of NaF and 5 g of NaK 2 TiF 6 were prepared. The base material contains diamond, and the diamond particles have a size of 1.5 micrometers or less. The coating material was prepared 2g of titanium in powder form and the titanium powder was to have a particle size of 100mesh.
4 (a) is a diamond powder before using the manufacturing method according to the present embodiment, Figure 4 (b) is a diamond powder coated with a coating material by the manufacturing method according to the present embodiment, Figure 4 (c) Is a scanning electron microscope (SEM) photograph which shows enlarged FIG. 4 (b).
Comparing Fig. 4 (a) with Fig. 4 (b) and Fig. 4 (c) it can be seen that the coating material is coated on the surface of each particle of the base material powder containing diamond. 5, these components can be easily identified. Fig. 5 (a) shows the diamond powder before coating by the manufacturing method according to the present embodiment, and Fig. 5 (b) shows the diamond powder after coating with the manufacturing method according to the present embodiment. The peaks indicated by the inverted triangle are present in both (a) and (b) of FIG. 5, indicating the diamond component. However, the peaks indicated by circles are present only in Fig. 5 (b), which indicates titanium carbide. Through this, it can be seen that titanium was evenly coated on the surface of the fine diamond particles by the manufacturing method according to the present embodiment.
FIG. 6 is a diagram illustrating a powder formed according to a method of preparing a high hardness coated powder according to another embodiment of the present invention with an electron microscope, and FIG. 7 is a diagram illustrating an X-ray diffraction pattern of the powder of FIG. 6.
For convenience of explanation, the following description will focus on differences from the above-described embodiment. This embodiment has a difference in that the base material using cubic boron nitride rather than diamond as compared with the above-described embodiment.
As in the above embodiment, first and second salts are dissolved in a solvent to form a solution. At this time, the solvent may be ethanol. Then, the base metal powder containing cubic boron nitride is put into the solution, and the coating material containing titanium is put into the solution. This mixed solution is then stirred to make it homogeneous and dried to form a mixed powder.
The particle size of the base metal powder containing cubic boron nitride is several micrometers or less. Preferably they are 50 nanometers or more and 5 micrometers or less.
If the size of the particles of the base material powder containing cubic boron nitride is less than 50 nanometers, it is difficult to disperse due to van der Waals' forces between the cubic boron nitride particles and aggregation occurs, so that there is a limit to coating the coating material on the base material powder particles. have. Therefore, the particle size of the base metal powder containing cubic boron nitride is preferably 50 nanometers or more.
In addition, when the size of the particles of the base metal powder containing boron cubic boron exceeds 5 micrometers, the toughness of the cutting tool is reduced when forming the cutting tool using the base material. Therefore, the particle size of the base metal powder containing cubic boron nitride is preferably 5 micrometers or less.
In the crucible 202, the mixed powder is melted and maintained for a period of time, so that the coating material is oxidized and reduced in the molten salt so that the coating material is coated on the surface of the base material. Specifically, the following reactions occur.
(1) Ti-> 2Ti 2+
(2) 2Ti 2+ -> Ti + Ti 4+
(3) 3Ti + 2BN-> TiB 2 + 2TiN
First, the coating material is melted in the molten salt in which the first salt and the second salt are molten to cause a reaction in the above reaction (1). Particularly, when K 2 TiF 6 or NaK 2 TiF 6 is used as the second salt, the reaction of Ti + Ti 4+ -> 2Ti 2 occurs in the molten salt because the second salt forms tetravalent titanium ions.
(2) reaction occurs in the above reaction on the surface of the base metal powder. That is, titanium divalent ions formed in the molten salt are reduced on the surface of the base material.
Then, reaction of (3) occurs on the surface of the base material. That is, boron and titanium, nitrogen and titanium react at a high temperature on the surface of the base material particles containing cubic boron nitride to form titanium boride and titanium nitride.
Subsequently, subsequent steps such as residual salt removal, residual coating material removal, and heat treatment are performed to obtain a high hardness coating powder having a coating material coated on the surface of the base material. Details of subsequent processes are the same as in the above-described embodiment and thus will be omitted.
6 (a) is a cubic boron nitride powder before using the manufacturing method according to the present embodiment, Figure 6 (b) is a cubic boron nitride powder coated with a coating material in the manufacturing method according to the present embodiment, Fig. 6 (c) is a scanning electron microscope (SEM) photograph showing an enlarged view of FIG. 6 (b).
Comparing FIG. 6 (a), FIG. 6 (b) and FIG. 6 (c), it can be seen that the coating material is coated on the surfaces of the particles of the base metal powder containing cubic boron nitride. Referring to FIG. 7, these components can be easily identified. (A) of FIG. 7 shows a cubic boron nitride powder before coating by the manufacturing method which concerns on a present Example, FIG. 7 (b) shows the cubic boron nitride powder after coating by a manufacturing method which concerns on a present Example. will be. The peaks indicated by the inverted triangle are present in both (a) and (b) of FIG. 7, indicating a cubic boron nitride component. However, the peaks indicated by circles are present only in FIG. 7B, which indicates titanium nitride. Through this, it can be seen that titanium was evenly coated on the surface of the fine cubic boron nitride particles by the manufacturing method according to the present embodiment.
8 is a cross-sectional view of the powder of FIG. 6 using a focused ion beam (FIB).
Referring to FIG. 8, it can be seen that a coating layer containing titanium formed on the surface of the cubic boron nitride is uniformly formed. In FIG. 8, a part indicated by a) is a layer for protecting the surface of the sample from the focused ion beam FIB with a protective layer formed of platinum Pt for experiment. In Figure 8 b) is the coating layer and in Figure 8 c) is the base material. Referring to FIG. 8, the coating layer has a thickness of 200 nm.
FIG. 9 is a diagram illustrating a cross section of the powder of FIG. 6 using a transmission electron microscope (TEM), and FIG. 10 is a diagram illustrating a component of part B of FIG. 9.
In FIG. 9, (a) shows a base material part, (c) shows a covering layer part, and (b) shows the boundary of a base material and a covering layer. It is a graph which shows the component analysis result of each part. In FIG. 10, (a) is boron, (b) is nitrogen, (c) is oxygen, and (d) is titanium.
Referring to Figure 10 (a) since the base material includes a cubic boron nitride, nitrogen, boron is the main component. At the boundary (b), titanium as a coating material increases, and titanium is most present at the coating layer (c). Through this, it can be seen that the coating material containing titanium was stably coated on the surface of the particles of the base material containing cubic boron nitride.
11 is a cross-sectional view of the powder of FIG. 6 after heat treatment using a transmission electron microscope, and FIG. 12 is a view illustrating the limited field diffraction pattern of FIG. 11. In Fig. 11, a) indicates the base material and b) indicates the coating layer. Referring to FIGS. 11 and 12, the titanium containing coating layer has a polycrystalline structure composed of crystals having a size of several tens of nanometers or less.
It is a figure for demonstrating the glass transition temperature of the powder of FIG. Specifically, the left Y-axis coordinate of FIG. 13 indicates that the heat flux is measured by differential scanning calorimetry (DSC), and shows that the heat flux decreases as the temperature increases, and the right Y-axis of FIG. The coordinates are values obtained by differentiating the heat flow rate value of the left Y coordinate, and change in value according to a minute temperature change. Referring to Figure 13, the glass transition temperature is about 950 ℃. This means that the coating layer containing titanium on the cubic boron nitride surface was crystallized at around 950 ° C in an amorphous state. The present invention can easily form a coating layer crystallized as described above by heat-treating the coated base material powder in a hydrogen atmosphere.
FIG. 14 is a view of a powder formed according to a method of preparing a high hardness coated powder according to another embodiment of the present invention with a transmission electron microscope, and FIG. 15 is an enlarged view of C of FIG. 14. FIG. 16 is a diagram illustrating a limited field of view diffraction pattern of the powder of FIG. 14.
For convenience of explanation, the following description will focus on differences from the above-described embodiment. This embodiment has a difference in that the base material using carbon nanotubes other than diamond or cubic boron nitride as compared with the above-described embodiment.
As in the above embodiment, first and second salts are dissolved in a solvent to form a solution. At this time, the solvent may be ethanol. The base material containing the carbon nanotubes is then added to the solution and the coating material containing titanium is added to the solution. This mixed solution is then stirred to make it homogeneous and dried to form a mixed powder.
The particle size of the base metal powder containing the carbon nanotubes is several micrometers or less. Preferably they are 5 nanometers or more and 50 nanometers or less.
If the particle size of the base metal powder containing carbon nanotubes is less than 5 nanometers, the base metal powder particles are not dispersed well due to van der Waals' forces between the respective base metal powder particles, and aggregation occurs between the particles. There is a limit to coating the coating material. Therefore, the particle size of the base metal powder containing diamond is preferably 5 nanometers or more.
In addition, when the size of the particles of the base metal powder containing the carbon nanotube exceeds 50 nanometers, the toughness of the cutting tool is reduced when forming the cutting tool using the base material. Therefore, the particle size of the base metal powder containing the carbon nanotubes is preferably 5 micrometers or less.
In the crucible 202, the mixed powder is melted and maintained for a period of time so that the coating material undergoes oxidation and reduction reactions in the molten salt so that the coating material is coated on the surface of the base material. Specifically, the following reactions occur.
(1) Ti-> 2Ti 2+
(2) 2Ti 2+ -> Ti + Ti 4+
(3) Ti + C (carbon nanotube)-> TiC
First, the coating material is melted in the molten salt in which the first salt and the second salt are molten to cause a reaction in the above reaction (1). Particularly, when K 2 TiF 6 or NaK 2 TiF 6 is used as the second salt, the reaction of Ti + Ti 4+ -> 2Ti 2 occurs in the molten salt because the second salt forms tetravalent titanium ions.
(2) reaction occurs in the above reaction on the surface of the base metal powder. That is, titanium divalent ions formed in the molten salt are reduced on the surface of the base material.
Then, reaction of (3) occurs on the surface of the base material. That is, carbon and titanium react at a high temperature on the surface of the particles of the base metal including the carbon nanotubes to form titanium carbide.
Subsequently, subsequent steps such as residual salt removal, residual coating material removal, and heat treatment are performed to obtain a high hardness coating powder having a coating material coated on the surface of the base material. Details of subsequent processes are the same as in the above-described embodiment and thus will be omitted.
14 and 15, it can be seen that a coating layer is formed on the surface of the carbon nanotube as the base material. In addition, it can be seen from FIG. 16 that the titanium-containing coating material is coated on the surface of the carbon nanotube to form titanium carbide in the coating layer.
Through this, it can be seen that titanium was evenly coated on the surface of the fine cubic boron nitride particles by the manufacturing method according to the present embodiment.
Although described with reference to the embodiment shown in the drawings it is merely exemplary, those skilled in the art will understand that various modifications and equivalent other embodiments are possible from this. Therefore, the true technical protection scope of the present invention will be defined by the technical spirit of the appended claims.
Carbon nanotubes have been studied for use in cutting tools as materials having high strength, high modulus of elasticity, high conductivity, and high thermal conductivity. However, when carbon nanotubes are used as the base material, evenly dispersed and bonding strength at the interface with the coating material is a problem.
In this embodiment, the coating material containing titanium can be uniformly coat | covered on the surface of the base material containing a carbon nanotube. Through this, it is possible to easily form a high hardness coating powder with improved hardness and surface properties.
Claims (14)
- (a) dissolving a first salt of chlorine (Cl) series and a second salt of fluorine (F) series in a solvent to form a solution;(b) mixing and drying the base material and a coating material containing titanium in the solution;(c) placing the mixture obtained in step (b) into a reactor; And(d) a method of producing a high hardness coating powder comprising heating and maintaining the reactor at a predetermined temperature to cause a molten salt reaction in which the first salt and the second salt are melted.
- According to claim 1,Wherein said first salt comprises at least two selected from the group consisting of KCl, NaCl and BaCl 2.
- According to claim 1,Wherein said second salt comprises at least one selected from the group consisting of NaF, K 2 TiF 6 and NaK 2 TiF 6 .
- According to claim 1,The solvent is a method for producing a high hardness coating powder comprising ethanol;
- According to claim 1,Step (d) is a method for producing a high hardness coating powder proceeds from 800 ℃ to 1000 ℃.
- According to claim 1,Step (d) is a method for producing a high hardness coating powder to proceed with the reaction while stirring the inside of the reactor in an Ar gas atmosphere.
- The method of claim 1Performing the step (d) and then putting the powder obtained after the molten salt reaction in the reactor into distilled water and performing ultrasonic treatment; AndA method of producing a high hardness coating powder comprising the step of reacting with a hydrochloric acid solution.
- The method of claim 1Removing the coating material remaining by the wet filling method after the step (d) further comprising the method of producing a hard coating powder.
- The method of claim 1After the step (d) and the heat treatment in a hydrogen atmosphere comprising the step of proceeding the crystallization method of producing a high hardness coating powder.
- The method of claim 1The base material powder is a method for producing a high hardness coating powder comprising a freezing one selected from the group consisting of diamond, cubic boron nitride and carbon nanotubes.
- The method of claim 1The base material powder is a method for producing a high hardness coating powder comprising diamond particles having a size of 5 nanometers to 5 micrometers.
- The method of claim 1The base material powder is a method for producing a high hardness coating powder comprising cubic boron nitride particles having a size of 50 nanometers to 5 micrometers.
- The method of claim 1The base material powder is a method of producing a high hardness coating powder comprising carbon nanotube particles having a size of 5 nanometers to 50 nanometers.
- The high hardness coating powder manufactured by the manufacturing method of any one of Claims 1-13.
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR20080113468A KR101492969B1 (en) | 2008-11-14 | 2008-11-14 | High hardness coated powder and method of manufacturing the same |
KR10-2008-0113468 | 2008-11-14 |
Publications (3)
Publication Number | Publication Date |
---|---|
WO2010056077A2 WO2010056077A2 (en) | 2010-05-20 |
WO2010056077A3 WO2010056077A3 (en) | 2010-08-19 |
WO2010056077A9 true WO2010056077A9 (en) | 2010-10-07 |
Family
ID=42170548
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/KR2009/006719 WO2010056077A2 (en) | 2008-11-14 | 2009-11-16 | High-hardness coating powder, and preparation method thereof |
Country Status (2)
Country | Link |
---|---|
KR (1) | KR101492969B1 (en) |
WO (1) | WO2010056077A2 (en) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR101701916B1 (en) | 2014-01-06 | 2017-02-03 | 한국과학기술연구원 | a method for preparing a carbide-coated diamond particle and a diamond prepared thereby |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ZA7801390B (en) * | 1978-03-09 | 1979-04-25 | De Beers Ind Diamond | The metal coating of abrasive particles |
US5106392A (en) * | 1991-03-14 | 1992-04-21 | General Electric Company | Multigrain abrasive particles |
JP2002317196A (en) * | 2001-04-19 | 2002-10-31 | Minebea Co Ltd | Abrasive cleaning composition |
US20050211950A1 (en) * | 2004-03-24 | 2005-09-29 | Cabot Microelectronics Corporation | Chemical-mechanical polishing composition and method for using the same |
-
2008
- 2008-11-14 KR KR20080113468A patent/KR101492969B1/en active IP Right Grant
-
2009
- 2009-11-16 WO PCT/KR2009/006719 patent/WO2010056077A2/en active Application Filing
Also Published As
Publication number | Publication date |
---|---|
WO2010056077A3 (en) | 2010-08-19 |
KR101492969B1 (en) | 2015-02-16 |
WO2010056077A2 (en) | 2010-05-20 |
KR20100054511A (en) | 2010-05-25 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CA2624887C (en) | Crucible for the crystallization of silicon and process for making the same | |
JP5405115B2 (en) | Method for producing grain refined mother alloy | |
US4812166A (en) | Process for producing ultrafine particles of metals, metal compounds and ceramics and apparatus used therefor | |
Ding et al. | Novel synthesis and characterization of silicon carbide nanowires on graphite flakes | |
Seeger et al. | SiOx-coating of carbon nanotubes at room temperature | |
EP2058289B1 (en) | Strongly adhesive silicium nitride release layer | |
Lee et al. | Semiconductor nanowires from oxides | |
Tsuzuki et al. | Synthesis of Cr2O3 nanoparticles by mechanochemical processing | |
US4808372A (en) | In situ process for producing a composite containing refractory material | |
Meng et al. | Growth and characterization of nanostructured β-SiC via carbothermal reduction of SiO2 xerogels containing carbon nanoparticles | |
Siddiqi et al. | The influence of iron on the preparation of silicon nitride from silica | |
Jian-Feng et al. | Influence of the preparation temperature on the phase, microstructure and anti-oxidation property of a SiC coating for C/C composites | |
US8012252B2 (en) | Durable hard coating containing silicon nitride | |
Sung et al. | Alpha-case formation mechanism on titanium investment castings | |
US8673053B2 (en) | Method of hardening an interface of carbon material using nano silicon carbide coating | |
JP5059602B2 (en) | Silicon crystallization crucible | |
Urena et al. | Oxidation treatments for SiC particles used as reinforcement in aluminium matrix composites | |
Bando et al. | Insulatingnanocables': Invar Fe–Ni alloy nanorods inside BN nanotubes | |
WO2012064102A2 (en) | Graphene-coated steel sheet, and method for manufacturing same | |
CN1308232C (en) | Preparation method of transition metal carbide material | |
Chakraborty et al. | Development of silicide coating over molybdenum based refractory alloy and its characterization | |
EP1786729A1 (en) | Metal carbides and process for producing same | |
TW200914371A (en) | Processing of fine silicon powder to produce bulk silicon | |
Zhang et al. | A novel fabrication technology of in situ TiB2/6063Al composites: high energy ball milling and melt in situ reaction | |
KR20140004067A (en) | Silicon melt contacting member and process for production thereof, and process for production of crystalline silicon |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
121 | Ep: the epo has been informed by wipo that ep was designated in this application |
Ref document number: 09826309 Country of ref document: EP Kind code of ref document: A2 |
|
NENP | Non-entry into the national phase in: |
Ref country code: DE |
|
122 | Ep: pct app. not ent. europ. phase |
Ref document number: 09826309 Country of ref document: EP Kind code of ref document: A2 |