WO2010004142A3 - Nanonitrure de bore cubique - Google Patents
Nanonitrure de bore cubique Download PDFInfo
- Publication number
- WO2010004142A3 WO2010004142A3 PCT/FR2009/000852 FR2009000852W WO2010004142A3 WO 2010004142 A3 WO2010004142 A3 WO 2010004142A3 FR 2009000852 W FR2009000852 W FR 2009000852W WO 2010004142 A3 WO2010004142 A3 WO 2010004142A3
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- boron nitride
- nanoscale
- cubic boron
- gpa
- pressure
- Prior art date
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/06—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron
- C01B21/064—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron with boron
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
- C04B35/58—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides
- C04B35/583—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides based on boron nitride
- C04B35/5831—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides based on boron nitride based on cubic boron nitrides or Wurtzitic boron nitrides, including crystal structure transformation of powder
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/64—Burning or sintering processes
- C04B35/645—Pressure sintering
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K3/00—Materials not provided for elsewhere
- C09K3/14—Anti-slip materials; Abrasives
- C09K3/1409—Abrasive particles per se
- C09K3/1418—Abrasive particles per se obtained by division of a mass agglomerated by sintering
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/76—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by a space-group or by other symmetry indications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
- C01P2002/82—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by IR- or Raman-data
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/38—Non-oxide ceramic constituents or additives
- C04B2235/3852—Nitrides, e.g. oxynitrides, carbonitrides, oxycarbonitrides, lithium nitride, magnesium nitride
- C04B2235/386—Boron nitrides
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6567—Treatment time
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/74—Physical characteristics
- C04B2235/78—Grain sizes and shapes, product microstructures, e.g. acicular grains, equiaxed grains, platelet-structures
- C04B2235/781—Nanograined materials, i.e. having grain sizes below 100 nm
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- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/95—Products characterised by their size, e.g. microceramics
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Ceramic Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Nanotechnology (AREA)
- Crystallography & Structural Chemistry (AREA)
- Structural Engineering (AREA)
- Inorganic Chemistry (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- Composite Materials (AREA)
- Ceramic Products (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Polishing Bodies And Polishing Tools (AREA)
Abstract
L'invention concerne un procédé de fabrication de nanonitrure de bore cubique ainsi que le nanonitrure de bore cubique ainsi obtenu. Le procédé de fabrication de nanonitrure de bore de structure cubique de l'invention est caractérisé en ce qu'il comprend les étapes suivantes : a) compression d'une poudre de nitrure de bore pyrolytique de structure de type graphite turbostratique monomodal à une pression comprise entre 19 et 21 GPa et à température ambiante et, b) chauffage sous une pression comprise entre 19 et 21 GPa de la poudre à une température comprise entre 1447°C (1720 K) et 1547°C (1820 K) pendant moins de 2 minutes. L'invention trouve application en particulier dans le domaine des matériaux abrasifs.
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP09784260A EP2318310A2 (fr) | 2008-07-11 | 2009-07-09 | Nanonitrure de bore cubique |
US13/003,651 US20110230122A1 (en) | 2008-07-11 | 2009-07-09 | Nanoscale cubic boron nitride |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR0803976 | 2008-07-11 | ||
FR0803976A FR2933690B1 (fr) | 2008-07-11 | 2008-07-11 | Nanonitrure de bore cubique |
Publications (2)
Publication Number | Publication Date |
---|---|
WO2010004142A2 WO2010004142A2 (fr) | 2010-01-14 |
WO2010004142A3 true WO2010004142A3 (fr) | 2010-03-04 |
Family
ID=40291318
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/FR2009/000852 WO2010004142A2 (fr) | 2008-07-11 | 2009-07-09 | Nanonitrure de bore cubique |
Country Status (4)
Country | Link |
---|---|
US (1) | US20110230122A1 (fr) |
EP (1) | EP2318310A2 (fr) |
FR (1) | FR2933690B1 (fr) |
WO (1) | WO2010004142A2 (fr) |
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8734748B1 (en) * | 2010-09-28 | 2014-05-27 | The United States Of America As Represented By The Administrator Of National Aeronautics And Space Administration | Purifying nanomaterials |
CN103569976B (zh) * | 2012-08-03 | 2016-09-14 | 燕山大学 | 超高硬度纳米孪晶氮化硼块体材料及其合成方法 |
US9150458B2 (en) | 2013-01-28 | 2015-10-06 | King Abdulaziz University | Method of increasing the hardness of wurtzite crystalline materials |
WO2018066261A1 (fr) * | 2016-10-06 | 2018-04-12 | 住友電気工業株式会社 | Procédé de production de polycristal de nitrure de bore, polycristal de nitrure de bore, outil de coupe, outil résistant à l'usure et outil de meulage |
WO2020066517A1 (fr) * | 2018-09-27 | 2020-04-02 | 住友電工ハードメタル株式会社 | Corps polycristallin de nitrure de bore cubique et son procédé de production |
WO2020175642A1 (fr) * | 2019-02-28 | 2020-09-03 | 住友電工ハードメタル株式会社 | Nitrure de bore cubique polycristallin et procédé de production associé |
WO2020174922A1 (fr) * | 2019-02-28 | 2020-09-03 | 住友電工ハードメタル株式会社 | Nitrure de bore cubique polycristallin et son procédé de production |
WO2020174923A1 (fr) * | 2019-02-28 | 2020-09-03 | 住友電工ハードメタル株式会社 | Nitrure de bore cubique polycristallin et son procédé de fabrication |
EP3932890A4 (fr) * | 2019-02-28 | 2022-04-27 | Sumitomo Electric Hardmetal Corp. | Nitrure de bore cubique polycristallin et son procédé de production |
CN110152558A (zh) * | 2019-05-28 | 2019-08-23 | 河南四方达超硬材料股份有限公司 | 一种超硬材料的烧结装置及其使用方法 |
KR20220078281A (ko) * | 2020-12-03 | 2022-06-10 | 삼성전자주식회사 | 비정질 질화 붕소막을 포함하는 하드 마스크 및 그 제조방법과, 하드마스크를 이용한 패터닝 방법 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0384857A1 (fr) * | 1989-02-20 | 1990-08-29 | Rhone-Poulenc Chimie | Procédé de préparation de nitrure de bore |
US6383465B1 (en) * | 1999-12-27 | 2002-05-07 | National Institute For Research In Inorganic Materials | Cubic boron nitride and its gas phase synthesis method |
-
2008
- 2008-07-11 FR FR0803976A patent/FR2933690B1/fr not_active Expired - Fee Related
-
2009
- 2009-07-09 WO PCT/FR2009/000852 patent/WO2010004142A2/fr active Application Filing
- 2009-07-09 EP EP09784260A patent/EP2318310A2/fr not_active Withdrawn
- 2009-07-09 US US13/003,651 patent/US20110230122A1/en not_active Abandoned
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0384857A1 (fr) * | 1989-02-20 | 1990-08-29 | Rhone-Poulenc Chimie | Procédé de préparation de nitrure de bore |
US6383465B1 (en) * | 1999-12-27 | 2002-05-07 | National Institute For Research In Inorganic Materials | Cubic boron nitride and its gas phase synthesis method |
Non-Patent Citations (6)
Title |
---|
BOLLO I ET AL: "Diamond and cubic boron nitride: synthesis and electronic applications", ADVANCED SEMICONDUCTOR DEVICES AND MICROSYSTEMS, 2002. THE FOURTH INTE RNATIONAL CONFERENCE ON 14-16 OCT 2002, PISCATAWAY, NJ, USA,IEEE, 14 October 2002 (2002-10-14), pages 1 - 11, XP010619349, ISBN: 978-0-7803-7276-4 * |
SACHDEV H: "Influence of impurities on the morphology and Raman spectra of cubic boron nitride", 1 August 2003, DIAMOND AND RELATED MATERIALS, ELSEVIER SCIENCE PUBLISHERS, AMSTERDAM, NL, PAGE(S) 1275 - 1286, ISSN: 0925-9635, XP004438859 * |
SAITOH H ET AL: "NUCLEATION OF BORON NITRIDE ON CUBIC BORON NITRIDE MICROCRYSTALLITEUSING CHEMICAL VAPOR DEPOSITION", APPLIED PHYSICS LETTERS, AIP, AMERICAN INSTITUTE OF PHYSICS, MELVILLE, NY, vol. 64, no. 13, 28 March 1994 (1994-03-28), pages 1638 - 1640, XP000441240, ISSN: 0003-6951 * |
THEVENIN P; SOLTANI A; BATH A: "Synthesis of cubic boron nitride thin films by microwave PECVD", CONFERENCE PAPER, 3RD INTERNATIONAL CONFERENCE, NOVEL APPLICATIONS OF WIDE BANDGAP LAYERS, ABSTRACT BOOK (CAT. NO.01EX500), 2001, Piscataway, NJ, USA, pages 118 - 119, XP002513415 * |
WERNINGHAUS T ET AL: "RAMAN SPECTROSCOPY INVESTIGATION OF SIZE EFFECTS IN CUBIC BORON NITRIDE", APPLIED PHYSICS LETTERS, AIP, AMERICAN INSTITUTE OF PHYSICS, MELVILLE, NY, vol. 70, no. 8, 24 February 1997 (1997-02-24), pages 958 - 960, XP001007781, ISSN: 0003-6951 * |
XU ZHANG: "Surface enhanced Raman study of cubic boron nitride", JOURNAL PAPER CHEMICAL PHYSICS LETTERS, vol. 373, no. 5-6, 28 May 2003 (2003-05-28), Netherlands, pages 506 - 512, XP002513414 * |
Also Published As
Publication number | Publication date |
---|---|
WO2010004142A2 (fr) | 2010-01-14 |
FR2933690A1 (fr) | 2010-01-15 |
FR2933690B1 (fr) | 2010-09-10 |
EP2318310A2 (fr) | 2011-05-11 |
US20110230122A1 (en) | 2011-09-22 |
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