WO2009085967A1 - Lubrifiant synthétique universel pénétrant, procédé et produit en résultant - Google Patents

Lubrifiant synthétique universel pénétrant, procédé et produit en résultant Download PDF

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Publication number
WO2009085967A1
WO2009085967A1 PCT/US2008/087449 US2008087449W WO2009085967A1 WO 2009085967 A1 WO2009085967 A1 WO 2009085967A1 US 2008087449 W US2008087449 W US 2008087449W WO 2009085967 A1 WO2009085967 A1 WO 2009085967A1
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Prior art keywords
weight
percent
solvent
penetrating lubricant
alpha
Prior art date
Application number
PCT/US2008/087449
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English (en)
Inventor
Ronald J. Sloan
Original Assignee
Bestline International Research, Inc.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Priority claimed from PCT/US2007/088252 external-priority patent/WO2009078882A1/fr
Application filed by Bestline International Research, Inc. filed Critical Bestline International Research, Inc.
Priority to US12/747,236 priority Critical patent/US8071513B2/en
Priority to JP2010539806A priority patent/JP2011508022A/ja
Priority to CN200880127051.3A priority patent/CN101952399B/zh
Priority to EP08867519A priority patent/EP2245122A1/fr
Priority to CA2710530A priority patent/CA2710530C/fr
Publication of WO2009085967A1 publication Critical patent/WO2009085967A1/fr
Priority to US12/887,834 priority patent/US8334244B2/en
Priority to HK11107522.9A priority patent/HK1153498A1/xx
Priority to US13/822,385 priority patent/US9309482B2/en

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    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M111/00—Lubrication compositions characterised by the base-material being a mixture of two or more compounds covered by more than one of the main groups C10M101/00 - C10M109/00, each of these compounds being essential
    • C10M111/04—Lubrication compositions characterised by the base-material being a mixture of two or more compounds covered by more than one of the main groups C10M101/00 - C10M109/00, each of these compounds being essential at least one of them being a macromolecular organic compound
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    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
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    • C10M141/00—Lubricating compositions characterised by the additive being a mixture of two or more compounds covered by more than one of the main groups C10M125/00 - C10M139/00, each of these compounds being essential
    • C10M141/08—Lubricating compositions characterised by the additive being a mixture of two or more compounds covered by more than one of the main groups C10M125/00 - C10M139/00, each of these compounds being essential at least one of them being an organic sulfur-, selenium- or tellurium-containing compound
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/34—Fragrance or deodorizing properties
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/60—Electro rheological properties
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/14—Electric or magnetic purposes
    • C10N2040/16—Dielectric; Insulating oil or insulators
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/14—Electric or magnetic purposes
    • C10N2040/17—Electric or magnetic purposes for electric contacts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/25—Internal-combustion engines
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2070/00—Specific manufacturing methods for lubricant compositions

Definitions

  • This invention relates to a synthetic penetrating lubricant capable of dissolving rust and corrosion caused by oxidation and harsh chemicals while offering extreme pressure lubrication capacities with a high dielectric protection.
  • This penetrating lubricant comprises alpha-olefins; low-odor aromatic solvents; and at least one a base oil selected from the base oil group consisting of hydrolsomerized high base oils and HT Severe Hydro-cracked Base Oils; as well as other ingredients. Also disclosed is a method for producing this penetrating lubricant.
  • universal synthetic penetrating lubricant for penetrating and dissolving rust and corrosion and cleaning metal and removing oxidation, while providing lubrication including extreme pressure lubrication, high dielectric protection, and corrosion resistance, comprising: alpha-olefins; low-odor aromatic solvents; at least one base oil selected from the base oil group consisting of hydrolsomerized high-base oils and HT severe hydro-cracked base oils; and high flash mineral spirits.
  • the invention relates to the use of a multi-functional penetrating lubricant with applications as a general penetrating liquid for dissolving and loosening of corrosion and rust caused by oxidation or harsh chemicals.
  • the invention further has the ability to penetrate into the crystalline surface of metal, leaving a lubricating film that is resistant to future corrosion. Further the invention leaves a barrier film that has extreme pressure capacity. Further the invention acts as a solvent to remove oxidation between electrical contacts to allow maximum flow of electricity while reducing resistance and heat associated with resistance. Although the invention cleans contacts for reduced resistance, it also isolates and insulates electrical contacts to protect them from moisture and other such elements which can cause electrical shorts and failure.
  • the invention demonstrates high dielectric strength while exhibiting the characteristics of a penetrant, lubricant, extreme pressure lubricant, and contact cleaner.
  • Alpha-Olefins This is a primary ingredient which is a derivative of linear alpha-olefins incorporating 1 -decene to distinguish it from other mono-olefins by way of polymerization and hydrogenation. These are also known as Alkenes, Polymerized Chlorowax Liquids, and Chlorinated Paraffins whose carbon chain length are C12, C14, C12-24, C16-18, C24-30 and C20-30 with said choleric weight percentage from 21.4% to 70%, an HCI of 4 to 10 ppm and molecular weight of 273.5 to 650 and Wt.
  • Cl (2) from 20 to 70% with specific gravity at 25 degrees centigrade of 1.050 to 1.50 and a JQD weight percentage of HCL being 0.20 to 0.60 maximum.
  • the primary use is for this ingredient is for lubricant formulations, lubricant additive compounds, extreme-pressure additive formulations and for metal working compounds.
  • alpha-olefins or associated products reduce the growth of algae in fuel as aging or excessive moisture accumulates and stabilize the fuel over time while providing extreme lubrication to the fuel system and the firing chamber of the engine.
  • Aromatic Solvents This is a primary ingredient which is a highly-refined, low toxic, low- odor solvent ideal for paints, varnishes, food grade coatings, adhesives, diluents, thinners, agrochemicals, household pesticides, a thinner for spray oils/lubricants and specialty chemicals.
  • Aromatic percentage is 5 to 40% (EC-A-G04), a flash point of 20 to 80 degrees centigrade (ASTM D-
  • Hydrolsomerized High-Base Oils or HT Severe Hydro-cracked Base Oils This primary ingredient is a severe hydro-cracked or hydrolsomerized base oil with low or no aromatics and impurities achieved by chemically reacting the feed stock with hydrogen (3000 P.S.I.) to reduce or remove polar compounds containing sulphur, nitrogen and oxygen and to convert aromatic hydrocarbons to saturated cyclic hydrocarbons breaking up the heavy polycyclo-paraffin molecules to light saturated hydrocarbons.
  • This may include fractionated oils that have been hydro-finished or hydro-polished.
  • the base oils can be used in a host of lubricating oils, motor oils, cutting oils, food processing, pharmaceutical, industry, agriculture lubricants and extreme pressure additives. These add to the lubrication of ultra low sulfur diesel fuel.
  • High Flash Mineral Spirits A colorless homogeneous solution with an evaporation rate of .11 (n- butyl acetate) and referred to as petroleum distillates that has been synthesized from selected hydrocarbons. This is often referred to as Stoddard Solvent #3 and / or Mineral Spirits, and is commonly used as an cleaning solvent, solvent in aerosols, paints, lacquers, varnishes and paint thinners for household and commercial use and has been subjected to hydrodesulfurization solvent extraction with a mixture of saturated aliphatic and alicyclic C7-C12 with a maximum of 40%.
  • the flash point ranges from 40 to 55 degrees centigrade, aniline point of 60 to 85 degrees centigrade and a vapor density of 0.758 (kg/L) at 15 degrees centigrade. This component assists in dissolving oxidation and is necessary when pressurizing the finished product in aerosol containers.
  • Synthetic Calcium Sulfonates An over based calcium sulfonate with a TBN of 100 to 600, which may be prepared from C20-C24 linear monoalkyl phenylsufonic acid, and whose primary purpose is for extreme pressure additive formulations offering corrosion protection, dispersants and detergency in oil soluble additives for ferrous and no-ferrous metals with a minimum calcium weight of 10.00 to
  • MIBK Methyl-Isobutyl Ketones
  • MIBK Formula (6H12) CAS 108-10-1, Flammable Liquid.
  • MIBK is general used a as solvent for vinyl, epoxy, acrylic and natural resins, nitrocellulose, paints, varnishes, lacquers, protective coatings, rare metal extractions and dyes. Further it is commonly used in manufacturing antibiotics, dry-cleaning preparations and the synthesis of methyl isobutyl carbinol. It occurs naturally in oranges, grapes and vinegar. It is colorless, has low boiling point, and is miscible in proportions with water, alcohols, most hydrocarbons and other organic liquids. MIBK has a flash point of 14 degrees centigrade.
  • MIBK is manufactured from acetones via a three-step process involving dimerised alcohol condensation to diacetone alcohol. Further diacetone readily hydrates to give mesityl oxides. Mesityl oxides can then be hydrogenated to MIBK. MIBK is used as a denaturing agent for denatured alcohols and as such lends itself a quick drying agent.
  • Solvent activated dyes An alcohol (NAHA) solution of polymer color forming compounds. These are commonly used to identify grades or designated uses of fuels and lubricants. They are produced in both powder and liquid form and when introduced to the product are stable and leave an identifiable color to the product.
  • NAHA an alcohol
  • Solvent- Activated Fragrance Alcohol-concentrated fragrance essence with an HA or NAHA of .005% to 1%. The active ingredient resists bacterial growth and contains a molecular encapulant (fixative) to maintain the selective fragrance uses to mask the chemical odor of certain compounds.
  • Blending Ratios The preferred blending ratios for each component are shown as below. It is important to maintain a blend of components that fall within the following percentages. Note that in the event one or more of the ingredients shown below is omitted from the penetrating lubricant, the percentages by weight of the remaining ingredients are proportionately increased:
  • Alpha-Olefins 2 to 30% by weight and preferably 7.0 to 25% by weight and more preferably 9.0 to 22% by weight. Most preferable is 17.0% by weight.
  • Low-odor Aromatic Solvents 2 to 25% by weight and preferably 4.5 to 18% by weight and more preferably 7 to 14% by weight. Most preferable is 9.4% by weight.
  • Hydrolsomerized High-Base Oils and HT Severe Hydro-cracked Base Oils 7 to 55% by weight and preferably 10 to 42% by weight and more preferably 15 to 35% by weight. Most preferable is 31.5% by weight.
  • High Flash Mineral Spirits 15 to 60% by weight and preferably 20 to 55% by weight and more preferably 25 to 49% by weight. Most preferable is 34.6% by weight.
  • Synthetic Calcium Sulfonates 0.05 to 1.05% by weight, preferably 0.25 to 0.95% by weight and more preferably 0.56 to 0.87% by weight. Most preferable is 0.833% by weight.
  • Methyl-Isobutyl Ketones 2.0 to 25% by weight and preferably 4 to 16% by weight and more preferably 5 to 11% by weight. Most preferable is 7.2%.
  • Solvent Activated Dyes 0.002 to 0.005% by weight and preferably 0.0025 to 0.004% by weight and more preferably 0.027 to 0.035% by weight. Most preferable is 0.003% by weight.
  • Solvent Activated Fragrances 0.001 to 0.005% by weight and preferably 0.0015 to 0.004 and more preferably 0.00175 to 0.003% by weight. Most preferable is 0.002% by weight.
  • Polytetrafluoroethylene (fluoroadditive): 0.012 to 0.097% by weight and preferably 0.022 to 0.0925% and more preferably 0.042 to 0.085% by weight. Most preferable is 0.0835 % by weight.
  • the initial blend (primary blend) will require the alpha olefins, the low-odor aromatic solvent and the base oils being blended until the liquid is a consistent amalgamation without any appearance of separation.
  • Blending is based on speed of the agitator and temperature will dictate the amount of time for the blend to complete.
  • the blending time range may vary from 4 to 6 hours.
  • the ideal temperature for each component is between 22 to 30 degrees centigrade for ideal blending. While this is blending, a secondary blend for the methyl isobutyl ketones, solvent activated dyes and solvent activated fragrance is prepared in a much smaller high-speed enclosed blender, and then added to the main blend.
  • the synthetic calcium sulfonates will be blended with the mineral spirits in an approximate .25/75 ratio in the initial stage of the blend to produce a tertiary blend.
  • the mineral spirits used will be from the preferred percentage set forth earlier.
  • This tertiary blend, or the mineral spirits alone absent the synthetic calcium sulfonates, together with the balance of the ingredients, can be then added to the main blend and the agitator is run until the components appear to have thoroughly blended into a consistent liquid.
  • Blend Equipment The process sequence involves a series of blending and holding tanks where the product can be weighed and then pumped through control valves to maintain consistent flow and pressure.
  • the blending should be performed in an enclosed tank to reduce product evaporation (loss) and prevent exposure to open spark.
  • Blending equipment can be by a combination of high or low speed blending apparatus. Size or volume of tank is not critical to the blend.
  • the product has been industrially tested, on an experimental basis, in extreme and harsh conditions.
  • the invention has been so-tested in various forms of machining, and in electrical applications where elements such as water are a constant source of shorting and electrical safety and failure are a concern.
  • the invention has been tested as an extreme pressure topical lubricant and has exceeded the performance of most lubricants available.
  • Finally the product has been severely tested, experimentally, in applications with extreme rust and corrosion and has demonstrated the ability to penetrate and loosen the same while leaving a protective barrier on the metal.
  • the product has shown its ability to work well with ferrous and non-ferrous material with profound results including the protection of brake rotors.

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Lubricants (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

L'invention concerne un lubrifiant pénétrant ayant la capacité de présenter une pénétration dans la rouille et la corrosion. De plus, ce lubrifiant pénètre activement la surface cristalline du métal tout en présentant une lubrification sous pression extrême, et une non migration avec une protection durable. De plus, le lubrifiant présente une résistance diélectrique supérieure à 8000 volts, en même temps qu'un nettoyage des contacts électriques, réduisant de ce fait la résistance et la chaleur associée. Le mode préféré de réalisation contient des alpha-oléfines, des solvants aromatiques à faible odeur, des huiles de base et des spiritueux minéraux à détente brusque élevée.
PCT/US2008/087449 2005-01-18 2008-12-18 Lubrifiant synthétique universel pénétrant, procédé et produit en résultant WO2009085967A1 (fr)

Priority Applications (8)

Application Number Priority Date Filing Date Title
US12/747,236 US8071513B2 (en) 2005-01-18 2008-12-18 Universal synthetic penetrating lubricant, method and product-by-process
JP2010539806A JP2011508022A (ja) 2007-12-19 2008-12-18 万能合成浸透性潤滑剤、方法およびプロダクトバイプロセス
CN200880127051.3A CN101952399B (zh) 2007-12-19 2008-12-18 通用的合成渗透润滑剂,方法和方法得到的产品
EP08867519A EP2245122A1 (fr) 2007-12-19 2008-12-18 Lubrifiant synthétique universel pénétrant, procédé et produit en résultant
CA2710530A CA2710530C (fr) 2007-12-19 2008-12-18 Lubrifiant synthetique universel penetrant, procede et produit en resultant
US12/887,834 US8334244B2 (en) 2005-01-18 2010-09-22 Universal synthetic water displacement multi-purpose penetrating lubricant, method and product-by-process
HK11107522.9A HK1153498A1 (en) 2007-12-19 2011-07-19 Universal synthetic penetrating lubricant, method and product-by-process
US13/822,385 US9309482B2 (en) 2005-01-18 2011-09-20 Universal synthetic water displacement multi-purpose penetrating lubricant, method and product-by-process

Applications Claiming Priority (6)

Application Number Priority Date Filing Date Title
USPCT/US2007/088252 2007-12-19
PCT/US2007/088252 WO2009078882A1 (fr) 2007-12-19 2007-12-19 Lubrifiant synthétique universel, procédé et produit obtenu à partir de ce procédé pour remplacer la lubrification au soufre perdu lors de l'utilisation de carburants diesels à faible teneur en soufre
PCT/US2008/050951 WO2009079020A1 (fr) 2007-12-19 2008-01-13 Produit nettoyant et protecteur de clubs de golf synthétique, procédé et produit obtenu par le procédé pour nettoyer, protéger les faces des clubs de golf et régénérer les poignées des clubs de golf
USPCT/US2008/050951 2008-01-13
US12/060,637 2008-04-01
US12/060,637 US8022020B2 (en) 2005-01-18 2008-04-01 Universal synthetic penetrating lubricant, method and product-by-process

Related Parent Applications (2)

Application Number Title Priority Date Filing Date
US11/290,596 Continuation-In-Part US7745382B2 (en) 2005-01-18 2005-12-01 Synthetic lubricant additive with micro lubrication technology to be used with a broad range of synthetic or miner host lubricants from automotive, trucking, marine, heavy industry to turbines including, gas, jet and steam
US12/060,637 Continuation-In-Part US8022020B2 (en) 2005-01-18 2008-04-01 Universal synthetic penetrating lubricant, method and product-by-process

Related Child Applications (5)

Application Number Title Priority Date Filing Date
US12/060,637 Continuation-In-Part US8022020B2 (en) 2005-01-18 2008-04-01 Universal synthetic penetrating lubricant, method and product-by-process
US12/290,596 A-371-Of-International US20090255215A1 (en) 2008-04-14 2008-10-30 Zipper registration using eye-mark encoder
US12/747,236 A-371-Of-International US8071513B2 (en) 2005-01-18 2008-12-18 Universal synthetic penetrating lubricant, method and product-by-process
US74723610A Continuation-In-Part 2005-01-18 2010-06-10
US12/887,834 Continuation-In-Part US8334244B2 (en) 2005-01-18 2010-09-22 Universal synthetic water displacement multi-purpose penetrating lubricant, method and product-by-process

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PCT/US2008/087433 WO2009085957A1 (fr) 2005-01-18 2008-12-18 Additif conditionneur d'essence synthétique universel, procédé et produit en résultant

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US (2) US8022020B2 (fr)
EP (2) EP2242821A1 (fr)
JP (1) JP2011508022A (fr)
CN (2) CN103865609B (fr)
CA (2) CA2710403C (fr)
HK (2) HK1153498A1 (fr)
WO (2) WO2009085967A1 (fr)

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US8071522B2 (en) 2005-01-18 2011-12-06 Bestline International Research, Inc. Universal synthetic golf club cleaner and protectant, method and product-by-process to clean, protect golf club faces and rejuvenate golf clubs grips
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US8071513B2 (en) 2011-12-06
CA2710530C (fr) 2016-07-05
US20080182769A1 (en) 2008-07-31
CA2710403A1 (fr) 2009-07-09
EP2242821A1 (fr) 2010-10-27
US8022020B2 (en) 2011-09-20
CA2710403C (fr) 2016-02-02
WO2009085957A1 (fr) 2009-07-09
EP2245122A1 (fr) 2010-11-03
HK1192900A1 (zh) 2014-09-05
CA2710530A1 (fr) 2009-07-09
CN101952399B (zh) 2014-01-01
CN103865609A (zh) 2014-06-18
CN101952399A (zh) 2011-01-19
HK1153498A1 (en) 2012-03-30
CN103865609B (zh) 2015-12-30
US20100273688A1 (en) 2010-10-28

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