WO2009034407A1 - Sustituto de grasa láctea y su proceso de obtención - Google Patents
Sustituto de grasa láctea y su proceso de obtención Download PDFInfo
- Publication number
- WO2009034407A1 WO2009034407A1 PCT/IB2007/002806 IB2007002806W WO2009034407A1 WO 2009034407 A1 WO2009034407 A1 WO 2009034407A1 IB 2007002806 W IB2007002806 W IB 2007002806W WO 2009034407 A1 WO2009034407 A1 WO 2009034407A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- approximately
- milk fat
- fractionation
- fat substitute
- production
- Prior art date
Links
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D7/00—Edible oil or fat compositions containing an aqueous phase, e.g. margarines
- A23D7/001—Spread compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
Definitions
- the present invention is related to a method for obtaining a milk fat substitute from vegetable oil and the product obtained by this method for the application in the field of the preparation of food products, which are generally prepared with fats derived from Milk
- the substitutes of the state of the art also have a high level of saturated short chain fatty acids, which are easily hydrolyzable, making the substitute unstable in the presence of water.
- Short chain acids among which are butyric, caproic, capric, caprylic and lauric acids, are noticeable to the palate even at very low concentrations.
- These fatty acids have flavor notes ranging from rancid to soapy, which are transmitted directly to the food produced with the substitutes of the state of the art. Therefore, it is clearly a felt need to obtain a substitute for milk fat that does not have or shows a sensitive decrease to the aforementioned problems.
- the product of the invention has the characteristics of a level of zero cholesterol, unlike those of the state of the art, as well as a much lower level of saturated fat, which makes it healthier.
- the product of the invention also contains a low level of saturated short chain fatty acids which gives greater stability to hydrolysis and therefore, food products made with this substitute have a longer shelf life, due to the fact that that unpleasant flavors are not easily generated.
- the product of the invention has some differences with respect to milk fat, which makes it more advantageous for its application in food products.
- Dairy fat tends to vary its fatty acid profile depending on the time of year, while the present product maintains its constant fatty acid profile.
- the amount of short chain fatty acids is smaller, compared with
- the product of the invention unlike milk fat, has a level of zero cholesterol.
- the product of the invention has greater flexibility in applications from the organoleptic point of view because it is possible to change the profiles of taste, smell and color, while with milk fat it is not possible to do this.
- US 5,395,629 describes a process for obtaining a milk fat substitute through the chemical or enzymatic interesterification of a hydrogenated vegetable oil rich in stearic acid with a vegetable oil rich in short chain fatty acids, such as caproic , caprylic and capric.
- the product obtained is 100% saturated, consisting solely of triglycerides of caproic, caprylic, capric, palmitic and stearic acids.
- the present invention provides a process for obtaining a milk fat substitute from vegetable oil, which comprises two stages of fractionation, and the milk fat substitute obtained, which comprises a mixture of the olein obtained in the first stage of fractionation with the olein obtained in the second stage of fractionation.
- said vegetable oil is palm oil.
- the product of the invention is used in the manufacture of edible products such as ice cream, cookies, cakes, bakery products, reconstituted milks, milk formulas and cheeses.
- the product of the invention has surprising advantages over milk fats of the state of the art such as a zero cholesterol content, low content of short chain saturated fatty acids and low level of total saturates.
- the present invention has as its object the production of milk fat substitutes and their process of obtaining from vegetable oils.
- the starting oil is palm oil of the species Elaeis guineensis, Elaeis oleifera (Elaeis melanocacca), or the fruit of the hybrids obtained from the crosses of E. guineensis x E. oleifera.
- the process for the production of milk fat substitutes of the invention comprises two stages of fractionation.
- the fractionation can be dynamic or static. Dynamic fractionation is carried out in dynamic crystallizers and maturators. Static fractionation It is carried out in trays which are kept in a cold room or in refrigerated plates.
- dynamic type fractionation is used.
- the oil is heated to a temperature in the range of approximately 60 ° C to 90 ° C 1 preferably in the range between approximately 75 ° C and 85 ° C.
- the fractionation time is between approximately , 8 to 20 hours. Preferably in the range of approximately 12 to 16 hours.
- the final temperature should be between approximately 14 ° C and 27 ° C, preferably between approximately 17 ° C to 24 ° C.
- the oil is subjected to a filtration process to obtain a liquid fraction known as olein and a solid fraction known as stearin.
- said filtration process can be carried out in a filter press.
- the feed pressure may be between approximately 50 and 500 kPa manometers, preferably between approximately 100 and 400 kPa manometers.
- the squeeze pressure must be between approximately 100 kPa at 1 MPa gauge, preferably between about 200 and 900 kPa gauge.
- the olein obtained could preferably have the following characteristics :
- the olein could have the following characteristics:
- the stearin obtained could preferably have the following characteristics:
- the esyearin could have the following characteristics:
- the stearin obtained in the first stage of fractionation is heated to a temperature in the range of approximately 60 ° C to 90 ° C, preferably in the range of approximately 75 ° C to 85 ° C.
- the fractionation time is between approximately 12 to 32 hours. Preferably in the range of approximately 14 to 24 hours.
- the final temperature should be between approximately 37 ° C and 47 ° C, preferably between approximately 39 ° C to 45 °
- the stearin is subjected to a second filtration process to obtain a second olein and a second stearin.
- the feed pressure must be between approximately 100 and 800 kPa manometers, preferably between approximately 200 and 700 kPa manometers.
- the squeeze pressure should be between approximately 1 to 3 MPa manometric, preferably between approximately 1, 2 and 2.4 MPa manometric.
- the olein obtained in this second fractionation should preferably have the following characteristics:
- the olein obtained in the second fractionation must have the following characteristics:
- a mixture of approximately 50 to 90% of the olein obtained in the first fractionation is made with approximately 10 to 50% of the olein of the second fractionation stage.
- the mixture must be between approximately 60 to 73% of the olein obtained in the first fractionation with between approximately 27 to 40% of the olein obtained in the second fractionation stage.
- the product of the invention is refined, bleached and deodorized, color, flavorings and emulsifiers are added and, finally, crystallized and packed.
- the product of the invention preferably has the following characteristics:
- the product has the following characteristics:
- the milk fat substitutes obtained with the process of the invention have advantageous characteristics with respect to those known in the state of the art, since they have a zero cholesterol content.
- these substitutes also have a lower level of saturated short-chain fatty acids that are not readily hydrolyzable making the substitute more stable in the presence of water. Therefore, fat does not develop odors or flavors that may interfere with the natural taste and smell of the food. Additionally, the percentage of saturated fat is low, which is convenient for the health of people who consume this type of products.
- the product of the invention is very suitable for the processing of food products such as ice cream, cookies, cakes, bakery products, reconstituted milk, milk formulas, cheeses and other products.
- Example 1 Obtaining milk fat substitute.
- Palm oil was taken, heated to 80 ° C and subjected to a 12-hour fractionation process and a final temperature of 18 ° C.
- the stearin obtained in this first fractionation was heated to 80 ° C again and fractionated during 24 hours and a final temperature of 42 ° C.
- 33% of the olein obtained in the second fractionation was mixed with 67% of the olein obtained in the first fractionation.
- the mixture was refined, bleached and deodorized. Color, flavorings and emulsifiers were added to the product obtained, then it was crystallized and packed.
- Curly cookies were made according to the following recipe: Components:
- the milk fat substitute obtained in example 1 was mixed at medium speed together with the sugar and salt for 10 minutes; the eggs were added along with the water and continued beating for 3 more minutes. Then the beating speed was reduced and the flour and milk were added.
- the product obtained was molded using a sleeve with a curly nozzle.
- the cookies were baked at 160 ° C for 14 minutes.
- the cookies obtained were powdery, soft, with open crumbs, golden and with butter flavor and smell
- the fat obtained in example 1 was used to reconstitute cow's milk; The following ingredients were used:
- the reconstituted milk was creamy with a texture and viscosity similar to those of natural whole milk.
- the viscosity of the reconstituted milk was 11.7 mPa.s at 25 ° C and the pH of 6.77.
- Example 1 Processing: on the water, the soy concentrate and the mixture of emulsifiers and stabilizers were added and heated to 40 ° C. Sugar and cocoa syrup were added, then the milk fat substitute obtained in Example 1 was added previously molten. This mixture was homogenized at 20 MPa and subjected to a UHT process. The product obtained was creamy and with a very good flavor, comparable to the chocolate milk soybeans found in the market.
- the water was mixed with the milk and the salts and allowed to hydrate for 20 minutes at 40 ° C.
- the integrated mixture of emulsifiers and stabilizers and the previously melted fat were added. It was pasteurized at 80 ° C for 5 minutes. The mixture was homogenized at 10 MPa. The product was then cooled to a temperature of 20 ° C and refrigerated.
- a tablespoon of the coffee cream substitute was added to a cup of hot coffee.
- the substitute dispersed easily and gave the coffee a good body and creaminess.
- the taste and aroma of the hot drink were very pleasant.
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Microbiology (AREA)
- Polymers & Plastics (AREA)
- Food Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Edible Oils And Fats (AREA)
- Dairy Products (AREA)
- Fats And Perfumes (AREA)
- Confectionery (AREA)
Abstract
Description
Claims
Priority Applications (7)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2010524584A JP2010539277A (ja) | 2007-09-13 | 2007-09-13 | 乳脂肪代替物及びその製造方法 |
US12/678,084 US8435591B2 (en) | 2007-09-13 | 2007-09-13 | Milk fat substitute and production method therefor |
EP07804981A EP2196524A4 (en) | 2007-09-13 | 2007-09-13 | SUBSTITUTE OF MILK FAT AND METHOD OF OBTAINING THE SAME |
PCT/IB2007/002806 WO2009034407A1 (es) | 2007-09-13 | 2007-09-13 | Sustituto de grasa láctea y su proceso de obtención |
BRPI0722007-3A BRPI0722007A2 (pt) | 2007-09-13 | 2007-09-13 | Processo para a produção de um substituto de gordura láctea e substituto de gordura láctea |
MX2010002828A MX2010002828A (es) | 2007-09-13 | 2007-09-13 | Sustituto de grasa lactea y su proceso de obtencion. |
CL2010000215A CL2010000215A1 (es) | 2007-09-13 | 2010-03-12 | Proceso para elaborar un sustituto de grasa lactea que comprende: fraccionar el aceite; filtrar el aceite para obtener una fraccion de oleica y estearina; fraccionar la estearina; mezclar la oleica del primer y segundo fraccionamiento; refinar, blanquear, desodorizar, adicionar color, saborizante, emulsionante; cristalizar. |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PCT/IB2007/002806 WO2009034407A1 (es) | 2007-09-13 | 2007-09-13 | Sustituto de grasa láctea y su proceso de obtención |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2009034407A1 true WO2009034407A1 (es) | 2009-03-19 |
Family
ID=40451618
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/IB2007/002806 WO2009034407A1 (es) | 2007-09-13 | 2007-09-13 | Sustituto de grasa láctea y su proceso de obtención |
Country Status (7)
Country | Link |
---|---|
US (1) | US8435591B2 (es) |
EP (1) | EP2196524A4 (es) |
JP (1) | JP2010539277A (es) |
BR (1) | BRPI0722007A2 (es) |
CL (1) | CL2010000215A1 (es) |
MX (1) | MX2010002828A (es) |
WO (1) | WO2009034407A1 (es) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2055195A1 (fr) * | 2007-10-29 | 2009-05-06 | Corman S.A. | Procédé de reduction de la teneur en acides gras saturés de la matiere grasse du lait , produits obtenus et applications de ceux-ci. |
Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1444820A (en) * | 1972-10-31 | 1976-08-04 | Unilever Ltd | Food fat |
US4447462A (en) * | 1981-11-04 | 1984-05-08 | The Procter & Gamble Company | Structural fat and method for making same |
US5395629A (en) | 1992-11-12 | 1995-03-07 | Nestec S.A. | Preparation of butterfat and vegetable butter substitutes |
ES2076293T3 (es) * | 1989-05-23 | 1995-11-01 | Unilever Nv | Cristalizacion fraccionada en seco en contracorriente. |
ES2136322T3 (es) * | 1994-12-23 | 1999-11-16 | Unilever Nv | Fraccionamiento de aceites trigliceridos. |
US20050276900A1 (en) * | 2004-06-14 | 2005-12-15 | Ullanoormadam Sahasranamam R | Trans free non-hydrogenated hard structural fat and non-hydrogenated hard palm oil fraction component |
ES2246287T3 (es) * | 2000-05-29 | 2006-02-16 | Premium Vegetable Oils Berhad | Grasa estructural solida, libre de acidos grasos trans para mezclas de margarina y pastas para untar. |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CH658163A5 (fr) * | 1983-10-07 | 1986-10-31 | Nestle Sa | Procede de production de fractions comestibles de matieres grasses et leur utilisation. |
-
2007
- 2007-09-13 WO PCT/IB2007/002806 patent/WO2009034407A1/es active Application Filing
- 2007-09-13 MX MX2010002828A patent/MX2010002828A/es active IP Right Grant
- 2007-09-13 EP EP07804981A patent/EP2196524A4/en not_active Withdrawn
- 2007-09-13 US US12/678,084 patent/US8435591B2/en not_active Expired - Fee Related
- 2007-09-13 BR BRPI0722007-3A patent/BRPI0722007A2/pt not_active IP Right Cessation
- 2007-09-13 JP JP2010524584A patent/JP2010539277A/ja not_active Ceased
-
2010
- 2010-03-12 CL CL2010000215A patent/CL2010000215A1/es unknown
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1444820A (en) * | 1972-10-31 | 1976-08-04 | Unilever Ltd | Food fat |
US4447462A (en) * | 1981-11-04 | 1984-05-08 | The Procter & Gamble Company | Structural fat and method for making same |
ES2076293T3 (es) * | 1989-05-23 | 1995-11-01 | Unilever Nv | Cristalizacion fraccionada en seco en contracorriente. |
US5395629A (en) | 1992-11-12 | 1995-03-07 | Nestec S.A. | Preparation of butterfat and vegetable butter substitutes |
ES2136322T3 (es) * | 1994-12-23 | 1999-11-16 | Unilever Nv | Fraccionamiento de aceites trigliceridos. |
ES2246287T3 (es) * | 2000-05-29 | 2006-02-16 | Premium Vegetable Oils Berhad | Grasa estructural solida, libre de acidos grasos trans para mezclas de margarina y pastas para untar. |
US20050276900A1 (en) * | 2004-06-14 | 2005-12-15 | Ullanoormadam Sahasranamam R | Trans free non-hydrogenated hard structural fat and non-hydrogenated hard palm oil fraction component |
Non-Patent Citations (3)
Title |
---|
ARNAUD E. ET AL.: "Thermal characterization of chicken fat dry fractionation process", JOURNAL OF FOOD ENGINEERING, vol. 72, no. 4, 1 February 2006 (2006-02-01), pages 390 - 397, XP025028841 * |
KELLENS M. ET AL.: "Palm oil fractionation", EUROPEAN JOURNAL OF LIPID SCIENCE TECHNOLOGY, vol. 109, no. 4, April 2007 (2007-04-01), pages 336 - 349, XP008132353 * |
See also references of EP2196524A4 |
Also Published As
Publication number | Publication date |
---|---|
JP2010539277A (ja) | 2010-12-16 |
BRPI0722007A2 (pt) | 2014-09-23 |
CL2010000215A1 (es) | 2010-12-31 |
US20100303992A1 (en) | 2010-12-02 |
EP2196524A1 (en) | 2010-06-16 |
EP2196524A4 (en) | 2012-11-14 |
MX2010002828A (es) | 2010-04-01 |
US8435591B2 (en) | 2013-05-07 |
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